CN207468747U - Prepare the electrolysis installation of high purity titanium - Google Patents
Prepare the electrolysis installation of high purity titanium Download PDFInfo
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- CN207468747U CN207468747U CN201721566818.5U CN201721566818U CN207468747U CN 207468747 U CN207468747 U CN 207468747U CN 201721566818 U CN201721566818 U CN 201721566818U CN 207468747 U CN207468747 U CN 207468747U
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- electrolysis
- degreaser
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Abstract
The utility model prepares the electrolysis installation of high purity titanium, belongs to the preparation field of titanium.Purpose is that by the recycling of electrolyte solution, saves production cost.Cathode plate and painting titanium anode plate including electrolysis reactor and positioned at electrolysis reactor；The electrolyte ingress pipe being connected with electrolysis reactor cavity is provided on the outside of electrolysis reactor；It is provided in electrolysis reactor positioned at the diversion pipe applied below titanium anode plate, one end stretches into outside electrolysis reactor and is provided with anolyte outlet；The anode diaphragm bag being connected with diversion pipe is set with outside painting titanium anode plate；Extraction tank and degreaser are further included, the inlet of extraction tank is connected with the anolyte outlet of diversion pipe, and the liquid outlet of extraction tank is connected with electrolyte ingress pipe by degreaser.The utility model not only realizes the recycling of electrolyte, also maintains the stability of electrolyte solution, the ingredient of electrolyte solution is avoided to change, so as to improve the quality of high-purity titanium products of subsequent production.
Description
Technical field
The utility model belongs to the preparation field of titanium, particularly prepares the electrolysis installation of high purity titanium.
Background technology
Titanium is because density is low, corrosion resistance, good mechanical property, and biocompatibility is excellent, is widely used in aviation boat
Its manufacture, dentistry processing and orthopaedics implantation processing and other fields.At present, by Ti content 3N and more than titanium be known as high purity titanium, mesh
Before, fused salt electrolysis process is one of main method for producing high purity titanium.The electrolyte solution utilization rate of current fused salt electrolysis process is low,
It is increased so as to cause the cost of fused salt electrolysis process.
Utility model content
The technical problem to be solved by the utility model is to provide a kind of electrolysis installations for preparing high purity titanium, can realize electricity
Production cost is saved in the recycling of electrolyte solution.
The technical solution adopted in the utility model is：The electrolysis installation of high purity titanium is prepared, including electrolysis reactor, cathode plate
With the painting titanium anode plate for electrolysis, electrolysis reactor seals the closed container formed for reactant and reaction lid；
The electrolyte ingress pipe being connected with electrolysis reactor cavity is provided on the outside of electrolysis reactor；
The cathode plate and painting titanium anode plate are located in electrolysis reactor, diversion pipe are provided in electrolysis reactor, institute
It states diversion pipe to be located at below painting titanium anode plate, one end stretches into outside electrolysis reactor and is provided with anolyte outlet；Applying titanium sun
Anode diaphragm bag is set with outside pole plate；The lower end of the anode diaphragm bag is connected with diversion pipe；
Including anolyte recovery system, the anolyte recovery system includes extraction tank and degreaser, the extraction tank
Inlet be connected with the anolyte outlet of diversion pipe, the liquid outlet of extraction tank is connected with the entrance of degreaser, deoils
The outlet of device is connected with electrolyte ingress pipe.
Further, the degreaser includes filtering ponds and separate tank；It is provided in the filtering ponds every strainer, it is described
Filtering ponds are divided into epimere filtrate area and hypomere every filter area every strainer；The entrance of the filtrate area and separate tank passes through drainage arrangement
It is connected；The entrance of the degreaser is located at hypomere every filter area.
Further, partition board is provided in the separate tank, separate tank is separated into leading portion oil separation area with after by the partition board
Section drainage region；It is provided with the spacing for connecting oil separation area and drainage region between the lower end of the partition board and the bottom of pond of separate tank, and every
The upper end of plate is higher than the liquid level of separate tank；The outlet of the degreaser is located at drainage region.
Further, the entrance of the separate tank is higher than the outlet of degreaser.
Further, the filtering ponds are located at the top of separate tank, and the drainage arrangement is siphon drainage device.
The beneficial effects of the utility model are：This prepares the electrolysis installation of high purity titanium, since anode diaphragm bag will not occur
The electrolyte of cell reaction is isolated, and the electrolyte that cell reaction occurs is drawn by diversion pipe with the electrolyte of cell reaction occurs
High-purity titanium products are extracted after going out, and except degreasing, makes to be used again after it is consistent with original bath composition, not only realize
The recycling of electrolyte, also maintains the stability of electrolyte solution, the ingredient of electrolyte solution is avoided to change, from
And improve the quality of high-purity titanium products of subsequent production.
Description of the drawings
FIG. 1 is a schematic structural view of the utility model；
In figure, electrolysis reactor 1, reaction lid 12, cathode plate 2, applies titanium anode plate 3, drainage arrangement 4, electrolysis at reactant 11
Liquid ingress pipe 5, diversion pipe 6, anolyte outlet 61, anode diaphragm bag 7, extraction tank 8, degreaser 9, filtering ponds 91, every strainer
911st, filtrate area 912, every filter area 913, separate tank 92, partition board 921, oil separation area 922, drainage region 923.
Specific embodiment
The utility model is described further with reference to the accompanying drawings and examples as follows：
The electrolysis installation of high purity titanium is prepared, including electrolysis reactor 1, cathode plate 2 and the painting titanium anode plate 3 for electrolysis,
Electrolysis reactor 1 is reactant 11 and the closed container of the reaction sealing formation of lid 12；
The electrolyte ingress pipe 5 being connected with 1 cavity of electrolysis reactor is provided in 1 outside of electrolysis reactor；
The cathode plate 2 and painting titanium anode plate 3 are located in electrolysis reactor 1, and diversion pipe is provided in electrolysis reactor 1
6, the diversion pipe 6, which is located at, applies 3 lower section of titanium anode plate, and one end stretches into outside electrolysis reactor 1 and is provided with anolyte outlet 61；
Anode diaphragm bag 7 is set with applying 3 outside of titanium anode plate；The lower end of the anode diaphragm bag 7 is connected with diversion pipe 6；
Including anolyte recovery system, the anolyte recovery system includes extraction tank 8 and degreaser 9, the extraction
The inlet of slot 8 is connected with the anolyte outlet 61 of diversion pipe 6, and the liquid outlet of extraction tank 8 is connected with the entrance of degreaser 9
Logical, the outlet of degreaser 9 is connected with electrolyte ingress pipe 5.
During electrolysis, electrolyte is transported to 1 cavity of electrolysis reactor by electrolyte ingress pipe 5, electrolyte immerse anode every
It is electrolysed in film bag 7, the anolyte after electrolysis enters diversion pipe 6 by the lower end of anode diaphragm bag 7, and by anolyte outlet 61
Output is to extraction tank 8, and back extraction obtains high-purity titanium products in extraction tank 8, and anolyte then goes out to deoil in degreaser 9
Fat, and the outlet for passing through degreaser 9 is sent the cavity of electrolysis reactor 1 back to through electrolyte ingress pipe 5 and is reused.
This prepares the electrolysis installation of high purity titanium, electrolyte and the generation that cell reaction will not occur due to anode diaphragm bag 7
The electrolyte isolation of cell reaction, and high-purity titanium products are extracted after the electrolyte that cell reaction occurs is drawn by diversion pipe 6, and
Except degreasing, make to be used again after it is consistent with original bath composition, not only realize the recycling of electrolyte, also
The stability of electrolyte solution is maintained, the ingredient of electrolyte solution is avoided to change, so as to improve the height of subsequent production
The quality of pure titanium products.
In order to fully filter out the grease in electrolyte, it is preferred that the degreaser 9 includes filtering ponds 91 and separate tank
92；Be provided in the filtering ponds 91 every strainer 911, it is described every strainer 911 filtering ponds 91 are divided be epimere filtrate area 912 and under
Duan Gelv areas 913；The filtrate area 912 is connected with the entrance of separate tank 92 by drainage arrangement 4；The degreaser 9
Entrance is located at hypomere every filter area 913.
The dual effect deoiled, enhance degreasing is realized by filtering ponds 91 and separate tank 92.
Since diversion pipe 6 is located at the lower part of electrolysis reactor 1, the structure of the filtering ponds 91, conducive to the anode in diversion pipe 6
Liquid flows out automatically, by grease by completely cutting off every strainer 911 in hypomere every filter area 913.
Due to grease floating with the water surface on, in order to further improve effect of deoiling, it is preferred that set in the separate tank 92
There is partition board 921, separate tank 92 is separated into leading portion oil separation area 922 and back segment drainage region 923 by the partition board 921；The partition board 921
Lower end and the bottom of pond of separate tank 92 between be provided with the spacing for connecting oil separation area 922 and drainage region 923, and partition board 921 is upper
End is higher than the liquid level of separate tank 92；The outlet of the degreaser 9 is located at drainage region 923.Partition board 921 will float with liquid level on
Grease is isolated in leading portion oil separation area 922, and the liquid below grease is then by between the lower end of partition board 921 and the bottom of pond of separate tank 92
Spacing flow into drainage region 923, so as to fulfill water-oil separating.
In order to realize the automatic outflow of liquid, it is preferred that the entrance of the separate tank 92 is higher than the outlet of degreaser 9.
In order to avoid using additionaling power, with energy saving, it is preferred that the filtering ponds 91 are located at the upper of separate tank 92
Side, the drainage arrangement 4 are siphon drainage device.
Claims (5)
1. prepare the electrolysis installation of high purity titanium, it is characterised in that：Including electrolysis reactor (1), cathode plate (2) and for electrolysis
Titanium anode plate (3) is applied, electrolysis reactor (1) seals the closed container formed for reactant (11) and reaction lid (12)；
The electrolyte ingress pipe (5) being connected with electrolysis reactor (1) cavity is provided on the outside of electrolysis reactor (1)；
The cathode plate (2) and painting titanium anode plate (3) are provided in electrolysis reactor (1) and lead in electrolysis reactor (1)
Flow tube (6), positioned at applying below titanium anode plate (3), one end stretches into electrolysis reactor (1) outside and is provided with the diversion pipe (6)
Anolyte outlet (61)；Applying anode diaphragm bag (7) is set with outside titanium anode plate (3)；The lower end of the anode diaphragm bag (7)
It is connected with diversion pipe (6)；
Including anolyte recovery system, the anolyte recovery system includes extraction tank (8) and degreaser (9), the extraction
The inlet of slot (8) is connected with the anolyte outlet (61) of diversion pipe (6), liquid outlet and the degreaser (9) of extraction tank (8)
Entrance be connected, the outlet of degreaser (9) is connected with electrolyte ingress pipe (5).
2. the electrolysis installation as described in claim 1 for preparing high purity titanium, it is characterised in that：The degreaser (9) included
Filter tank (91) and separate tank (92)；It is provided in the filtering ponds (91) every strainer (911), it is described to be filtered every strainer (911)
Pond (91) is divided into epimere filtrate area (912) and hypomere every filter area (913)；The filtrate area (912) and the entrance of separate tank (92)
It is connected by drainage arrangement (4)；The entrance of the degreaser (9) is located at hypomere every filter area (913).
3. the electrolysis installation as claimed in claim 2 for preparing high purity titanium, it is characterised in that：It is provided in the separate tank (92)
Separate tank (92) is separated into leading portion oil separation area (922) and back segment drainage region (923) by partition board (921), the partition board (921)；Institute
It states to be provided between the lower end of partition board (921) and the bottom of pond of separate tank (92) and connect between oil separation area (922) and drainage region (923)
Away from, and the upper end of partition board (921) is higher than the liquid level of separate tank (92)；The outlet of the degreaser (9) is located at drainage region
(923)。
4. the electrolysis installation as claimed in claim 3 for preparing high purity titanium, it is characterised in that：The entrance of the separate tank (92) is high
In the outlet of degreaser (9).
5. the electrolysis installation for preparing high purity titanium as described in Claims 2 or 3 or 4, it is characterised in that：Filtering ponds (91) position
In the top of separate tank (92), the drainage arrangement (4) is siphon drainage device.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721566818.5U CN207468747U (en) | 2017-11-21 | 2017-11-21 | Prepare the electrolysis installation of high purity titanium |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721566818.5U CN207468747U (en) | 2017-11-21 | 2017-11-21 | Prepare the electrolysis installation of high purity titanium |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207468747U true CN207468747U (en) | 2018-06-08 |
Family
ID=62262028
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721566818.5U Active CN207468747U (en) | 2017-11-21 | 2017-11-21 | Prepare the electrolysis installation of high purity titanium |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207468747U (en) |
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2017
- 2017-11-21 CN CN201721566818.5U patent/CN207468747U/en active Active
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