CN207463234U - A kind of production equipment of sodium Diacetate - Google Patents
A kind of production equipment of sodium Diacetate Download PDFInfo
- Publication number
- CN207463234U CN207463234U CN201721534506.6U CN201721534506U CN207463234U CN 207463234 U CN207463234 U CN 207463234U CN 201721534506 U CN201721534506 U CN 201721534506U CN 207463234 U CN207463234 U CN 207463234U
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- CN
- China
- Prior art keywords
- autoclave body
- production equipment
- stirring blade
- sodium diacetate
- driving spindle
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Abstract
The utility model provides a kind of production equipment of sodium Diacetate, include the autoclave body of horizontal reacting kettle, it is horizontal in the autoclave body to be equipped with driving spindle, described driving spindle one end is connected with driving motor, the driving spindle is equipped with and is connected with agitating device, the stirring blade includes internal helical blades and external spiral blade, described two stirring blades are in reversed distributing installation along the center line where driving spindle, autoclave body outer surface side is connected with chuck, by in chuck circulating hot water realize in kettle reactant carry out duration heating, the utility model provides a kind of horizontal reacting kettle, it stirs evenly, it is easy to operate, the synthesis of sodium Diacetate and dry two procedures are completed in autoclave body and can self-emptyings simultaneously.
Description
Technical field
The utility model is related to technical field of chemical, specifically, being related to a kind of production equipment of sodium Diacetate.
Background technology
Sodium Diacetate is a kind of multi-functional edible chemical, drug chemical, is mainly used as food and feed industry
Preservative, mould inhibitor, chelating agent, flavoring agent, PH conditioning agents, meat products preservative agent and composite type mouldproof agent primary raw material.
With high-effect anti-mould, the fresh-keeping, value that has additional nutrients, improve palatability, be particularly suitable for corn, cereal it is fresh-keeping.It is domestic at present
The technique of outer large-scale production sodium Diacetate mainly have sodium acetate-method of acetic acid, acetic acid~acetic anhydride-sodium acetate method and acetic acid-
Sodium-hydroxide method.
During traditional sodium Diacetate prepares, the degree of automation is low, and operating personnel is needed to be manipulated in real time, in order to
Product can the reaction was complete increases purity, often require to use a large amount of human resources be responsible for purification repeatedly, the manipulation of equipment and
The processes such as the examination and test of products this reduces the productive profit space of enterprise, and increase security risk.
Utility model content
In order to achieve the above objectives, the utility model discloses a kind of production equipment of sodium Diacetate, including：
Autoclave body, the autoclave body upper end connection are equipped with solid material import and liquid material import, the autoclave body lower end connection
It is horizontal in the autoclave body to be equipped with driving spindle, described driving spindle one end and the drive outside the autoclave body equipped with discharge port
Dynamic motor is connected；
Agitating device, including helical-ribbon type stirring blade, the helical-ribbon type stirring blade is fixed along driving spindle for axle center
Connection setting.
In order to make material stirring more fully with uniformly, improving stirring efficiency and mixing quality, preferred technical solution
Be, the helical-ribbon type stirring blade include interior ribbon stirring blade and outer ribbon stirring blade, the interior ribbon stirring blade and
External screw thread stirring blade is along installing and be arranged alternately in the opposite direction in driving spindle, in the interior ribbon stirring blade
Heart line along centered on driving spindle the circular helix coiling of line form.
In order to be heated evenly the material in autoclave body, slow down reaction process, convenient for observation, preferred technical solution is institute
It states autoclave body outer wall and is connected with chuck, the production equipment further includes：Circulation hot-water system, the circulation hot-water system include heat
Water pump group, feed pipe and return pipe, described feed pipe one end are connected to chuck, and the other end is connected with pumping water device water outlet,
Described return pipe one end is connected to chuck, and the other end is connected with pumping water device water inlet.
For the ease of the dry parsing of reactant, preferred technical solution is to further include：Negative pressure device, the negative pressure dress
It puts by being connected inside negative-pressure pipeline and autoclave body.
For the ease of adjusting the rotating speed of agitating device proportioning, mixing quality is improved, preferred technical solution is in addition, the drive
Dynamic that speed reducer is connected between main shaft and driving motor, the driving motor is variable-frequency motor.
For the ease of monitor in real time autoclave body internal-response object pressure and temperature and chuck in circulating hot water pressure and
Temperature, preferred technical solution are that first pressure sensor and the first temperature sensor are connected with inside the autoclave body, described
Second pressure sensor and second temperature sensor are connected with inside chuck, the first pressure sensor, the first temperature pass
Sensor, second pressure sensor and second temperature sensor are electrically connected with the display device outside the autoclave body.
For the ease of observing the response situation of autoclave body internal-response object, preferred technical solution is, the solid material into
Mouth is connected with the sealing that it is coordinated to use, and peep hole is connected in the sealing.
Sodium Diacetate belongs to edible chemical, and has negative pressure technique inside autoclave body, in order to protect the safety and sanitation of material and
The safety of preparation process, preferred technical solution are that the equipment integrally uses stainless steel.
In order to give autoclave body there are spare mouth, preferred technical solution is that the autoclave body upper end is connected with spare mouth.
For the ease of the self-emptying of discharge port, prevent material from being deposited in discharge port, preferred technical solution is institute
It states discharge port and is connected with rotary discharge valve.
The utility model has the following advantages that：
(1) a kind of production equipment of sodium Diacetate in horizontal reacting kettle by being connected with along in being reversely distributed
Ribbon stirring blade and outer ribbon stirring blade, stir evenly, easy to operate, are conducive to improve stirring efficiency and mixing quality simultaneously
Property that raising parallel reaction is selectively and the reaction was complete.
(2) a kind of production equipment of sodium Diacetate is by negative pressure device, by the synthesis of material and dry two procedures
It is completed in autoclave body simultaneously, self-emptying is realized by the rotary discharge valve for being connected at discharge port.
Description of the drawings
It, below will be right in order to illustrate more clearly of specific embodiment of the present invention or technical solution of the prior art
Specific embodiment or attached drawing needed to be used in the description of the prior art are briefly described, it should be apparent that, it is described below
In attached drawing be some embodiments of the present invention, for those of ordinary skill in the art, do not making the creative labor
Under the premise of, it can also be obtained according to these attached drawings other attached drawings.
Fig. 1 is 1 overall structure figure of the utility model embodiment；
Fig. 2 is 1 autoclave body internal structure chart of the utility model embodiment；
Fig. 3 is 1 autoclave body side view of the utility model embodiment；
Fig. 4 is 1 stirring blade structure chart of the utility model embodiment；
Fig. 5 is 2 stirring blade structure chart of the utility model embodiment；
Fig. 6 is 2 stirring blade connection figure of the utility model embodiment.
In figure：1. autoclave body；2. agitating device；3. circulation hot-water system；4. negative pressure device；1-2. solid material imports；1-
3. liquid material import；1-4. discharge port；1-5. driving spindle；1-6. driving motor；1-7. speed reducer；1-8. first pressures pass
Sensor；The first temperature sensors of 1-9.；1-10. sealing；1-11. spare mouth；1-12. rotary discharge valve；2-1. stirring blade；3-
1 chuck；3-2. hot water pump groups；3-3. return pipe；3-4. feed pipe；3-5. second pressure sensors；3-6. second temperatures sense
Device；4-1. negative-pressure pipeline；Ribbon stirring blade in 2-11.；The outer ribbon stirring blades of 2-12.；2-13. long-neck blade；It is 2-14. short
Neck blade；2-15. semi-circular fastener；2-16. connecting rod；2-17. clamping plate.
Specific embodiment
The technical solution of the utility model is clearly and completely described below in conjunction with attached drawing, it is clear that described
Embodiment is part of the embodiment of the present invention, instead of all the embodiments.Based on the embodiment in the utility model, this field
Those of ordinary skill's all other embodiments obtained without making creative work, belong to the utility model
The range of protection.
Embodiment 1
The utility model is described further below in conjunction with attached drawing.
As shown in Figure 1, Figure 2, Figure 3 shows, the production equipment of a kind of sodium Diacetate provided in this embodiment, including：
Autoclave body 1, the autoclave body 1 are placed across on stent 1-1, and 1 upper end of autoclave body is connected with solid material import
1-2 and liquid material import 1-3,1 lower end of autoclave body are connected with discharge port 1-4, and 1 outer wall of autoclave body is connected with chuck
3-1, horizontal in the autoclave body 1 to be equipped with driving spindle 1-5, described driving spindle 1-5 one end is connected with driving motor 1-6；
Agitating device 2, including helical-ribbon type stirring blade 2-1, the helical-ribbon type stirring blade 2-1 is along driving spindle 1-5
It connects and sets for axle center.
As shown in figure 4, in order to make material stirring more fully with uniformly, improving stirring efficiency and mixing quality, this reality
It is that the helical-ribbon type stirring blade 2-1 includes interior ribbon stirring blade 2-11 and outer ribbon is stirred with novel preferred embodiment
It is axially reversed along driving spindle 1-5 to mix blade 2-12, the interior ribbon stirring blade 2-11 and external screw thread stirring blade 2-12
Installation, the center line of the interior ribbon stirring blade 2-11 along the line centered on driving spindle 1-5 circular helix coiling
It forms.
In order to be heated evenly the material in autoclave body 1, slow down reaction process, convenient for observation, the utility model is preferably real
Scheme is applied in addition, further including：Circulation hot-water system 3, the circulation hot-water system 3 include pumping water device 3-2, feed pipe 3-3 and
Return pipe 3-4, described feed pipe 3-3 one end are connected to chuck 3-1, and the other end is connected with pumping water device 3-2 water outlets, described
Water return outlet 3-4 one end is connected to chuck 3-1, and the other end is connected with pumping water device 3-2 water inlets.
For the ease of the dry parsing of reactant, the utility model preferred embodiment is in addition, further include：Negative pressure device
4, the negative pressure device 4 inside negative-pressure pipeline 4-1 and autoclave body 1 by being connected.
For the ease of adjusting the rotating speed of agitating device 2 proportioning, mixing quality, the utility model preferred embodiment are improved
It is that speed reducer 1-7 is connected between the driving spindle 1-5 and driving motor 1-6, the driving motor 1-6 is variable-frequency electric
Machine.
For the ease of the pressure of circulating hot water in the real time monitoring pressure and temperature of 1 internal-response object of autoclave body and chuck 3-1
Power and temperature, the utility model preferred embodiment are that the autoclave body 1 is connected with first pressure sensor 1-8 and first
Temperature sensor 1-9, the chuck 3-1 are connected with second pressure sensor 3-5 and second temperature sensor 3-6.
For the ease of observing the response situation of 1 internal-response object of autoclave body, the utility model preferred embodiment is in addition, institute
It states solid material import 1-2 and is connected with the sealing 1-10 that it is coordinated to use, described seal is connected with peep hole on 1-10.
Sodium Diacetate belongs to edible chemical, and has negative pressure technique inside autoclave body 1, in order to protect the safety and sanitation of material and
The safety of preparation process, the utility model preferred embodiment are that the equipment is integrally using stainless steel, the kettle
1 outer wall thickness of body is more than the chuck 3-1 outer wall thickness.
In order to give autoclave body 1 there are spare mouth, the utility model preferred embodiment is that 1 upper end of the autoclave body connection is set
There is spare mouth 1-11.
For the ease of the self-emptying of discharge port 1-4, prevent material from being deposited in discharge port 1-4, the utility model is excellent
The embodiment of choosing is that the discharge port 1-4 is connected with rotary discharge valve 1-12.
A kind of technological process of the production equipment of sodium Diacetate be divided into feed intake → stirring → heat → negative pressure parsing → discharging,
Reaction mass is put by solid material import 1-2, agitating device 2 is thrown during stirring by liquid material import 1-3 again
Enter reaction mass, open pumping water device 3-2, the hot water of thermophilic is imported and heats temperature in autoclave body 1 in chuck 3-1, by the
The pressure and temperature of one pressure sensor 1-8 and the first temperature sensor 1-9 real time monitoring 1 internal-response objects of autoclave body, by the
The pressure and temperature of circulating hot water, is treated anti-in two pressure sensor 3-5 and second temperature sensor 3-6 real time monitoring chucks 3-1
After answering fully, negative pressure device 4 is opened, other all uncorrelated pipeline valves of closing autoclave body 1 make the reactant in autoclave body 1
Negative pressure drying parses, generation sodium Diacetate crystallization, at this time by rotary discharge valve 1-12 automatically by sodium Diacetate finished product from autoclave body 1
Interior export.
Embodiment 2
As shown in figure 5, the present embodiment devises a kind of stirring blade 2, the stirring blade 2 include long-neck blade 2-13 and
Short neck blade 2-14, the long-neck blade 2-13 are connected to semi-circular by connecting rod 2-16 respectively with the short neck blade 2-14
Fastener 2-15, the stirring blade 2 are equipped with multiple and are fixedly connected on driving spindle 1-5 by semi-circular fastener 2-15,
The long-neck blade 2-13 replaces connection setting with the short neck blade 2-14 in the opposite direction along driving spindle 1-5, passes through
The angle of adjacent stirring blade 2 is adjusted, is connected to adjacent long-neck blade 2-13 and adjacent short neck blade 2-14 to drive
Centered on main shaft 1-5 on the helix of line.
As shown in fig. 6, in order to optimize the structure of long-neck blade 2-13 and short neck blade 2-14, convenient for adjacent stirring blade 2
Between installation, the utility model preferred embodiment is, to be ginseng with the perpendicular end face of line centered on driving spindle 1-5
It shows up, arc angle and the short neck blade 2-14 perpendicular projection of the long-neck blade 2-13 perpendicular projections in the reference plane
It is equal in the arc angle of the reference plane.
For the ease of the connection of two groups of semi-circular fastener 2-15 and driving spindle 1-5, semi-circular fastener 2-15 is reinforced
With the connection of driving spindle 1-5, the utility model preferred embodiment is that the semi-circular fastener 2-15 is led close to driving
The semicircle arc dia at axis 1-5 ends is equal with driving spindle 1-5 diameters, and the semi-circular fastener 2-15 is close to driving spindle 1-5
End is connected with rubber layer, and the semi-circular fastener 2-15 both ends are connected with clamping plate 2-17, and the clamping plate 2-17 is equipped with
The bolt hole that fitted bolt uses.
It is stirred in autoclave body 1 for the ease of stirring blade 2, reduces resistance of the stirring blade 2 with respect to material in autoclave body 1, this
Utility model preferred embodiment is that the long-neck blade 2-13 is equipped with multiple logical with the short neck blade 2-14 outer surfaces
Hole.
The axial agitation with radial direction, the preferred technical side of the utility model are realized in autoclave body 1 for the ease of stirring blade 2
Case is that distances of the long-neck blade 2-13 with respect to driving spindle 1-5 is more than the short neck blade 2-14 with respect to driving spindle 1-5
Distance.
As different from Example 1, the stirring blade 2 of the present embodiment 2 is equipped with multiple and independently installed, during installation, is ensured
Adjacent long-neck blade 2-13 ensures adjacent short neck blade 2-14 on a helix, the phase on a helix
Adjacent stirring blade 2 can also be there are isometric distance, when stirring blade 2 damages in this way in autoclave body 1, as long as by phase when installing
The stirring blade 2 that position should be damaged is removed and is reinstalled, and needs entirety when being damaged from stirring blade 2 in embodiment 1
It replaces.
Obviously, the above embodiments are merely examples for clarifying the description, and is not intended to limit the embodiments.It is right
For those of ordinary skill in the art, can also make on the basis of the above description it is other it is various forms of variation or
It changes.There is no necessity and possibility to exhaust all the enbodiments.And the obvious variation thus extended out or
Among changing still in the protection domain of the invention.
Claims (9)
1. a kind of production equipment of sodium Diacetate, which is characterized in that including：
Autoclave body (1), autoclave body (1) the upper end connection is equipped with solid material import (1-2) and liquid material import (1-3), described
The connection of autoclave body (1) lower end is equipped with discharge port (1-4), and level is equipped with driving spindle (1-5), the driving master in the autoclave body (1)
Axis (1-5) one end is connected with positioned at the external driving motor (1-6) of the autoclave body (1)；
Agitating device (2), including helical-ribbon type stirring blade (2-1), the helical-ribbon type stirring blade (2-1) is along driving spindle
(1-5) is fixedly connected with setting for axle center.
A kind of 2. production equipment of sodium Diacetate according to claim 1, which is characterized in that the helical-ribbon type stirring blade
(2-1) includes interior ribbon stirring blade (2-11) and outer ribbon stirring blade (2-12), the interior ribbon stirring blade (2-11)
With outer ribbon stirring blade (2-12) along installing and be arranged alternately in the opposite direction in driving spindle (1-5), the interior spiral shell
Center line with stirring blade (2-11) is formed along the circular helix coiling of the line centered on driving spindle (1-5).
3. the production equipment of a kind of sodium Diacetate according to claim 1, which is characterized in that autoclave body (1) outer wall connects
Chuck (3-1) is equipped with, the production equipment further includes：Circulation hot-water system (3), the circulation hot-water system (3) is including heat
Water pump group (3-2), feed pipe (3-3) and return pipe (3-4), described feed pipe (3-3) one end is connected to chuck (3-1), another
End is connected with hot water pump group (3-2) water outlet, and described return pipe (3-4) one end is connected to chuck (3-1), the other end and hot water
Pump group (3-2) water inlet is connected.
4. a kind of production equipment of sodium Diacetate according to claim 1, which is characterized in that negative pressure device (4) is further included,
The negative pressure device (4) inside negative-pressure pipeline (4-1) and autoclave body (1) by being connected.
A kind of 5. production equipment of sodium Diacetate according to claim 1, which is characterized in that the driving spindle (1-5)
Speed reducer (1-7) is connected between driving motor (1-6), the driving motor (1-6) is variable-frequency motor.
6. the production equipment of a kind of sodium Diacetate according to claim 3, which is characterized in that connect inside the autoclave body (1)
First pressure sensor (1-8) and the first temperature sensor (1-9) are equipped with, second is connected with inside the chuck (3-1)
Pressure sensor (3-5) and second temperature sensor (3-6), the first pressure sensor (1-8), the first temperature sensor
(1-9), second pressure sensor (3-5) and second temperature sensor (3-6) are electric with the external display device of the autoclave body (1)
Connection.
A kind of 7. production equipment of sodium Diacetate according to claim 1, which is characterized in that the solid material import
(1-2) is connected with the sealing (1-10) that it is coordinated to use, and peep hole is connected on the sealing (1-10).
8. the production equipment of a kind of sodium Diacetate according to claim 1, which is characterized in that autoclave body (1) upper end connects
It is equipped with spare mouth (1-11).
9. the production equipment of a kind of sodium Diacetate according to claim 1, which is characterized in that the discharge port (1-4) is even
It is equipped with rotary discharge valve (1-12).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721534506.6U CN207463234U (en) | 2017-11-16 | 2017-11-16 | A kind of production equipment of sodium Diacetate |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721534506.6U CN207463234U (en) | 2017-11-16 | 2017-11-16 | A kind of production equipment of sodium Diacetate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207463234U true CN207463234U (en) | 2018-06-08 |
Family
ID=62260975
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721534506.6U Expired - Fee Related CN207463234U (en) | 2017-11-16 | 2017-11-16 | A kind of production equipment of sodium Diacetate |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207463234U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117443010A (en) * | 2023-12-19 | 2024-01-26 | 江苏科洛吉健康科技有限公司 | Crystallization device is used in processing of sodium diacetate |
-
2017
- 2017-11-16 CN CN201721534506.6U patent/CN207463234U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN117443010A (en) * | 2023-12-19 | 2024-01-26 | 江苏科洛吉健康科技有限公司 | Crystallization device is used in processing of sodium diacetate |
| CN117443010B (en) * | 2023-12-19 | 2024-03-26 | 江苏科洛吉健康科技有限公司 | Crystallization device is used in processing of sodium diacetate |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180608 Termination date: 20201116 |