CN207769801U - A kind of spiral reaction kettle - Google Patents

A kind of spiral reaction kettle Download PDF

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Publication number
CN207769801U
CN207769801U CN201721917314.3U CN201721917314U CN207769801U CN 207769801 U CN207769801 U CN 207769801U CN 201721917314 U CN201721917314 U CN 201721917314U CN 207769801 U CN207769801 U CN 207769801U
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reactor body
reactor
gas channel
gas
liquid
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易苗
任应能
缪永奕
武长安
毛伟
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Zhejiang Jitai New Material Co ltd
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ZHEJIANG LINJIANG CHEMICAL Co Ltd
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Abstract

本实用新型公开一种螺旋式反应釜,包括反应釜本体,该反应釜本体的顶部设有液体加料口,底部为平底;设有伸入所述反应釜本体底部的布气管,所述布气管内设有第一气体通道和第二气体通道,以及与所述第一气体通道和第二气体通道连通的出气孔;所述反应釜本体的底部安装有驱动电机,该驱动电机连接有伸入反应釜本体内的搅拌螺旋;所述反应釜本体的中部内壁间隔设置4~8块扰流板,扰流板的高度为所述反应釜本体的1/5~1/3。本实用新型结构简单,设计合理,利用底部伸入的搅拌螺旋,使气体快速扩散至液体的顶部,两者混合均匀,充分接触反应,提升产品的合格率。

The utility model discloses a spiral reactor, which comprises a reactor body. The top of the reactor body is provided with a liquid feeding port and the bottom is a flat bottom; an air distribution pipe extending into the bottom of the reactor body is provided, and the air distribution pipe There are a first gas channel and a second gas channel inside, and an air outlet that communicates with the first gas channel and the second gas channel; a drive motor is installed on the bottom of the reaction kettle body, and the drive motor is connected with a protruding A stirring screw in the reactor body; 4 to 8 spoilers are arranged at intervals on the inner wall of the middle of the reactor body, and the height of the spoilers is 1/5 to 1/3 of the reactor body. The utility model is simple in structure and reasonable in design. The gas is quickly diffused to the top of the liquid by using the stirring screw extending from the bottom, and the two are evenly mixed, fully contacted and reacted, and the qualified rate of the product is improved.

Description

一种螺旋式反应釜A spiral reactor

技术领域technical field

本实用新型涉及化工设备领域,尤其涉及一种螺旋式反应釜。The utility model relates to the field of chemical equipment, in particular to a spiral reaction kettle.

背景技术Background technique

反应釜是综合反应容器,根据反应条件对反应釜结构功能及配置附件的设计。从开始的进料-反应-出料均能够以较高的自动化程度完成预先设定好的反应步骤,对反应过程中的温度、压力、力学控制(搅拌、鼓风等)、反应物/产物浓度等重要参数进行严格的调控。其结构一般由釜体、传动装置、搅拌装置、加热装置、冷却装置、密封装置组成。相应配套的辅助设备:分馏柱、冷凝器、分水器、收集罐、过滤器等。The reactor is a comprehensive reaction vessel, and the structure, function and configuration accessories of the reactor are designed according to the reaction conditions. From the initial feeding-reaction-discharging, the preset reaction steps can be completed with a high degree of automation, and the temperature, pressure, mechanical control (stirring, blasting, etc.), reactants/products during the reaction process Important parameters such as concentration are strictly regulated. Its structure is generally composed of kettle body, transmission device, stirring device, heating device, cooling device and sealing device. Corresponding supporting auxiliary equipment: fractionation column, condenser, water separator, collection tank, filter, etc.

在气液反应装置中,为使气体与液体充分接触,一般采用气体从下部通入,液体从上部通入的方式;但是在现有的反应釜中,并不能使气体与液体完全充分混合,尤其是液体扩散至顶部的速度较慢,导致反应不够均匀。In the gas-liquid reaction device, in order to fully contact the gas and the liquid, the gas is generally introduced from the bottom and the liquid is passed from the top; but in the existing reactor, the gas and the liquid cannot be fully mixed. In particular, the liquid diffuses to the top more slowly, resulting in a less uniform reaction.

实用新型内容Utility model content

针对现有技术中存在的问题,本实用新型提供一种螺旋式反应釜,利用底部伸入的搅拌螺旋,使气体快速扩散至液体的顶部,两者混合均匀,充分接触反应,提升产品的合格率。Aiming at the problems existing in the prior art, the utility model provides a spiral reaction kettle, which uses the stirring spiral extending from the bottom to rapidly diffuse the gas to the top of the liquid, mix the two evenly, fully contact the reaction, and improve the qualification of the product Rate.

本实用新型采用的具体技术方案如下:The concrete technical scheme that the utility model adopts is as follows:

一种螺旋式反应釜,包括反应釜本体,该反应釜本体的顶部设有液体加料口,底部为平底;A spiral reactor, comprising a reactor body, the top of the reactor body is provided with a liquid feeding port, and the bottom is a flat bottom;

设有伸入所述反应釜本体底部的布气管,所述布气管内设有第一气体通道和第二气体通道,以及与所述第一气体通道和第二气体通道连通的出气孔;A gas distribution pipe extending into the bottom of the reaction kettle body is provided, and a first gas channel and a second gas channel are arranged in the gas distribution tube, as well as an air outlet communicating with the first gas channel and the second gas channel;

所述反应釜本体的底部安装有驱动电机,该驱动电机连接有伸入反应釜本体内的搅拌螺旋;The bottom of the reactor body is equipped with a drive motor connected with a stirring screw extending into the reactor body;

所述反应釜本体的中部内壁间隔设置4~8块扰流板,扰流板的高度为所述反应釜本体的1/5~1/3。The middle inner wall of the reactor body is provided with 4 to 8 spoilers at intervals, and the height of the spoilers is 1/5 to 1/3 of the reactor body.

本实用新型中,两种与液体混合反应的气体由布气管内的第一气体通道和第二气体通道通入,在扰流板与所述搅拌螺旋的作用下,快速向上扩散,与液充分混合接触反应。In the utility model, two kinds of gas mixed and reacted with the liquid are introduced through the first gas channel and the second gas channel in the gas distribution pipe, and under the action of the spoiler and the stirring screw, they diffuse upward quickly and fully mix with the liquid. contact reaction.

所述的扰流板与搅拌螺旋保持平行,但与釜体内壁保持倾斜,角度在30~60度之间,加快液体与气体的混合。The spoiler is kept parallel to the stirring spiral, but is kept inclined to the inner wall of the kettle, and the angle is between 30° and 60°, so as to speed up the mixing of liquid and gas.

为避免液体停留在扰流板间,应合理设置扰流板的长度,如扰流板的高度为所述反应釜本体的1/5~1/3,使扰流板的上部和下部均留有空间,提升液体的流动性。In order to prevent the liquid from staying between the baffles, the length of the baffles should be set reasonably, for example, the height of the baffles is 1/5-1/3 of the reactor body, so that the upper and lower parts of the baffles are left There is space to enhance the fluidity of the liquid.

为使扩散后的气体与液体继续保持流动性,作为优选的,所述反应釜本体的顶部安装有电机,连接有伸入反应釜本体内的搅拌叶。In order to maintain the fluidity of the diffused gas and liquid, preferably, a motor is installed on the top of the reactor body, and a stirring blade extending into the reactor body is connected.

为提供反应所需的温度,作为优选的,所述的扰流板的至少一侧表面设有加热盘管,加热反应釜内的气体和液体。In order to provide the temperature required for the reaction, preferably, at least one side surface of the spoiler is provided with a heating coil to heat the gas and liquid in the reactor.

作为优选的,所述布气管与反应釜本体外的进气接头连接,所述进气接头上设置有第一进气口和第二进气口,气体通过两个进气口分别进入两个气体通道,最终扩散至反应釜内。As preferably, the air distribution pipe is connected to the air inlet joint outside the reactor body, the air inlet joint is provided with a first air inlet and a second air inlet, and the gas enters two air inlets respectively through the two air inlets. The gas channel eventually diffuses into the reactor.

本实用新型结构简单,设计合理,利用底部伸入的搅拌螺旋,使气体快速扩散至液体的顶部,两者混合均匀,充分接触反应,提升产品的合格率。The utility model has the advantages of simple structure and reasonable design. The gas is quickly diffused to the top of the liquid by using the stirring screw extending from the bottom, and the two are evenly mixed, fully contacted and reacted, and the qualified rate of the product is improved.

附图说明Description of drawings

图1为本实用新型中反应釜的结构图;Fig. 1 is the structural diagram of reactor in the utility model;

图2为布气管的剖视图。Figure 2 is a cross-sectional view of the air distribution pipe.

具体实施方式Detailed ways

下面结合实施例和附图来详细说明本实用新型,但本实用新型并不仅限于此。The utility model is described in detail below in conjunction with embodiment and accompanying drawing, but the utility model is not limited thereto.

如图1和图2所示的螺旋式反应釜,包括反应釜本体1,该反应釜本体1的顶部设有液体加料口2,底部为平底;设有伸入反应釜本体1底部的布气管10,布气管10内设有第一气体通道14和第二气体通道15,以及与第一气体通道14和第二气体通道15连通的出气孔16;反应釜本体1的底部安装有驱动电机7,该驱动电机7连接有伸入反应釜本体1内的搅拌螺旋8;反应釜本体1的中部内壁间隔设置4~8块扰流板6。The spiral reactor shown in Figure 1 and Figure 2 includes a reactor body 1, the top of which is provided with a liquid feeding port 2, and the bottom is a flat bottom; 10. The gas distribution pipe 10 is provided with a first gas channel 14 and a second gas channel 15, and an air outlet 16 communicating with the first gas channel 14 and the second gas channel 15; the bottom of the reactor body 1 is equipped with a drive motor 7 The driving motor 7 is connected with a stirring screw 8 protruding into the reactor body 1; the middle inner wall of the reactor body 1 is provided with 4 to 8 spoilers 6 at intervals.

本实施例中,两种与液体混合反应的气体由布气管10内的第一气体通道和第二气体通道通入,在扰流板6与搅拌螺旋8的作用下,快速向上扩散,与液充分混合接触反应。In this embodiment, two kinds of gas mixed and reacted with the liquid are introduced through the first gas channel and the second gas channel in the gas distribution pipe 10, and under the action of the spoiler 6 and the stirring screw 8, they diffuse upward quickly and fully mix with the liquid. Mixed contact reactions.

扰流板6与搅拌螺旋8保持平行,但与釜体内壁保持倾斜,角度在30~60度之间,加快液体与气体的混合。为避免液体停留在扰流板间,应合理设置扰流板的长度,如扰流板6的高度为反应釜本体1的1/5~1/3,使扰流板的上部和下部均留有空间,提升液体的流动性。The spoiler 6 is kept parallel to the stirring screw 8, but is kept inclined with the inner wall of the kettle, and the angle is between 30 and 60 degrees, so as to speed up the mixing of liquid and gas. In order to prevent the liquid from staying between the spoilers, the length of the spoilers should be set reasonably. For example, the height of the spoiler 6 is 1/5-1/3 of the reactor body 1, so that the upper and lower parts of the spoiler are left There is space to enhance the fluidity of the liquid.

为使扩散后的气体与液体继续保持流动性,反应釜本体1的顶部安装有电机3,连接有伸入反应釜本体内的搅拌轴4和搅拌叶5。In order to maintain the fluidity of the diffused gas and liquid, a motor 3 is installed on the top of the reactor body 1, and a stirring shaft 4 and a stirring blade 5 extending into the reactor body are connected.

为提供反应所需的温度,扰流板6的至少一侧表面设有加热盘管9,加热反应釜内的气体和液体。In order to provide the temperature required for the reaction, at least one side surface of the spoiler 6 is provided with a heating coil 9 to heat the gas and liquid in the reactor.

布气管10与反应釜本体外的进气接头11连接,进气接头11上设置有第一进气口12和第二进气口13,气体通过两个进气口分别进入两个气体通道,最终扩散至反应釜内。The air distribution pipe 10 is connected with the air inlet joint 11 outside the reactor body, the air inlet joint 11 is provided with a first air inlet 12 and a second air inlet 13, and the gas enters two gas passages respectively through the two air inlets, Finally diffused into the reactor.

以上所述仅为本实用新型的较佳实施举例,并不用于限制本实用新型,凡在本实用新型精神和原则之内,所作的任何修改、等同替换、改进等,均应包含在本实用新型的保护范围之内。The above descriptions are only examples of the preferred implementation of the present utility model, and are not intended to limit the present utility model. Any modifications, equivalent replacements, improvements, etc. made within the spirit and principles of the present utility model shall be included in the present utility model. within the scope of the new protection.

Claims (4)

1.一种螺旋式反应釜,其特征在于,包括反应釜本体,该反应釜本体的顶部设有液体加料口,底部为平底;1. A spiral reactor, characterized in that, comprises a reactor body, the top of the reactor body is provided with a liquid feeding port, and the bottom is a flat bottom; 设有伸入所述反应釜本体底部的布气管,所述布气管内设有第一气体通道和第二气体通道,以及与所述第一气体通道和第二气体通道连通的出气孔;A gas distribution pipe extending into the bottom of the reactor body is provided, and a first gas channel and a second gas channel are arranged in the gas distribution tube, as well as an air outlet communicating with the first gas channel and the second gas channel; 所述反应釜本体的底部安装有驱动电机,该驱动电机连接有伸入反应釜本体内的搅拌螺旋;The bottom of the reactor body is equipped with a drive motor connected with a stirring screw extending into the reactor body; 所述反应釜本体的中部内壁间隔设置4~8块扰流板,扰流板的高度为所述反应釜本体的1/5~1/3。The middle inner wall of the reactor body is provided with 4 to 8 spoilers at intervals, and the height of the spoilers is 1/5 to 1/3 of the reactor body. 2.如权利要求1所述的螺旋式反应釜,其特征在于,所述反应釜本体的顶部安装有电机,连接有伸入反应釜本体内的搅拌叶。2. The spiral reactor according to claim 1, wherein a motor is installed on the top of the reactor body, and a stirring blade extending into the reactor body is connected. 3.如权利要求1所述的螺旋式反应釜,其特征在于,所述的扰流板的至少一侧表面设有加热盘管。3. The spiral reactor according to claim 1, characterized in that, at least one side surface of the spoiler is provided with a heating coil. 4.如权利要求1所述的螺旋式反应釜,其特征在于,所述布气管与反应釜本体外的进气接头连接,所述进气接头上设置有第一进气口和第二进气口。4. The spiral reactor according to claim 1, wherein the air distribution pipe is connected with an air inlet joint outside the reactor body, and the air inlet joint is provided with a first air inlet and a second air inlet. breath.
CN201721917314.3U 2017-12-31 2017-12-31 A kind of spiral reaction kettle Expired - Fee Related CN207769801U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108905946A (en) * 2018-09-05 2018-11-30 上海世卿防滑防护科技有限公司 A kind of novel gas-liquid reaction kettle and its stirring mixing method

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108905946A (en) * 2018-09-05 2018-11-30 上海世卿防滑防护科技有限公司 A kind of novel gas-liquid reaction kettle and its stirring mixing method
CN108905946B (en) * 2018-09-05 2024-01-23 上海世卿防滑防护科技有限公司 Novel gas-liquid reaction kettle and stirring and mixing method thereof

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Address after: 312369, No. three, No. 8, Shangyu economic and Technological Development Zone, Hangzhou Bay, Zhejiang, Shaoxing, China

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