CN207472733U - A kind of permeable compression testing device of porous material - Google Patents

A kind of permeable compression testing device of porous material Download PDF

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Publication number
CN207472733U
CN207472733U CN201721708213.5U CN201721708213U CN207472733U CN 207472733 U CN207472733 U CN 207472733U CN 201721708213 U CN201721708213 U CN 201721708213U CN 207472733 U CN207472733 U CN 207472733U
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China
Prior art keywords
hole
porous material
liquid chamber
gas
annular sealing
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Withdrawn - After Issue
Application number
CN201721708213.5U
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Chinese (zh)
Inventor
孙公权
燕召
王二东
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Dalian Institute of Chemical Physics of CAS
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Dalian Institute of Chemical Physics of CAS
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Priority to CN201721708213.5U priority Critical patent/CN207472733U/en
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Withdrawn - After Issue legal-status Critical Current
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Abstract

A kind of permeable compression testing device of porous material, including gas injection apparatus, gas buffer chamber, porous material fixture and pressure gauge;Gas injection apparatus realizes being slowly increased for test pressure with gas buffer chamber, improves the accuracy of test.

Description

A kind of permeable compression testing device of porous material
Technical field:
The utility model is related to a kind of permeable pressure measuring devices.
Background technology:
Porous gas diffusive electrode is widely used in fuel cell, metal-air battery.Porous electrode was at work both Gas (such as oxygen, hydrogen) is allowed to penetrate, prevents solution leakage again.The permeable pressure of porous material is that reflection material is prevented The only important parameter of solution leakage when measuring permeable pressure, needs that porous material side is made to immerse in water or electrolyte, and gradually Increase fluid pressure, the liquid pressure value when drop is oozed out by porous material opposite side is the permeable pressure of porous material.
Utility model content
In order to accurately measure the permeable pressure of porous material, need slowly to increase fluid pressure, the utility model patent proposes A kind of permeable pressure measuring device is pressurized, and pass through gas by peristaltic pump or other devices that can be slowly injected into gas to liquid Body cushion chamber reduces rate of pressure rise.
The utility model solves the above problems by the following technical programs, specific as follows:
A kind of permeable compression testing device of porous material, including gas injection apparatus, gas buffer chamber, porous material fixture and Device for pressure measurement;
Porous material fixture is to include closed liquid chamber and hollow ring tablet, and through-hole is equipped in the upper surface of liquid chamber A, hollow ring tablet is placed in above through-hole A, and through-hole A is in the hollow region of hollow ring tablet;On the outside of through-hole A Annular sealing gaskets is placed in liquid chamber upper surface, and through-hole A is in the hollow region that annular sealing gaskets is surrounded;It is to be measured more Porous materials are placed between hollow ring tablet and annular sealing gaskets, and the lower surface edge of porous material to be measured and annular are close Liquid chamber upper surface on the outside of gasket, annular sealing gaskets and through-hole A is amplexiformed, the upper surface edge of porous material to be measured It is amplexiformed with the hollow ring tablet lower face on the outside of hollow region;
In applying the thrust to liquid chamber upper surface on hollow ring tablet, the lower surface surrounding of porous material to be measured can be made Edge is sealed with the liquid chamber upper surface on the outside of annular sealing gaskets, annular sealing gaskets and through-hole A;
The lower part of gas buffer chamber is connected with liquid chamber lower part by pipeline;Pass through pipeline in the top of gas buffer chamber It is connected with the gas outlet of gas injection apparatus;Device for pressure measurement is equipped in gas buffer chamber top.
Peristaltic pump, diaphragm pump or gear pump may be used in the test device, the gas injection apparatus.
The test device, the gas buffer chamber act as further reducing gas pressure increase rate, carry
High permeable pressure measurement accuracy.
The test device is evenly equipped with the through-hole of 3 or more in hollow ring tablet edge, corresponding in liquid Offer the threaded hole of 3 or more on chamber upper wall face, the screw rod of 3 or more is each passed through after through-hole and corresponding threaded hole spiral shell It closes.
The test device is equipped with transparent windows in the lower face of liquid chamber;The effect of the observation window is to inject After water or electrolyte, whether observation porous electrode surface has bubble.
The test device is equipped with through-hole B in the lower face of liquid chamber, transparent material plate, transparent material is equipped at through-hole B The edge airtight connection of the upper surface of flitch and through-hole B, lower face or internal face forms transparent windows.
The permeable compression testing device of porous material described in this patent, can significantly reduce liquid rate of pressurization, improve porous material Expect the measurement accuracy of permeable pressure.
Description of the drawings
In order to illustrate more clearly of the technical solution of the utility model embodiment, the attached drawing to being used needed for embodiment below Make brief introduction.Obviously, it is only some embodiments of the utility model that middle attached drawing, which is described below, for the common of this field Technical staff without creative efforts, can also be obtained according to these attached drawings other accompanying drawings.
Fig. 1 be the permeable compression testing device schematic diagram of porous material, including gas injection apparatus (1), gas buffer chamber (2), Device for pressure measurement (3), porous material fixture (4), wherein porous material fixture (4) include hollow ring tablet (5), bolt (6), porous material (7), annular sealing gaskets (8), liquid chamber (9), observation window (10).
Specific embodiment
It is clearly and completely described with reference to the technical scheme in the embodiment of the utility model, it is clear that described Embodiment is only the part of the embodiment of the utility model, instead of all the embodiments.Implementation based on the utility model Example, those of ordinary skill in the art's all other embodiments obtained under the premise of no creative work belong to this The protection domain of utility model.
Embodiment
As shown in Figure 1, after porous material is cut into a certain size, material is fixed using porous material fixture, it is porous There is annular sealing gaskets to prevent fluid seepage between material and fixture.Water is filled in fixture fluid chamber, and it is true to pass through observation window Recognize porous material surface bubble-free.Gas buffer chamber surplus air cavity volume is about 200mL, connects gas piping, uses wriggling Pump is as gas injection apparatus, and wriggling revolution speed 20rpm, Pressure rise rates are about 0.1kPa/min at this time.Pass through drop Porous material is observed by observation ward, when first Liquid Penetrant comes out, reads pressure reading immediately, as the porous material is saturating Hydraulic pressure.
Comparative example 1
After porous material is cut into a certain size, material is fixed using porous material fixture, porous material and fixture Between there is annular sealing gaskets to prevent fluid seepage.Water is filled in fixture fluid chamber, and passes through observation window and confirms porous material Surface bubble-free.
Gas buffer cavity volume is reduced to residue about 10mL air chambers, is connected gas piping, will be used peristaltic pump as gas Body injection device, wriggling revolution speed 20rpm, Pressure rise rates are about 20kPa/min at this time.Rate of pressure rise mistake at this time Soon, it is not easy to observe Liquid Penetrant.
Comparative example 2
After porous material is cut into a certain size, material is fixed using porous material fixture, porous material and fixture Between there is annular sealing gaskets to prevent fluid seepage.Water is filled in fixture fluid chamber, and passes through observation window and confirms porous material Surface bubble-free.Gas piping is connected, using centrifugal liquid pump as supercharging device, Pressure rise rates are too fast at this time, existing Equipment can not accurately measure rate of pressure rise, can not also prepare to measure the permeable pressure of porous material.

Claims (6)

1. a kind of permeable compression testing device of porous material, it is characterised in that:Including gas injection apparatus, gas buffer chamber, porous Material fixture and device for pressure measurement;
Porous material fixture is to include closed liquid chamber and hollow ring tablet, and through-hole A is equipped in the upper surface of liquid chamber, in Empty ring plate is placed in above through-hole A, and through-hole A is in the hollow region of hollow ring tablet;Liquid on the outside of through-hole A Annular sealing gaskets is placed in room upper surface, and through-hole A is in the hollow region that annular sealing gaskets is surrounded;Porous material to be measured Material is placed between hollow ring tablet and annular sealing gaskets, the lower surface edge of porous material to be measured and Gask-O-Seal Liquid chamber upper surface on the outside of piece, annular sealing gaskets and through-hole A is amplexiformed, and the upper surface edge of porous material to be measured is in It amplexiforms hollow ring tablet lower face on the outside of empty region;
In applying the thrust to liquid chamber upper surface on hollow ring tablet, the lower surface edge of porous material to be measured can be made It is sealed with the liquid chamber upper surface on the outside of annular sealing gaskets, annular sealing gaskets and through-hole A;
The lower part of gas buffer chamber is connected with liquid chamber lower part by pipeline;Pass through pipeline and gas in the top of gas buffer chamber The gas outlet of body injection device is connected;Device for pressure measurement is equipped in gas buffer chamber top.
2. device as described in claim 1, it is characterised in that:The gas injection apparatus may be used peristaltic pump, diaphragm pump or Gear pump.
3. device as described in claim 1, it is characterised in that:The acting as of the gas buffer chamber further reduces gas pressure Increase rate, improve permeable pressure measurement accuracy.
4. device as described in claim 1, it is characterised in that:3 or more are evenly equipped in hollow ring tablet edge Through-hole, it is corresponding in the threaded hole that 3 or more are offered on liquid chamber upper wall surface, after the screw rod of 3 or more is each passed through through-hole It is screwed togather with corresponding threaded hole.
5. device as described in claim 1, it is characterised in that:Transparent windows are equipped in the lower face of liquid chamber;The observation The effect of window is after injection water or electrolyte, and whether observation porous electrode surface has bubble.
6. device as claimed in claim 5, it is characterised in that:Through-hole B is equipped in the lower face of liquid chamber, is equipped at through-hole B Transparent material plate, the edge airtight connection of the upper surface of transparent material plate and through-hole B, lower face or internal face, is formed saturating Bright observation window.
CN201721708213.5U 2017-12-11 2017-12-11 A kind of permeable compression testing device of porous material Withdrawn - After Issue CN207472733U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721708213.5U CN207472733U (en) 2017-12-11 2017-12-11 A kind of permeable compression testing device of porous material

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721708213.5U CN207472733U (en) 2017-12-11 2017-12-11 A kind of permeable compression testing device of porous material

Publications (1)

Publication Number Publication Date
CN207472733U true CN207472733U (en) 2018-06-08

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CN201721708213.5U Withdrawn - After Issue CN207472733U (en) 2017-12-11 2017-12-11 A kind of permeable compression testing device of porous material

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109900612A (en) * 2017-12-11 2019-06-18 中国科学院大连化学物理研究所 A kind of permeable compression testing device of porous material

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109900612A (en) * 2017-12-11 2019-06-18 中国科学院大连化学物理研究所 A kind of permeable compression testing device of porous material
CN109900612B (en) * 2017-12-11 2023-12-15 中国科学院大连化学物理研究所 Porous material water permeability pressure testing device

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Granted publication date: 20180608

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Granted publication date: 20180608

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