CN207738679U - 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill - Google Patents

2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill Download PDF

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Publication number
CN207738679U
CN207738679U CN201721811281.4U CN201721811281U CN207738679U CN 207738679 U CN207738679 U CN 207738679U CN 201721811281 U CN201721811281 U CN 201721811281U CN 207738679 U CN207738679 U CN 207738679U
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washing machine
liquid
tank
propen
chloromethyl
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CN201721811281.4U
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杜德平
沈平
曹忠诚
王宜运
王锡春
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Shandong Xinhua Pharmaceutical Co Ltd
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Shandong Xinhua Pharmaceutical Co Ltd
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Abstract

The utility model belongs to pharmaceutical technology field, and in particular to a kind of separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate.The separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate described in the utility model, including filtration washing machine, salt-forming reaction tank, washing liquid tank, mother liquor tank and washing mother liquor holding tank;The discharge port of salt-forming reaction tank is connect with the feed inlet of filtration washing machine, the discharge port of washing liquid tank is connect with the feed inlet of filtration washing machine, the feed inlet of mother liquor tank is connected with the liquid outlet of filtration washing machine, and the feed inlet for washing mother liquor holding tank is connected with the liquid outlet of filtration washing machine.2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate described in the utility model is separated by solid-liquid separation and wash mill, it is scientific and reasonable, structure design is simple, by mother liquor press filtration it is complete after, then with cleaning solution 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate solid is washed, integrate filtering and washing, operating environment is improved, the process time is shortened, is improved work efficiency, reduce energy consumption, with good economic efficiency and social benefit.

Description

2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill
Technical field
The utility model is related to a kind of separation of solid and liquid of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate and wash mills, belong to pharmaceutical equipment technology neck Domain.
Background technology
2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is a kind of polymer that will not be absorbed by the body, and is free of metal and calcium.It carries multiple amidos, It is connect with polymer backbone by a carbon atom.These amidos can be protonated in enteron aisle inside points, and with ion exchange and hydrogen bond It is combined with phosphoric acid molecules.2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate reduces its absorption, reaching reduces serium inorganic phosphorus concentration by combining the phosphorus in gastrointestinal tract Effect.
It is domestic at present and in the world in 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate production, it is to carry out after the completion of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate reaction mostly It is centrifuged repeatedly, washs, complex process, the complex for operation step and time is longer, therefore in order to shorten the process time and improve environment Friendliness simultaneously makes up the market vacancy, and it is very necessary to develop the process unit being simple to operate and friendly to environment.
Utility model content
According to the above-mentioned deficiencies of the prior art, the technical problems to be solved in the utility model is:A kind of carbonic acid department dimension is provided The separation of solid and liquid and wash mill for drawing nurse can shorten the production cycle, improve working efficiency.
The separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate described in the utility model, including filtration washing machine, at salt Retort, washing liquid tank, mother liquor tank and washing mother liquor holding tank;The discharge port of salt-forming reaction tank is logical with the feed inlet of filtration washing machine Feeding pipe connection is crossed, the discharge port of washing liquid tank is connect with the feed inlet of filtration washing machine by feeding pipe, mother liquor tank Feed inlet is connected with the liquid outlet of filtration washing machine, and the feed inlet for washing mother liquor holding tank is connected with the liquid outlet of filtration washing machine.
The material that salt-forming reaction tank generates enters filtration washing machine by feeding pipe and is filtered, and the mother liquor filtered out is logical The liquid outlet for crossing filtration washing machine enters mother liquor tank, and 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate solid then stays in filtration washing machine;Filtering is completed Afterwards, cleaning solution enters filtration washing machine by feeding pipe and is washed to 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate solid;After washing, carbonic acid Sevelamer is discharged from filtration washing machine.
The filtration washing machine is connected with pressure gas cylinder, and pressure gas cylinder can be adjusted in filtration washing machine Mother liquor in filtration washing machine is pressed into mother liquor tank by gas pressure by liquid outlet.
The filtration washing machine is connected with drier, drier to the 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate solid after filtration washing into Row drying.
The filtration washing machine includes driving motor, and driving motor is located at filtration washing machine top, for agitating shaft with stir It mixes paddle and power is provided, driving motor is connect by agitating shaft with agitating paddle, and filtration washing machine is internally provided with filter plate, and filter plate setting exists Filtration washing motor spindle, filter plate is as filter medium, and under the action of pressure difference, solid material is retained by filter plate, and mother liquor from Filter plate passes through, to achieve the purpose that separation of solid and liquid.
Possessed advantageous effect is the utility model compared with prior art:
2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate described in the utility model is separated by solid-liquid separation and wash mill, and scientific and reasonable, structure design is simple, By mother liquor press filtration it is complete after, then with cleaning solution 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate solid is washed, integrates filtering and washing, improve Operating environment shortens the process time, improves work efficiency, and reduces energy consumption, with good economic efficiency and social effect Benefit.
Description of the drawings
Fig. 1 is the structural schematic diagram of the utility model;
Fig. 2 is the structural schematic diagram of filtration washing machine.
In figure:1, filtration washing machine;2, salt-forming reaction tank;3, washing liquid tank;4, mother liquor tank;5, drier;6, high pressure gas Body steel cylinder;7, mother liquor holding tank is washed;8, feeding pipe;9, filtration washing machine discharge port;10, liquid outlet;11, filter plate;12, it stirs Paddle;13, agitating shaft;14, driving motor.
Specific implementation mode
The utility model is described further with reference to embodiment:
The separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate described in the utility model, including filtration washing machine 1, at salt Retort 2, washing liquid tank 3, mother liquor tank 4 and washing mother liquor holding tank 7;The discharge port of salt-forming reaction tank 2 passes through feeding pipe 8 and mistake The feed inlet of filter washing machine 1 connects, and the discharge port of washing liquid tank 3 is connected by the feed inlet of feeding pipe 8 and filtration washing machine 1 It connects, the feed inlet of mother liquor tank 4 is connected with the liquid outlet 10 of filtration washing machine 1, washs the feed inlet and filtration washing of mother liquor holding tank 7 The liquid outlet 10 of machine 1 is connected.Filtration washing machine discharge port 9 is connected with drier 5, and filtration washing machine 1 is also associated with high pressure gas Steel cylinder 6.Filtration washing machine 1 includes driving motor 14, and driving motor 14 is located at 1 top of filtration washing machine, by agitating shaft 13 and Agitating paddle 12 connects, and filtration washing machine 1 is internally provided with filter plate 11.
The course of work or operation principle of the utility model:
By 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate indentation filtration washing machine 1 obtained by the reaction in salt-forming reaction tank 2, by filtration washing machine 1 Agitating paddle 12 rises to a high position, and it is 0.25MPa to open pressure gas cylinder 6 and adjust gas pressure in filtration washing machine 1, and mother liquor is led to It crosses liquid outlet 10 and is pressed into mother liquor tank 4 until no liquid outflow, drops to surface of material by agitating paddle 12 and open, material is flattened Afterwards, stop stirring, press filtration 0.5-1 hours.After the completion of filtering, pressure in filtration washing machine 1 is emptied, it will be in washing liquid tank 3 Cleaning solution is put into filtration washing machine 1, opens agitating paddle 12, and mashing washing forms washing mother liquor for 1 hour, after washing, incited somebody to action The agitating paddle 12 of filter washing machine 1 rises to a high position, opens gas pressure in the adjusting filtration washing of pressure gas cylinder 6 machine 1 and is Agitating paddle 12 is dropped to material table by 0.25MPa at this time by washing mother liquor indentation washing mother liquor holding tank 7 until no liquid flows out Face is simultaneously opened, and after material is flattened, stops stirring, press filtration 0.5-1 hours.After washing, pressure in filtration washing machine 1 is arranged Sky transfers the material into drying box 5, sets the temperature of drying box 5 as 60-70 DEG C, drying 24-30 hours obtains carbonic acid department Wella nurse.

Claims (4)

1. the separation of solid and liquid and wash mill of a kind of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate, it is characterised in that:Including filtration washing machine (1), at salt Retort (2), washing liquid tank (3), mother liquor tank (4) and washing mother liquor holding tank (7);The discharge port of salt-forming reaction tank (2) and filtering The feed inlet of rinsing maching (1) connects, and the discharge port of washing liquid tank (3) is connect with the feed inlet of filtration washing machine (1), mother liquor tank (4) feed inlet is connected with the liquid outlet (10) of filtration washing machine (1), the feed inlet and filtration washing of washing mother liquor holding tank (7) The liquid outlet (10) of machine (1) is connected.
2. the separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate according to claim 1, it is characterised in that:The mistake Filter washing machine (1) is connected with pressure gas cylinder (6).
3. the separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate according to claim 1, it is characterised in that:The mistake Filter washing machine (1) is connected with drier (5).
4. the separation of solid and liquid and wash mill of 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate according to claim 1, it is characterised in that:The mistake Filter washing machine (1) includes driving motor (14), and driving motor (14) is connect by agitating shaft (13) with agitating paddle (12), crosses diafiltration It washs machine (1) and is internally provided with filter plate (11).
CN201721811281.4U 2017-12-21 2017-12-21 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill Active CN207738679U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721811281.4U CN207738679U (en) 2017-12-21 2017-12-21 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721811281.4U CN207738679U (en) 2017-12-21 2017-12-21 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill

Publications (1)

Publication Number Publication Date
CN207738679U true CN207738679U (en) 2018-08-17

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CN201721811281.4U Active CN207738679U (en) 2017-12-21 2017-12-21 2-Propen-1-amine polymer with(chloromethyl)oxirane carbonate is separated by solid-liquid separation and wash mill

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CN (1) CN207738679U (en)

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