CN207632730U - A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device - Google Patents
A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device Download PDFInfo
- Publication number
- CN207632730U CN207632730U CN201721650021.3U CN201721650021U CN207632730U CN 207632730 U CN207632730 U CN 207632730U CN 201721650021 U CN201721650021 U CN 201721650021U CN 207632730 U CN207632730 U CN 207632730U
- Authority
- CN
- China
- Prior art keywords
- reaction
- butylperoxyisopropyl carbonate
- tower
- hydrogen chloride
- isopropanol
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- YFLBCDPISIYMHR-UHFFFAOYSA-N C(OCCl)(OC(C)(C)OOCCCC)=O Chemical compound C(OCCl)(OC(C)(C)OOCCCC)=O YFLBCDPISIYMHR-UHFFFAOYSA-N 0.000 title claims abstract description 18
- 238000006243 chemical reaction Methods 0.000 claims abstract description 48
- 239000002994 raw material Substances 0.000 claims description 8
- 238000003541 multi-stage reaction Methods 0.000 claims 1
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 abstract description 29
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract description 22
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract description 18
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract description 18
- 239000007789 gas Substances 0.000 abstract description 13
- JYWJULGYGOLCGW-UHFFFAOYSA-N chloromethyl chloroformate Chemical compound ClCOC(Cl)=O JYWJULGYGOLCGW-UHFFFAOYSA-N 0.000 abstract description 6
- 238000003756 stirring Methods 0.000 abstract description 5
- 238000009833 condensation Methods 0.000 abstract description 2
- 230000005494 condensation Effects 0.000 abstract description 2
- 238000010521 absorption reaction Methods 0.000 abstract 1
- 238000010438 heat treatment Methods 0.000 abstract 1
- 239000002253 acid Substances 0.000 description 8
- 239000011230 binding agent Substances 0.000 description 8
- 238000000034 method Methods 0.000 description 6
- 238000005086 pumping Methods 0.000 description 4
- 238000000066 reactive distillation Methods 0.000 description 4
- 239000003513 alkali Substances 0.000 description 2
- JHYNXXBAHWPABC-UHFFFAOYSA-N chloromethyl propan-2-yl carbonate Chemical compound CC(C)OC(=O)OCCl JHYNXXBAHWPABC-UHFFFAOYSA-N 0.000 description 2
- 239000012043 crude product Substances 0.000 description 2
- 239000012452 mother liquor Substances 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 229960004556 tenofovir Drugs 0.000 description 2
- VCMJCVGFSROFHV-WZGZYPNHSA-N tenofovir disoproxil fumarate Chemical compound OC(=O)\C=C\C(O)=O.N1=CN=C2N(C[C@@H](C)OCP(=O)(OCOC(=O)OC(C)C)OCOC(=O)OC(C)C)C=NC2=C1N VCMJCVGFSROFHV-WZGZYPNHSA-N 0.000 description 2
- MELVWBNHOCNRGG-UHFFFAOYSA-N (2-methylpropan-2-yl)oxy carbonochloridate Chemical compound CC(C)(C)OOC(Cl)=O MELVWBNHOCNRGG-UHFFFAOYSA-N 0.000 description 1
- 208000030507 AIDS Diseases 0.000 description 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical compound [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 239000000460 chlorine Substances 0.000 description 1
- 229910052801 chlorine Inorganic materials 0.000 description 1
- -1 chloro-carbonic acid chloromethane Chemical compound 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 208000002672 hepatitis B Diseases 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Landscapes
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
Description
Claims (5)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721650021.3U CN207632730U (en) | 2017-12-01 | 2017-12-01 | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201721650021.3U CN207632730U (en) | 2017-12-01 | 2017-12-01 | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device |
Publications (1)
Publication Number | Publication Date |
---|---|
CN207632730U true CN207632730U (en) | 2018-07-20 |
Family
ID=62855438
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN201721650021.3U Active CN207632730U (en) | 2017-12-01 | 2017-12-01 | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN207632730U (en) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107805202A (en) * | 2017-12-01 | 2018-03-16 | 内蒙古圣氏化学股份有限公司 | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device and method |
-
2017
- 2017-12-01 CN CN201721650021.3U patent/CN207632730U/en active Active
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN107805202A (en) * | 2017-12-01 | 2018-03-16 | 内蒙古圣氏化学股份有限公司 | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device and method |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN100439305C (en) | Method of preparing dichloropropanols from glycerine | |
CN103415496A (en) | Low temperature production of 2-chloro-3,3,3-trifluoropropene | |
CN104744423B (en) | A kind of process of continuous prodution vinylene carbonate | |
CN103113257B (en) | Continuous reactive distillation equipment for synthesising methoxylamine hydrochloride and process thereof | |
CN106242961A (en) | Production of chloroacetic acid equipment | |
CN207632730U (en) | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device | |
CN101891583A (en) | Method for co-production of trichloroethylene and tetrachloroethylene by gas phase catalysis method | |
CN101747176B (en) | Method for preparation of trifluoro acetyl chloride with trifluoroethane chlorinated mixture | |
CN110613946A (en) | Backpack reaction rectification equipment for synthesizing diethyl oxalate and process thereof | |
CN101306980B (en) | Method for preparing perchloro cyclopentadiene | |
CN104262177B (en) | A kind of separation purification method of thick diglycolamine | |
CN108658722A (en) | The synthetic method of one kind 1,2,3- trichloropropanes | |
CN110240536A (en) | A kind of production of vinyl chloride and process for refining | |
CN107805202A (en) | A kind of chloromethyl butylperoxyisopropyl carbonate continuous reacting device and method | |
CN210214799U (en) | Chlorine recovery unit in chlorine tail gas | |
CN205635422U (en) | Device of moisture acetone hydrogenation result separation isopropyl alcohol | |
CN102516058B (en) | Device for synthesizing 5-chlorovaleryl chloride | |
CN209778707U (en) | System for but chloride solution continuous hydrolysis formula production ethyl maltol | |
JP3710514B2 (en) | Method for producing 2,3,5,6-tetrafluoroaniline | |
CN102701920A (en) | Method for purifying vinyl isobutyl ether | |
CN202379911U (en) | 5-chlorovaleryl chloride synthesizer | |
CN106478402A (en) | The method that ethanol acid crystal is prepared by methyl glycollate | |
CN115317941B (en) | Method for preparing vinyl tri (beta-methoxyethoxy) silane by catalytic rectification | |
TW201704192A (en) | Method for manufacturing dichlorohydrin and method for manufacturing epichlorohydrin by using glycerol as raw material | |
CN213951046U (en) | Combined preparation device of trifluoroacetyl fluoride |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
GR01 | Patent grant | ||
GR01 | Patent grant | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A continuous reaction device for chloromethyl isopropyl carbonate Effective date of registration: 20210324 Granted publication date: 20180720 Pledgee: Bank of China Limited BAYANHOT branch Pledgor: INNER MONGOLIA SAINTCHEM CHEMICALS Co.,Ltd. Registration number: Y2021150000028 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right | ||
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20220518 Granted publication date: 20180720 Pledgee: Bank of China Limited BAYANHOT branch Pledgor: INNER MONGOLIA SAINTCHEM CHEMICALS CO.,LTD. Registration number: Y2021150000028 |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right | ||
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of utility model: A continuous reaction device for chloromethyl isopropyl carbonate Effective date of registration: 20220526 Granted publication date: 20180720 Pledgee: Bank of China Limited BAYANHOT branch Pledgor: INNER MONGOLIA SAINTCHEM CHEMICALS CO.,LTD. Registration number: Y2022150000044 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Granted publication date: 20180720 Pledgee: Bank of China Limited BAYANHOT branch Pledgor: INNER MONGOLIA SAINTCHEM CHEMICALS CO.,LTD. Registration number: Y2022150000044 |