CN207575845U - A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction - Google Patents

A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction Download PDF

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Publication number
CN207575845U
CN207575845U CN201721663462.7U CN201721663462U CN207575845U CN 207575845 U CN207575845 U CN 207575845U CN 201721663462 U CN201721663462 U CN 201721663462U CN 207575845 U CN207575845 U CN 207575845U
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drum
agitator
type
stirring
ultrasonic wave
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张万喜
李彦志
张国明
赵永涛
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Xi Wan environmental protection materials Co., Ltd
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Qicaibeike New Material Technology Co Ltd
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Abstract

The utility model discloses a kind of stirrings of drum-type counterflow centrifugal and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction, belong to ingredient separation and extraction technology field, including agitator, drum-type extractor, support and lifting gear, agitating device, transmission device, ultrasonic vibrator, heating and temperature regulating device.The agitating device includes stirring motor, mixing control case, agitating shaft, paddle and whirlpool blade, and the transmission device includes driving gear, driven gear, shaft and bearing.Stirring motor drives paddle and whirlpool blade to stir solvent counterclockwise by agitating shaft, at the same time, fixed driving gear drives driven gear on agitating shaft, drum-type extractor is driven to carry out rotation clockwise, then open external ultrasonic vibrator and heating unit simultaneously by shaft and sealing cover.The synergistic effect of the stirring of drum-type counterflow centrifugal, ultrasonic wave and temperature accelerates the release of active ingredient and dissolving diffusion, greatly improves extraction rate and yield.

Description

A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant of ultrasonic wave synergistic reaction Extraction element
Technical field
The utility model belongs to ingredient separation and extraction technology field, and in particular to a kind of drum-type counterflow centrifugal stirring is with surpassing The effective ingredients in plant extraction element of sound wave synergic effect.
Background technology
Containing in natural plants has many beneficial functional components, if it is possible to than more efficient, completely extract, it will It is widely applied in many fields, such as daily-use chemical industry, pharmacy, food, health products and the multiple industries of biochemical industry.Mesh Before, the main method of effective component extracting has infusion process, decocting method and reflux extraction etc. from plant.These methods are all adopted Plant is handled to dissolve out useful component therein under room temperature or heating condition with appropriate solvent, the advantage is that Journey is simple and convenient to operate, and is suitable for almost the constituents extraction of all plants, but due to being static extraction, therefore recovery rate is poor, time-consuming It is long.In view of the above-mentioned problems, in recent years, people start to be gradually introduced dynamic agitation in traditional static extracting mode to improve Rate and yield are taken, but the mode also used mostly at present is all simply to carry out mechanical agitation to extraction solution to improve dissolution And diffusion rate, since simple and mechanical whipping process will not generate centrifugal force, it cannot more effectively make the ingredient in plant Abundant solution modeling.Therefore, a kind of extraction element efficiently, stable is designed and developed out to improve extraction efficiency and efficiency, is mesh Preceding effective ingredients in plant extraction field key technical problem urgently to be resolved hurrily.
Utility model content
In order to solve the deficiencies in the prior art, the purpose of this utility model is to provide a kind of drum-type adverse current from The heart stirs the effective ingredients in plant extraction element with ultrasonic wave synergistic reaction.
To achieve these goals, the utility model is achieved through the following technical solutions:
A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction, including stirring Bucket 10, drum-type extractor 12, support and lifting gear, agitating device, heating and temperature regulating device, transmission device and ultrasonic vibration Device 13;
The ultrasonic vibrator 13 is set on the outer wall of agitator 10;10 top of agitator is equipped with mixing bucket lid 9;
The support and lifting gear include support base 18, support post 19, support beam 21, motor 15 and rise Drop machine 1, the support base 18 are located on level ground, and the support post 19 is located at the upper surface of the support base 18 On, and vertical with the support base 18, the support beam 21 is located at the upper end of the support post 19, and with the support Pedestal 18 is parallel, and the support base 18, support post 19, support beam 21 are integrated cast structure, and the motor 15 is located at On the support post 19, and pass through screw thread and be fixedly connected with support beam 21, the elevator 1 is located at the support beam 21 On, and pass through screw thread and be fixedly connected with support post 19;
The agitating device includes stirring motor 3, mixing control case 2, agitating shaft 4, paddle 14 and whirlpool blade 16, described Stirring motor 3 is to control rotating speed by the mixing control case 2, and the stirring motor 3 and mixing control case 2 are both secured to the branch It supports on crossbeam 21,3 lower section of stirring motor is connected with agitating shaft 4, and the epimere of the agitating shaft 4 is provided with coaxial main transmission Gear 5, the hypomere of the agitating shaft 4 pass through mixing bucket lid 9, and the bottom end of the agitating shaft 4 is provided with whirlpool blade 16, whirlpool blade 16 Several coaxial paddles 14 are provided on agitating shaft 4 between top and mixing bucket lid 9;
The transmission device is by a shaft 20 of driven gear 6, four of driving gear 5, four and four 7 structures of bearing Into the driving gear 5 is coaxially fixed on agitating shaft 4, and the size of four driven gears 6 is less than driving gear 5 Size, and being engaged on same horizontal plane with driving gear 5 simultaneously, the upper ends of four shafts 20 respectively with it is described The lower end of four driven gears 6 is fixedly connected, and is each passed through the mixing bucket lid 9 and is deep into agitator 10, the shaft 20 lower end and drum-type extraction cover 11 center be connected as a single entity by welding, drum-type extraction cover 11 with Drum-type extractor 12 threadedly connects;
It is described heating and temperature regulating device be the digital display thermostatical oil bath 17 with temperature sensor 8, the digital display thermostatical oil Bath 17 is positioned in the support base 18, and the agitator 10 is positioned in the digital display thermostatical oil bath 17, the temperature Degree sensor 8 is positioned over the agitator 10 and contains in solution.
Further, the agitator 10 is stainless steel, and with hollow drum-shaped structure, the mixing bucket lid 9 be the circular cover of stainless steel, and the diameter of the mixing bucket lid 9 is more than 10 diameter of agitator, and the mixing bucket lid 9 is at it Center location setting along the circumferential direction symmetrically opens up that there are four circular through-holes there are one circular through hole.
Further, the hypomere of the agitating shaft 4 passes through the circular through hole of the center location of mixing bucket lid 9 to be deep into institute It states in agitator 10.
Further, four circles that the shaft 20 passes through the mixing bucket lid 9 along the circumferential direction symmetrically to open up are led to Hole is deep into agitator 10.
Further, the hollow cylinder that the tank body of the drum-type extractor 12 is opened for the upper end of stainless steel, institute The barrel for stating hollow cylinder is hollow out filter structure, and the strainer is the stainless steel filter screen of 200-500 mesh fineness, described Drum-type extractor 12 extracts cover 11 equipped with the drum-type of stainless steel.
Further, which further includes automatic injecting device, and the automatic injecting device includes suction pump and water pipe, institute It states on the level ground that suction pump is located near the support base, the water pipe includes water inlet pipe and outlet pipe, the water inlet Pipe one end is extend into cistern, and the other end is connect with the water pump, and described outlet pipe one end is connect with the water pump, the other end Entered in agitator by the water filling port in mixing bucket lid.
Further, which further includes pumping equipment, and the pumping equipment is arranged on the bottom of agitator, the row Liquid device includes drain pipe and water discharging valve, and the drain pipe is located at the bottom of the agitator, one end by welding manner and The leakage fluid dram of stirring bottom of the barrel is connected, and draining valve is equipped on the drain pipe.
Further, it is also opened in the mixing bucket lid 9 there are one circular exhaust outlet, and the exhaust outlet is with condensing Pipe is connected.
Compared with prior art, it is as follows the advantages of the utility model:
Whirlpool blade and paddle on agitating shaft is driven by stirring motor, the extraction solution in agitator is made to generate one Anticlockwise flowing, while carried out with four driven gears for being arranged symmetrically in agitating shaft with the driving gear on agitating shaft Gear engages, and the shaft for passing through driven gear lower end drives extractor to carry out rotation, due to gear-driven inversion principle, carries Take tank rotation direction and agitator in the direction flowed of solution on the contrary, therefore can generate it is a kind of similar to roller washing machine from Heart adverse current impact effect, at the same time, the ultrasonic wave for being arranged in the ultrasonic vibrator transmitting on agitator outer wall can be deeper into The organization internal for entering plant, destroy cell wall, accelerate the release of active ingredient.It can be seen that drum-type counterflow centrifugal Both stirring and ultrasonic wave synergistic effect accelerate the release of effective ingredients in plant, improve dissolving diffusion velocity, greatly improve Plant component extraction efficiency and yield.
Description of the drawings
Fig. 1 is a kind of drum-type counterflow centrifugal stirring of the utility model and the effective ingredients in plant of ultrasonic wave synergistic reaction The structure diagram of extraction element;
In figure:Elevator 1, mixing control case 2, stirring motor 3, agitating shaft 4, driving gear 5, driven gear 6, bearing 7, Temperature sensor 8, mixing bucket lid 9, agitator 10, drum-type extraction cover 11, drum-type extractor 12, ultrasonic vibrator 13, Paddle 14, motor 15, whirlpool blade 16, digital display thermostatical oil bath 17, support base 18, support post 19, shaft 20, support are horizontal Beam 21.
Specific embodiment
The present invention is described further below in conjunction with the accompanying drawings.
Embodiment 1
A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction, including stirring Bucket 10, drum-type extractor 12, support and lifting gear, agitating device, heating and temperature regulating device, transmission device and ultrasonic vibration Device 13;
The ultrasonic vibrator 13 is set on the outer wall of agitator 10;10 top of agitator is equipped with mixing bucket lid 9;
The support and lifting gear include support base 18, support post 19, support beam 21, motor 15 and rise Drop machine 1, the support base are located on level ground, and the support post is located on the upper surface of the support base, and with The support base is vertical, and the support beam is located at the support post upper end, and, the branch parallel with the support base Support pedestal, support post, support beam are integrated cast structure, and the motor is located on the support post, and passes through screw thread It is fixedly connected with support beam, the elevator is located in the support beam, and passes through screw thread and be fixedly connected with support post;
The agitating device includes stirring motor 3, mixing control case 2, agitating shaft 4, paddle 14 and whirlpool blade 16, described Stirring motor 3 is to control rotating speed by the mixing control case 2, and the stirring motor 3 and mixing control case 2 are both secured to the branch It supports on crossbeam 21,3 lower section of stirring motor is connected with agitating shaft 4, and the epimere of the agitating shaft 4 is provided with coaxial main transmission Gear 5, the hypomere of the agitating shaft 4 pass through mixing bucket lid 9, and the bottom end of the agitating shaft 4 is provided with whirlpool blade 16, whirlpool blade 16 Several coaxial paddles 14 are provided on agitating shaft 4 between top and mixing bucket lid 9;
The transmission device is by a shaft 20 of driven gear 6, four of driving gear 5, four and four 7 structures of bearing Into the driving gear 5 is coaxially fixed on agitating shaft 4, and the size of four driven gears 6 is less than driving gear 5 Size, and being engaged on same horizontal plane with driving gear 5 simultaneously, the upper ends of four shafts 20 respectively with it is described The lower end of four driven gears 6 is fixedly connected, and is each passed through the mixing bucket lid 9 and is deep into agitator 10, the shaft 20 lower end and drum-type extraction cover 11 center be connected as a single entity by welding, drum-type extraction cover 11 with Drum-type extractor 12 threadedly connects;
It is described heating and temperature regulating device be the digital display thermostatical oil bath 17 with temperature sensor 8, the digital display thermostatical oil Bath 17 is positioned in the support base 18, and the agitator 10 is positioned in the digital display thermostatical oil bath 17, the temperature Degree sensor 8 is positioned over the agitator 10 and contains in solution.
Further, the agitator 10 is stainless steel, and with hollow drum-shaped structure, the mixing bucket lid 9 be the circular cover of stainless steel, and the diameter of the mixing bucket lid 9 is more than 10 diameter of agitator, and the mixing bucket lid 9 is at it Center location setting along the circumferential direction symmetrically opens up that there are four circular through-holes there are one circular through hole;
Further, the hypomere of the agitating shaft 4 passes through the circular through hole of the center location of mixing bucket lid 9 to be deep into institute It states in agitator 10.
Further, four circles that the shaft 20 passes through the mixing bucket lid 9 along the circumferential direction symmetrically to open up are led to Hole is deep into agitator 10.
Further, the hollow cylinder that the tank body of the drum-type extractor 12 is opened for the upper end of stainless steel, institute The barrel of hollow cylinder is stated as hollow out filter structure, the strainer is 200-500 mesh fineness stainless steel filter screens, the rolling Cartridge type extractor 12 extracts cover 11 equipped with the drum-type of stainless steel.
Further, which further includes automatic injecting device, and the automatic injecting device includes suction pump and water pipe, institute It states on the level ground that suction pump is located near the support base, the water pipe includes water inlet pipe and outlet pipe, the water inlet Pipe one end is extend into cistern, and the other end is connect with the water pump, and described outlet pipe one end is connect with the water pump, the other end Entered in agitator by the water filling port in mixing bucket lid.
Further, which further includes pumping equipment, and the pumping equipment is arranged on the bottom of agitator, the row Liquid device includes drain pipe and draining valve, and the drain pipe is located at the bottom of the agitator, one end by welding manner and The leakage fluid dram of stirring bottom of the barrel is connected, and draining valve is equipped on the drain pipe.
Further, it is also opened in the mixing bucket lid 9 there are one circular exhaust outlet, and the exhaust outlet is with condensing Pipe is connected.
A kind of drum-type counterflow centrifugal stirring of the utility model and the effective ingredients in plant of ultrasonic wave synergistic reaction extract The operation principle of device is:
Agitator is placed in thermostatical oil bath first, Extraction solvent is injected into agitator, and (water is other organic molten Agent), the temperature sensor probe that thermostatical oil bath carries is positioned in the solvent in agitator, opens thermostatical oil bath switch And set extraction reaction temperature.Then the plant of ingredient to be extracted is respectively placed in four drum-type extractors, and twisted Close capping, mixing bucket lid is covered in agitator upper edge, and agitating shaft is adjusted up and down to suitable position by motor and elevator, It is opened and stirred by mixing control case, the whirlpool blade on agitating shaft and paddle can drive solvent to carry out counterclockwise flow at this time, Meanwhile four cartridge type extractors can be driven by shaft and be rotated clockwise, and at the same time, be opened on setting and agitator outer wall Ultrasonic vibrator release ultrasonic wave.After the completion of reaction to be extracted, stop stirring and heating, by elevator by cartridge type extractor It removes more than liquid level, unscrews sealing cover, remove cartridge type extractor and pour out plant residue therein, while by carrying in agitator Liquid is taken to export, thoroughly cleaning is finally carried out to agitator and cartridge type extractor in case making next time with clear water or other solvents With.

Claims (8)

1. a kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction, feature exist In including agitator (10), drum-type extractor (12), support and lifting gear, agitating device, heating and temperature regulating device, biography Dynamic device and ultrasonic vibrator (13);
The ultrasonic vibrator (13) is set on the outer wall of agitator (10);Equipped with agitator above the agitator (10) It covers (9);
The support and lifting gear include support base (18), support post (19), support beam (21), motor (15) with And elevator (1), the support base (18) is on level ground, and the support post (19) is positioned at the support base (18) on upper surface, and it is vertical with the support base (18), and the support beam (21) is positioned at the support post (19) Upper end, and parallel with the support base (18), the support base (18), support post (19), support beam (21) are Integrally casting structure, the motor (15) is on the support post (19), and it is fixed with support beam (21) to pass through screw thread Connection, the elevator (1) pass through screw thread and are fixedly connected with support post (19) in the support beam (21);
The agitating device includes stirring motor (3), mixing control case (2), agitating shaft (4), paddle (14) and whirlpool blade (16), the stirring motor (3) is to control rotating speed, the stirring motor (3) and mixing control case by the mixing control case (2) (2) it is both secured in the support beam (21), agitating shaft (4), the agitating shaft is connected with below the stirring motor (3) (4) epimere is provided with coaxial driving gear (5), and the hypomere of the agitating shaft (4) passes through mixing bucket lid (9), the stirring The bottom end of axis (4) is provided with whirlpool blade (16), is set on the agitating shaft (4) between whirlpool blade (16) top and mixing bucket lid (9) There are several coaxial paddles (14);
The transmission device is by a driving gear (5), four driven gears (6), four shafts (20) and four bearings (7) It forms, the driving gear (5) is coaxially fixed on agitating shaft (4), and the size of four driven gears (6) is less than actively The size of gear (5), and be engaged on same horizontal plane with driving gear (5) simultaneously, four shafts (20) Lower end of the upper end respectively with four driven gears (6) is fixedly connected, and is each passed through the mixing bucket lid (9) and is deep into and stir It mixes in bucket (10), the lower end and the center of drum-type extraction cover (11) of the shaft (20) are linked as by welding One, drum-type extraction cover (11) are threadedly connect with drum-type extractor (12);
It is described heating and temperature regulating device be the digital display thermostatical oil bath (17) with temperature sensor (8), the digital display thermostatical oil Bath (17) is positioned in the support base (18), and the agitator (10) is positioned over the digital display thermostatical oil bath (17) In, the temperature sensor (8) is positioned over the agitator (10) and contains in solution.
2. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that the agitator (10) is stainless steel, and with hollow drum-shaped structure, the stirring Bung (9) is the circular cover of stainless steel, and the diameter of the mixing bucket lid (9) is more than agitator (10) diameter, described to stir Bung (9) is mixed in the setting of its center location there are one circular through hole, while along the circumferential direction symmetrically opens up and leads to there are four circular Hole.
3. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that the hypomere of the agitating shaft (4) passes through the circular through hole of the center location of mixing bucket lid (9) deep Enter into the agitator (10).
4. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that four circles that the shaft (20) is along the circumferential direction symmetrically opened up across the mixing bucket lid (9) Shape through-hole is deep into agitator (10).
5. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that the hollow cylinder that the tank body of the drum-type extractor (12) is opened for the upper end of stainless steel, The barrel of the hollow cylinder be hollow out filter structure, the strainer be 200-500 mesh fineness stainless steel filter screen, institute State drum-type extraction cover (11) of the drum-type extractor (12) equipped with stainless steel.
6. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Taking device, which is characterized in that the device further includes automatic injecting device, and the automatic injecting device includes suction pump and water pipe, The suction pump is located on the level ground near the support base, the water pipe include water inlet pipe and outlet pipe, it is described into Water pipe one end is extend into cistern, and the other end is connect with the water pump, and described outlet pipe one end is connect with the water pump, another End is entered by the water filling port in mixing bucket lid in agitator.
7. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that the device further includes pumping equipment, and the pumping equipment is arranged on the bottom of agitator, described Pumping equipment includes drain pipe and water discharging valve, and the drain pipe is located at the bottom of the agitator, and one end passes through welding manner It is connected with the leakage fluid dram for stirring bottom of the barrel, draining valve is installed on the drain pipe.
8. a kind of drum-type counterflow centrifugal stirring as described in claim 1 and the effective ingredients in plant of ultrasonic wave synergistic reaction carry Take device, which is characterized in that also opened in the mixing bucket lid (9) there are one circular exhaust outlet, and the exhaust outlet with Condenser pipe is connected.
CN201721663462.7U 2017-12-04 2017-12-04 A kind of drum-type counterflow centrifugal stirring and the effective ingredients in plant extraction element of ultrasonic wave synergistic reaction Active CN207575845U (en)

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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109393001A (en) * 2018-11-20 2019-03-01 武红亮 A kind of thorough ultrasonic wave cray cleaning machine of cleaning
CN109692498A (en) * 2019-01-30 2019-04-30 沈阳人和机电工程设备有限公司 A method of it is extracted for effective ingredients in plant
CN110665251A (en) * 2019-10-12 2020-01-10 西藏天虹科技股份有限责任公司 Tibetan medicine extraction device
CN111991841A (en) * 2020-09-07 2020-11-27 湖南省药品检验研究院(湖南药用辅料检验检测中心) Multifunctional ultrasonic extraction device
CN112619200A (en) * 2020-11-04 2021-04-09 福建智罗科技有限公司 Natural products polysaccharide draws concentrated all-in-one
CN114432970A (en) * 2020-10-30 2022-05-06 中国石油化工股份有限公司 System and method for evaluating oil product hydrogenation catalyst
CN118079450A (en) * 2024-04-26 2024-05-28 四川省畜牧科学研究院 Auxiliary extraction device and extraction method for sinapine in rapeseed meal

Cited By (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109393001A (en) * 2018-11-20 2019-03-01 武红亮 A kind of thorough ultrasonic wave cray cleaning machine of cleaning
CN109393001B (en) * 2018-11-20 2021-09-24 陈巍 Wash thorough ultrasonic wave crayfish cleaning machine
CN109692498A (en) * 2019-01-30 2019-04-30 沈阳人和机电工程设备有限公司 A method of it is extracted for effective ingredients in plant
CN110665251A (en) * 2019-10-12 2020-01-10 西藏天虹科技股份有限责任公司 Tibetan medicine extraction device
CN110665251B (en) * 2019-10-12 2022-03-08 西藏天虹科技股份有限责任公司 Tibetan medicine extraction device
CN111991841A (en) * 2020-09-07 2020-11-27 湖南省药品检验研究院(湖南药用辅料检验检测中心) Multifunctional ultrasonic extraction device
CN114432970A (en) * 2020-10-30 2022-05-06 中国石油化工股份有限公司 System and method for evaluating oil product hydrogenation catalyst
CN112619200A (en) * 2020-11-04 2021-04-09 福建智罗科技有限公司 Natural products polysaccharide draws concentrated all-in-one
CN118079450A (en) * 2024-04-26 2024-05-28 四川省畜牧科学研究院 Auxiliary extraction device and extraction method for sinapine in rapeseed meal

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Effective date of registration: 20200804

Address after: No.4, Longxing Road, Changchun Nong'an Economic Development Zone, Helong Town, Nong'an County, Changchun City, Jilin Province

Patentee after: Xi Wan environmental protection materials Co., Ltd

Address before: Longxing Changchun Nong'an Road Economic Development Zone in Jilin province Changchun joint jiulongzhen 130200 No. 3

Patentee before: QICAIBEIKE NEW MATERIAL TECHNOLOGY Co.,Ltd.

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