CN207463224U - Experiment reaction kettle device - Google Patents
Experiment reaction kettle device Download PDFInfo
- Publication number
- CN207463224U CN207463224U CN201721459492.6U CN201721459492U CN207463224U CN 207463224 U CN207463224 U CN 207463224U CN 201721459492 U CN201721459492 U CN 201721459492U CN 207463224 U CN207463224 U CN 207463224U
- Authority
- CN
- China
- Prior art keywords
- reaction kettle
- blade unit
- experiment
- paddle
- kettle device
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model is related to test with reaction kettle device, rabbling mechanism is arranged in autoclave body, rabbling mechanism is included in the multiple blade units set on agitating shaft, blade unit has scraper part, through portion, paddle portion and fixed part, scraper part is located at the front end of blade unit, the outer rim of scraper part is bonded with inner wall of kettle, through portion is located at the middle part of blade unit, both ends are connected respectively with scraper part and paddle portion, through portion is the plank of an arc facade, it is offered in through portion multiple through hole, paddle portion is located at the tail end of blade unit, the tail portion in paddle portion is connected with the tail end of through portion, the front end in paddle portion has the wedge structure shunk, the front end in paddle portion and inner wall of kettle are spaced apart, fixed part is used to blade unit being attached by through portion and agitating shaft, the fixed through portion of fixed part one end connection, the other end and stirring axis connection.The utility model can increase the mixed effect of reaction kettle.
Description
Technical field
The utility model is related to laboratory consersion unit structures, and in particular to experiment reaction kettle device.
Background technology
In the prior art, it researches and develops a reaction process flow and generally requires multiple stages.Including lab scale, pilot scale,
It could be used for plant produced later.Lab scale can be find reaction process the problem of early stage, and can be in laboratory stage
These problems are just solved or taken with corresponding measure, reduces the input of research and development, sufficient standard is carried out for expanding production
It is standby.In synthesis field, reaction kettle is a kind of important reaction unit, however in existing laboratory, the reaction kettle of design without
The problem of method meets the needs of blending or even if meeting, but it is excessive to cause reaction kettle volume, cost increase.
Invention content
The good experiment reaction kettle device of effect is blended the purpose of this utility model is to provide a kind of.
To achieve these goals, the experiment reaction kettle apparatus structure of the utility model is as follows：
Autoclave body and rabbling mechanism including reaction kettle, rabbling mechanism are arranged in autoclave body, and the rabbling mechanism is included in
The multiple blade units set on agitating shaft, the blade unit have scraper part, through portion, paddle portion and fixed part,
The scraper part is located at the front end of blade unit, and the outer rim of scraper part is bonded with inner wall of kettle,
The through portion is located at the middle part of blade unit, and both ends are connected respectively with scraper part and paddle portion, through portion one
The plank of arc facade, offered in through portion it is multiple through hole,
The paddle portion is located at the tail end of blade unit, and the tail portion in paddle portion is connected with the tail end of through portion, the front end in paddle portion
Wedge structure with contraction, the front end in paddle portion and inner wall of kettle are spaced apart,
The fixed part is for blade unit to be attached by through portion and agitating shaft, described fixed part one end
The fixed through portion of connection, the other end and stirring axis connection.
Aforesaid reaction vessel device also has following optimization structure：
One or more imports for adding each reactive component are provided on the autoclave body and are discharged for reacting
Outlet.
Liquid storage pipe is provided in the import.
Valve is provided in the inlet and outlet.
The bleeding point for vacuumizing is provided on the autoclave body.
The blade unit stepped is fixed on agitating shaft around the axial screw of agitating shaft.
There is deflection angle between the blade unit in three-dimensional.
The shaft bottom is provided with agitating paddle.
Pedestal is provided with below the autoclave body, autoclave body is made of cover and cavity sealed connection.
The utility model can the prior art compare, hybrid blade can realize including blending, prevent liquid level deposition etc. works
With, can pass through the structure of scraper part, through portion and paddle portion increase turbulence, increase mixed effect.
[description of the drawings]
Fig. 1 is the structure diagram of experiment reaction kettle device；
Fig. 2 is the partial schematic diagram of rabbling mechanism；
In figure, 1. blade unit, 2. agitating shaft, 3. agitating paddle 4. exports 5. autoclave body, 6. import, 7. valve
8. 12. through portion of liquid storage pipe 9. motor, 10. bleeding point, 11. scraper part, 13. connecting portion 14. penetrates hole 15.
Paddle portion.
[specific embodiment]
Hereinafter, be described further with attached drawing for the utility model in conjunction with the embodiments, embodiment and attached drawing are only used for solving
It releases explanation rather than limits the scope of protection of the utility model.
Experiment reaction kettle apparatus structure in the present embodiment is as follows：
The structure of reaction kettle can pass through sealing as shown in Figure 1, autoclave body is made of cover and cavity between cover and cavity
The mating connections such as circle, bolt thread in the internal space for forming a relative closure, are provided with to add each reaction on autoclave body
Two imports of component and the outlet for reacting discharging, are provided with liquid storage pipe, in import, outlet, pumping in each import
Valve is provided on gas port, further in order to fix reaction kettle, pedestal or fixing bracket can also be set below autoclave body
Deng.
Be provided with rabbling mechanism in reaction kettle, rabbling mechanism by the transmissions such as motor, deceleration mechanism, shaft coupling drive into
Row rotation, the present embodiment are studied and are improved mainly for the rabbling mechanism in reaction kettle, and structure is as follows：
Rabbling mechanism is made of the multiple blade units and the agitating paddle of bottom set on agitating shaft, in the present embodiment
Setting is there are two symmetrical blade unit, in other embodiments in order to further increase mixed effect, such as three can be increased,
4th, five, six blade units etc., it is even more, and it sets angle, it can also be various dimensions, the transformation of multi-angle can be with
It is fixed on agitating shaft around the axial screw of agitating shaft is stepped, the blade unit has scraper part, through portion, paddle portion
And fixed part, as shown in Fig. 2,
The scraper part is located at the front end of blade unit, and the outer rim of scraper part is bonded with inner wall of kettle,
The through portion is located at the middle part of blade unit, and both ends are connected respectively with scraper part and paddle portion, through portion one
The plank of arc facade, offered in through portion it is multiple through hole,
The paddle portion is located at the tail end of blade unit, and the tail portion in paddle portion is connected with the tail end of through portion, the front end in paddle portion
Wedge structure with contraction, the front end in paddle portion and inner wall of kettle are spaced apart,
The fixed part is for blade unit to be attached by through portion and agitating shaft, described fixed part one end
The fixed through portion of connection, the other end and stirring axis connection.
In mixing, due to the synergistic effect of the various pieces of blade unit, there is 1+1>2 effect, takes up little area, mixing
Effect is more preferable.It is suitble to use in laboratory or actual production.
Claims (9)
1. a kind of experiment is with reaction kettle device, autoclave body and rabbling mechanism including reaction kettle, rabbling mechanism is arranged in autoclave body,
It is characterized in that the rabbling mechanism is included in the multiple blade units set on agitating shaft, the blade unit has scraper
Portion, through portion, paddle portion and fixed part,
The scraper part is located at the front end of blade unit, and the outer rim of scraper part is bonded with inner wall of kettle,
The through portion is located at the middle part of blade unit, and both ends are connected respectively with scraper part and paddle portion, and through portion is an arc
The plank of facade, offered in through portion it is multiple through hole,
The paddle portion is located at the tail end of blade unit, and the tail portion in paddle portion is connected with the tail end of through portion, and the front end in paddle portion has
The wedge structure of contraction, the front end in paddle portion and inner wall of kettle are spaced apart,
The fixed part is for blade unit to be attached by through portion and agitating shaft, the connection of described fixed part one end
Fixed through portion, the other end and stirring axis connection.
2. experiment as described in claim 1 reaction kettle device, it is characterised in that be provided with to add on the autoclave body
One or more imports of each reactive component and the outlet for reacting discharging.
3. experiment as claimed in claim 2 reaction kettle device, it is characterised in that be provided with liquid storage pipe in the import.
4. experiment as claimed in claim 2 reaction kettle device, it is characterised in that be provided in the inlet and outlet
Valve.
5. experiment as described in claim 1 reaction kettle device, it is characterised in that be provided on the autoclave body true for taking out
Empty bleeding point.
6. experiment as described in claim 1 reaction kettle device, it is characterised in that the blade unit is around the axis of agitating shaft
To being fixed on agitating shaft for spiral step formula.
7. experiment as claimed in claim 6 reaction kettle device, it is characterised in that between the blade unit in three-dimensional
With deflection angle.
8. experiment as described in claim 1 reaction kettle device, it is characterised in that the shaft bottom is provided with stirring
Paddle.
9. experiment as described in claim 1 reaction kettle device, it is characterised in that be provided with pedestal, kettle below the autoclave body
Body is made of cover and cavity sealed connection.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721459492.6U CN207463224U (en) | 2017-11-06 | 2017-11-06 | Experiment reaction kettle device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721459492.6U CN207463224U (en) | 2017-11-06 | 2017-11-06 | Experiment reaction kettle device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207463224U true CN207463224U (en) | 2018-06-08 |
Family
ID=62263003
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721459492.6U Expired - Fee Related CN207463224U (en) | 2017-11-06 | 2017-11-06 | Experiment reaction kettle device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207463224U (en) |
-
2017
- 2017-11-06 CN CN201721459492.6U patent/CN207463224U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180608 Termination date: 20201106 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |