CN207525311U - One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank - Google Patents

One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank Download PDF

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Publication number
CN207525311U
CN207525311U CN201721515551.7U CN201721515551U CN207525311U CN 207525311 U CN207525311 U CN 207525311U CN 201721515551 U CN201721515551 U CN 201721515551U CN 207525311 U CN207525311 U CN 207525311U
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CN
China
Prior art keywords
boat
boat body
segmental arc
magnesium
tank
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Expired - Fee Related
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CN201721515551.7U
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Chinese (zh)
Inventor
禹健
贺成杰
张亚彬
郭天星
高超
刘靖亮
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Shanxi University
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Shanxi University
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Priority to CN201721515551.7U priority Critical patent/CN207525311U/en
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Publication of CN207525311U publication Critical patent/CN207525311U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model is related to vacuum metallurgy equipment technical fields, specially one kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank, including boat body, at least one baffle and center flat tube, the radial section of the boat body is symmetrical about central axis, it is followed successively by horizontal segmental arc from top to bottom, tank cuts segmental arc, vertical segmental arc and upper wall segmental arc, feed inlet is equipped in the upper wall of boat body and through boat body left and right ends, and boat body is closed at both ends, at least one baffle is vertical to be located in the inner cavity of boat body, center flat tube level is located in the inner cavity of boat body, and through each baffle.The utility model is designed reasonably, heat transfer efficiency are high, indeformable under high temperature and vacuum condition, long lifespan, at low cost, and condition is created for operations such as refining magnesium mechanized handling material, scarfing cinders.Available for magnesium, lithium, the production of the high-vapor-pressure metals such as strontium, calcium thermal reduction.

Description

One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank
Technical field
The utility model is related to vacuum metallurgy equipment technical field, specially one kind is placed in horizontal positioned magnesium vacuum reduction tank Interior material boat prepares magnesium, lithium, the equipment of the high-vapor-pressure metals such as strontium, calcium available for thermal reduction.
Background technology
Magnesium, lithium, the high-vapor-pressure metals such as strontium, calcium can under vacuum be prepared using thermal reduction.Industry refining magnesium Main method has electrolysis and thermal reduction.Smelting magnesium by thermal reduction process technology based on ferrosilicon process (i.e. Pidgeon process) is more perfect, It is widely used for domestic most lifes.At present, it in China overwhelming majority magnesium smelting reduction pot without heat source, is come under vacuum state External heat is successively transmitted from outside to inside with forms of radiation, and reductive jar central axis temperature is minimum, and pelletizing material is heated most slowly, This temperature uneven phenomenon seriously restricts the raising of rate of reduction.Therefore, new technique and technology are studied, strengthens in tank and passes Heat improves energy utilization rate, shortens reduction cycle, has higher research and application value.
Magnesium-smelting silicothermic process uses horizontal tank reduction furnace mostly:This reduction furnace is the structure of cylinder tank, due to its long-term work Under 1200 DEG C of temperature, an extraneous atmospheric pressure, tank body is very long in addition, is just inevitably acted on by external force.This Kind of high temperature, high pressure, external force integrated condition, reductive jar can deform in a short period of time so that the reductive jar lost of life.It is this In addition to state increases energy consumption when because tank skin slagging, due also to its tank skin deformation and leading to not carries out mechanical Cosmetic material, discharging, clearly The implementation and operation of a series of mechanization measures such as slag drastically influence the development process of refining magnesium industry.
Heat-transfer device is installed additional in reductive jar for the slow problem of heat conduction of material in reductive jar, Su Ming etc., so as to enhance Heat transfer in tank makes the recovery time shorten to 4~5h, but heat-transfer device is chronically in hot environment, easily causes deformation, Service life is shorter.Feng Jun little is using material in reductive jar as research object, influence of the analysis material distribution mode to heating time, and right The diabatic process of material carries out numerical simulation, proposes a kind of novel refining magnesium material block.The material block can improve the heat transfer type of material, contracting Short heating time improves production efficiency.The problems such as magnesium vacuum reduction tank overcomes yielding previous reductive jar, short life.Due to Previous process for smelting magnesium so that reductive jar is yielding and leads to not carry out a series of mechanizations such as mechanical Cosmetic material, discharging, scarfing cinder The implementation and operation of measure.Tinkling of pieces of jade etc. is appointed to be proposed for the present situation for manually taking on material in current metal magnesiothermic reduction process using nothing Machinery dress discharge method of the axis conveyor screw as Guan Nei executing agencies.Dress discharging time can be shorten to 15min by 2h, contracted significantly The time of short thermal reduction process.
Problem of the existing technology is:Without heat source in China's overwhelming majority magnesium smelting reduction pot, come under vacuum state External heat is successively transmitted from outside to inside with forms of radiation, and reductive jar central axis spot temperature is minimum, and pelletizing material is heated Most slow, this temperature uneven phenomenon seriously restricts the raising of rate of reduction;Previous process for smelting magnesium cause reductive jar yielding and Lead to not carry out the implementation and operation of a series of mechanization measures such as mechanical Cosmetic material, discharging, scarfing cinder, extend reduction process Time.
Utility model content
For existing magnesium smelting reduction pot, the utility model provides one kind and is placed in horizontal positioned magnesium vacuum Material boat in reductive jar.
In order to solve the above technical problems, the technical solution adopted in the utility model is:
One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank, including boat body, at least one baffle and center flat tube, institute The radial section for stating boat body is symmetrical about central axis, be followed successively by horizontal segmental arc from top to bottom, tank cuts segmental arc, vertical segmental arc and on Wall segmental arc, the arc radius of the horizontal segmental arc is more than there are spaces inside reductive jar inside radius, with reductive jar bottom wall;With arc of horizon What section was connected is to expect that the tank of boat cuts segmental arc, and arc radius is identical with reduction top tank structure radius, is in contact with reductive jar, by changing Become there are the size in space inside horizontal segmental arc and reductive jar bottom wall, adjustable material-saving boat tank cuts the big of segmental arc and reductive jar contact surface It is small;Cut that segmental arc is connected with tank is the vertical segmental arc of expecting boat, after expecting that boat is put into reductive jar, about reductive jar central axis Symmetrically, after material boat lifts, there are allowances for outside and the reduction top tank structure of the material vertical segmental arc of boat;It is connected with vertical segmental arc It is the upper wall segmental arc for expecting boat, keeps respectively equidistant with reductive jar, design principle is:Make material boat volume big as far as possible, but work as After material boat lifts, upper wall segmental arc is just tangent with reductive jar;In order to enable the loading, unloading material of reductive jar is more convenient, in boat body Upper wall be equipped with feed inlet, and boat body is closed at both ends, and the loading, unloading material of reductive jar feeds by that will expect that boat takes out and is directly attached to expect In boat, material boat is directly toppled in discharging, and material boat total is approximately cylindrical shape, uniform wall thickness;At least one baffle is vertical to be located at In the inner cavity of boat body, center flat tube level is located in the inner cavity of boat body, and through each baffle.
The upper end that the tank cuts segmental arc is less than reductive jar horizontal center line.
The feed inlet for being located at boat body upper wall is symmetrical about the central axis of boat body.
The center flat tube is located in the center of gravity of fully loaded material boat after expecting.
The described and matching used crowbar for having loading and unloading of center flat tube, crowbar are located in the flat tube of center, are set in crowbar There is water cooling plant.
When reduction reaction occurs, the material boat is in vacuum environment, and stress very little is not susceptible to deformation.And due to true Empty protection is not oxidizable.
During work, crowbar is tilted upwards stretch into the flat tube of center first, it is gradually that crowbar is gentle with going deep into for crowbar It places, after crowbar places, reduction furnace charge is inserted from feed inlet in material boat, after honest material to be installed, material boat is lifted into certain height It is sent into reductive jar after degree, then material boat is slowly moved down, it is ensured that material boat both sides are contacted with reductive jar, finally screw out crowbar.Material Boat leans on the portion of heat transfer contacted with reductive jar.After the completion of reduction reaction, it is flat to be fixed on center by vacuum breaker as stated above for crowbar In pipe, material boat is up lifted certain altitude, gradually will material boat removed out of reductive jar, carry out slag dumping, skim after, entrance is next A work period.
Compared with prior art, the utility model advantage specific as follows:
1st, expect boat tubular article made of certain thickness heat-resisting steel sheet and plate, structural strength is big, loads and unloads not rapid wear in charge process It is bad;
When reduction reaction the 2nd, occurs, material boat is in vacuum environment, and stress very little is not susceptible to deformation.And due to vacuum Protection it is not oxidizable, so heating temperature can be higher than Pidgeon process in stove, greatly improve reduction reaction speed and furnace charge and utilize Rate;
3rd, the horizontal segmental arc of material boat to expect that boat facilitates placement in loading and unloading;
4th, material boat both sides is allowed to be contacted with reductive jar so that heat transfer disperses and has sufficiently large heat transfer area and shorter biography Hot distance, shortens reduction cycle;
5th, material boat top is with restoring top tank structure there are space, convenient for material boat is lifted certain altitude in loading and unloading;
6th, the arc radius of the horizontal segmental arc of inner lining material boat is more than reductive jar inside radius, and tank cuts the upper end of segmental arc less than reductive jar Horizontal center line.Ensure in loading and unloading, after material boat is lifted, be successfully sent into or remove out of reductive jar;
7th, material boat upper wall is equipped with about the symmetrical feed inlet and outlet of central axis so that expects that the loading, unloading material mode of boat is very square Just, fast;
8th, material boat center is provided through the center flat tube of baffle and matches with crowbar so that loading and unloading process compatible;
9th, water cooling plant is equipped in crowbar, crowbar hot operation is solved the problems, such as substantially, extends the service life of crowbar.
The utility model is designed reasonably, heat transfer efficiency is high, greatly shortens the time of thermal reduction process;It is mainly used for magnesium, lithium, The high-vapor-pressure metals such as strontium, calcium thermal reduction produces, and has practical promotion and application value.
Description of the drawings
Fig. 1 is the unclosed structure diagram in the utility model front end;
Fig. 2 is the radial cutaway view that the utility model is packed into after reductive jar;
Fig. 3 is the utility model center flat tube and crowbar and the installation diagram of water cooling plant.
Specific embodiment
Specific embodiment of the utility model is described in detail below in conjunction with the accompanying drawings.
As shown in Figs. 1-3, one kind in the present embodiment is placed in material boat in horizontal positioned magnesium vacuum reduction tank, including boat body 2, 3 baffles 7 and center flat tube 3, entire to expect that boat is made of heat-resistant steel, structural strength is big, loads and unloads and is hardly damaged in charge process, resistance to Hot steel is the steel alloy for having at high temperature higher intensity and good chemical stability, including oxidation resistant steel (or high temperature Non-scaling steel) and two class of refractory steel;The radial section of the boat body 2 is symmetrical about central axis, is followed successively by level from top to bottom Segmental arc, tank cut segmental arc, vertical segmental arc and upper wall segmental arc, and the arc radius of the horizontal segmental arc is more than reductive jar inside radius, with reduction There are spaces for tank bottom pars intramuralis;What is be connected with horizontal segmental arc is to expect that the tank of boat cuts segmental arc, arc radius and reduction top tank structure half Diameter is identical, and tank cuts the upper end of segmental arc less than reductive jar horizontal center line, is in contact with reductive jar, by changing horizontal segmental arc with going back For former tank bottom pars intramuralis there are the size in space, adjustable material-saving boat tank cuts the size of segmental arc and reductive jar contact surface;Segmental arc is cut with tank What is be connected is the vertical segmental arc for expecting boat, symmetrical about reductive jar central axis after expecting that boat is put into reductive jar, when material boat lift After rising, there are allowances for outside and the reduction top tank structure of the material vertical segmental arc of boat;What is be connected with vertical segmental arc is the upper wall for expecting boat Segmental arc keeps respectively equidistant with reductive jar, and design principle is:Make material boat volume big as far as possible, but after expecting that boat lifts, Upper wall segmental arc is just tangent with reductive jar;In order to enable the loading, unloading material of reductive jar is more convenient, the upper wall of boat body 2 be equipped with into Material mouth 6, and it is symmetrical about 2 central axis of boat body, boat body 2 is closed at both ends, and the loading, unloading material of reductive jar will be by that will expect that boat takes out, dress Material is directly attached in material boat, and material boat is directly toppled in discharging, and material boat total is approximately cylindrical shape, uniform wall thickness;3 baffles 7 Vertical is located in the inner cavity of boat body 2, and flat tube 3 level in center is located in the inner cavity of boat body 2, and through each baffle 7, and center is flat Pipe 3 is located in the center of gravity of fully loaded material boat after expecting, the matching used crowbar 4 for having loading and unloading of center flat tube 3, crowbar 4 is located at center In flat tube 3, water cooling plant 5 is equipped in crowbar 4.
During work, crowbar 4 is tilted upwards and is stretched into center flat tube 3, it is gradually that crowbar 4 is gentle with going deep into for crowbar 4 It places, after crowbar 4 places, reduction furnace charge is packed into from feed inlet 6 in boat body 2, after honest material to be installed, boat body 2 is lifted one It is sent into reductive jar 1, then boat body 2 is slowly moved down after determining height, it is ensured that 2 both sides of boat body are contacted with reductive jar 1, finally by crowbar 4 screw out.Boat body 2 leans on the portion of heat transfer contacted with reductive jar 1.After the completion of reduction reaction, vacuum breaker, as stated above by crowbar 4 It is fixed in center flat tube 3, boat body 2 is up lifted certain altitude, gradually boat body 2 out of reductive jar 1 is removed, is unloaded Slag, after skimming, into next work period.
When reduction reaction occurs, boat body 2 is in vacuum environment, and stress very little is not susceptible to deformation.And due to vacuum Protection is not oxidizable, so heating temperature can be higher than Pidgeon process in stove, greatly improves reduction reaction speed and furnace charge utilization rate. Above-mentioned vacuum reduction stove is mainly used for the production of the high-vapor-pressure metals such as magnesium, lithium, strontium, calcium thermal reduction.
It should be noted last that above example is merely intended for describing the technical solutions of the present application, but not for limiting the present application, to the greatest extent Pipe is described in detail with reference to the utility model embodiment, it will be understood by those of ordinary skill in the art that, it is new to this practicality The technical solution of type is modified or replaced equivalently, without departure from the spirit and scope of the technical solution of the utility model, In the claims that the utility model should all be covered.

Claims (4)

1. one kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank, it is characterised in that:Including boat body (2), at least one baffle (7) and center flat tube (3), the radial section of the boat body (2) is symmetrical about central axis, is followed successively by arc of horizon from top to bottom Section, tank cut segmental arc, vertical segmental arc and upper wall segmental arc, and feed inlet (6), and (2) two end seal of boat body are equipped in the upper wall of boat body (2) It closes, at least one baffle (7) is vertical to be located in the inner cavity of boat body (2), and center flat tube (3) level is located at the inner cavity of boat body (2) In, and through each baffle (7).
2. one kind according to claim 1 is placed in material boat in horizontal positioned magnesium vacuum reduction tank, it is characterised in that:The tank The upper end for cutting segmental arc is less than reductive jar horizontal center line.
3. one kind according to claim 2 is placed in material boat in horizontal positioned magnesium vacuum reduction tank, it is characterised in that:It is described to set It is symmetrical about the central axis of boat body (2) in the feed inlet (6) of boat body (2) upper wall.
4. being placed in horizontal positioned magnesium vacuum reduction tank according to claim 1-3 any one of them one kind and expecting boat, feature exists In:The center flat tube (3) is located in the center of gravity of fully loaded material boat after expecting.
CN201721515551.7U 2017-11-14 2017-11-14 One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank Expired - Fee Related CN207525311U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721515551.7U CN207525311U (en) 2017-11-14 2017-11-14 One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721515551.7U CN207525311U (en) 2017-11-14 2017-11-14 One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank

Publications (1)

Publication Number Publication Date
CN207525311U true CN207525311U (en) 2018-06-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107663594A (en) * 2017-11-14 2018-02-06 山西大学 One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107663594A (en) * 2017-11-14 2018-02-06 山西大学 One kind is placed in material boat in horizontal positioned magnesium vacuum reduction tank
CN107663594B (en) * 2017-11-14 2022-12-30 山西大学 Material boat in horizontal magnesium-containing vacuum reduction tank

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20180622

Termination date: 20211114