CN207446222U - A kind of 6B acid high-efficiency sulfonation bakes reactor - Google Patents
A kind of 6B acid high-efficiency sulfonation bakes reactor Download PDFInfo
- Publication number
- CN207446222U CN207446222U CN201720911955.1U CN201720911955U CN207446222U CN 207446222 U CN207446222 U CN 207446222U CN 201720911955 U CN201720911955 U CN 201720911955U CN 207446222 U CN207446222 U CN 207446222U
- Authority
- CN
- China
- Prior art keywords
- stirring rod
- reactor
- stirring
- scraping blade
- bakes
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses a kind of 6B acid high-efficiency sulfonations to bake reactor, including autoclave body, it is provided in the autoclave body and extends vertically into the in vivo agitating shaft of kettle, the first stirring rod and the second stirring rod are installed on the agitating shaft, first stirring rod and the second stirring rod are horizontal horizontal, agitating shaft sequentially passes through the middle part of the first stirring rod and the second stirring rod, several scraping blades are respectively equipped on first stirring rod and the second stirring rod, arc stirring sheet is installed on the second stirring rod, the both ends of arc stirring sheet are respectively and fixedly installed to the both ends of the second stirring rod, stirring the tip of the axis is fixedly connected in the middle part of arc stirring sheet, the radian of arc stirring sheet and the bottom radian of autoclave body match.The sulfonation of the utility model, which bakes reactor, efficiently to be disperseed the larger substance of proportion, increase solid phase reaction area, improve reaction efficiency and product yield, while also ensure product quality.
Description
Technical field
The utility model is related to sulfonation baking device technical fields, and in particular to a kind of 6B acid high-efficiency sulfonation bakes reaction
Device.
Background technology
The broad understanding of reactor has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter
It puts, realizes the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.
Reactor is widely used in oil, chemical industry, rubber, pesticide, dyestuff, medicine, food, for completing to vulcanize, nitrifying,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle etc.；Material
Matter generally has carbon manganese steel, stainless steel, zirconium, Ni-based (Kazakhstan, Monel, inconel) alloy and other composite materials.
At present, the agitating mode of reactor has anchor formula, frame, paddle, turbine type, scraper-type, helical-ribbon type etc., but for one
A little special material such as proportions are larger, solid phase reaction sulfonation bakes pattern, single agitating mode be difficult be sufficiently stirred it is anti-
It should.Therefore, it is necessary to designing a kind of new sulfonation bakes reactor, to which efficiently the larger substance of proportion can be disperseed,
Increase solid phase reaction area, improve reaction efficiency and product yield, while also ensure product quality.
The content of the invention
For problems of the prior art, the utility model is by the processing to agitating device, by traditional anchor formula
Fixing axle and the second stirring rod are added in stirring, while increases different angle, the scraping blade of length in stirring, so as to provide one kind
Efficiently the larger substance of proportion can be disperseed, increase solid phase reaction area, improve reaction efficiency and product yield, simultaneously also
It can guarantee that the 6B acid high-efficiency sulfonation of product quality bakes reactor.
To achieve the above object, the technical solution adopted in the utility model is：A kind of 6B acid high-efficiency sulfonation bakes reactor,
Including autoclave body, it is provided in the autoclave body and extends vertically into the in vivo agitating shaft of kettle, first is installed on the agitating shaft
Stirring rod and the second stirring rod, the first stirring rod and the second stirring rod are horizontal horizontal, and agitating shaft sequentially passes through the first stirring rod
With the middle part of the second stirring rod, several scraping blades are respectively equipped on the first stirring rod and the second stirring rod, are installed on the second stirring rod
There is arc stirring sheet, the both ends of arc stirring sheet are respectively and fixedly installed to the both ends of the second stirring rod, the middle part of arc stirring sheet
Stirring the tip of the axis is fixedly connected with, the radian of arc stirring sheet and the bottom radian of autoclave body match.
Agitating shaft is 2 ㎝ with inner wall of kettle distance.
First stirring rod and the second stirring rod angle in 90 °.
The upper surface at the second stirring rod both ends is respectively equipped with the fixinig plate of right angle trigonometry type, two right-angle sides point of fixinig plate
The second stirring rod and arc stirring sheet are not fixedly connected with.
Fixinig plate is isosceles right triangle.
Scraping blade on second stirring rod is set to the first scraping blade, the first scraping blade and the second stirring rod 60 ° of angles of ∽ at 45 °.
First stirring rod is stirred axis and is divided into left-half and right half part, and the end of left-half is equipped with the second scraping blade,
The middle part of left-half is equipped with the 3rd scraping blade, and the end of right half part is equipped with the 4th scraping blade, and the middle part of right half part is equipped with the 5th
Scraping blade, the second scraping blade and the 4th scraping blade are respectively with the first stirring rod into equal angular angle and direction on the contrary, the 3rd scraping blade and
Five scraping blades respectively with the first stirring rod into equal angular angle and direction it is opposite.
Reactor further includes transmission device, kettle cover, A type clamps, and the outer layer of the autoclave body is provided with chuck, and bottom is provided with
Bottom valve, side are provided with heat conductive oil inlet and conduction oil outlet, are provided on the kettle cover into hole, thermometer wrap nozzle, charging
Mouth, visor, vacuum port, drain.
The operation principle of the utility model is：The design with scraping blade can make material overturning dynamics increase on agitating shaft,
Increase material reaction contact area, and reduce stress, ensure product reaction efficiency, traditional agitating device is avoided to bring big negative
Lotus, the halfway phenomenon of reaction.
The beneficial effects of the utility model are：The sulfonation of the utility model bakes reactor can be efficiently larger by proportion
Substance disperse, increase solid phase reaction area, improve reaction efficiency and product yield, while also ensure product quality.
Description of the drawings
Fig. 1 is the sectional view of the utility model；
Fig. 2 is the cross-sectional view of autoclave body；
Fig. 3 is the schematic diagram of kettle cover.
Specific embodiment
In conjunction with attached drawing, the utility model is described in further detail.
As shown in Figs. 1-3, a kind of 6B acid high-efficiency sulfonation bakes reactor, including autoclave body 6, is provided in the autoclave body 6 vertical
The agitating shaft 7 in autoclave body 6 is directly stretched into, the first stirring rod 9 and the second stirring rod 10 are installed on the agitating shaft 7, the
One stirring rod 9 and the second stirring rod 10 are horizontal horizontal, and agitating shaft 7 sequentially passes through the first stirring rod 9 and the second stirring rod 10
Several scraping blades are respectively equipped on middle part, the first stirring rod 9 and the second stirring rod 10, arc stirring is installed on the second stirring rod 10
Piece 12, the both ends of arc stirring sheet 12 are respectively and fixedly installed to the both ends of the second stirring rod 10, and the middle part of arc stirring sheet 12 is consolidated
Surely the end of agitating shaft 7 is connected, the radian of arc stirring sheet 12 matches with the bottom radian of autoclave body 6.
Agitating shaft 7 is 2 ㎝ with 6 inner wall of autoclave body distance.
10 angle in 90 ° of first stirring rod 9 and the second stirring rod.
The upper surface at 10 both ends of the second stirring rod is respectively equipped with the fixinig plate 13 of right angle trigonometry type, and two of fixinig plate 13 are straight
The arm of angle is respectively fixedly connected with the second stirring rod 10 and arc stirring sheet 12.
Fixinig plate 13 is isosceles right triangle.
Scraping blade on second stirring rod 10 is set to the first scraping blade 11,10 60 ° of ∽ at 45 ° of the first scraping blade 11 and the second stirring rod
Angle.
First stirring rod 9 is stirred axis 7 and is divided into left-half and right half part, and the end of left-half is equipped with the second scraping blade
14, the middle part of left-half is equipped with the 3rd scraping blade 15, and the end of right half part is equipped with the 4th scraping blade 16, is set in the middle part of right half part
Have the 5th scraping blade 17, the second scraping blade 14 and the 4th scraping blade 16 respectively with the first stirring rod 9 into equal angular angle and direction on the contrary,
3rd scraping blade 15 and the 5th scraping blade 17 respectively with the first stirring rod 9 into equal angular angle and direction it is opposite.
Reactor further includes transmission device 1, kettle cover 3, A types clamp 4, and the outer layer of the autoclave body 6 is provided with chuck 8, bottom
Bottom valve is provided with, side is provided with heat conductive oil inlet 20 and conduction oil outlet 5, manhole 2, thermometer are provided on the kettle cover 3
Sleeve opening 18, feed inlet 19, visor 21, vacuum port 22, drain 23.
The preferred embodiment of the utility model described in detail above, it should be understood that the ordinary skill people of this field
Member according to the present utility model can conceive without creative work makes many modifications and variations, therefore, all this technology necks
Technical staff passes through logic analysis, reasoning or limited reality on the basis of existing technology according to the design of the utility model in domain
Available technical solution is tested, it all should be in the protection domain being defined in the patent claims.
Claims (8)
1. a kind of 6B acid high-efficiency sulfonation bakes reactor, including autoclave body (6), which is characterized in that is provided in the autoclave body (6) vertical
The agitating shaft (7) in autoclave body (6) is directly stretched into, the first stirring rod (9) and the second stirring are installed on the agitating shaft (7)
Bar (10), the first stirring rod (9) and the second stirring rod (10) are horizontal horizontal, and agitating shaft (7) sequentially passes through the first stirring rod (9)
With the middle part of the second stirring rod (10), several scraping blades are respectively equipped on the first stirring rod (9) and the second stirring rod (10), second stirs
It mixes and arc stirring sheet (12) is installed on bar (10), the both ends of arc stirring sheet (12) are respectively and fixedly installed to the second stirring rod
(10) both ends, are fixedly connected with the end of agitating shaft (7) in the middle part of arc stirring sheet (12), the radian of arc stirring sheet (12) with
The bottom radian of autoclave body (6) matches.
2. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that the agitating shaft (7) and kettle
Body (6) inner wall distance is 2 ㎝.
3. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that first stirring rod (9)
With the second stirring rod (10) angle in 90 °.
4. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that second stirring rod (10)
The upper surface at both ends is respectively equipped with the fixinig plate (13) of right angle trigonometry type, and two right-angle sides of fixinig plate (13) are respectively fixedly connected with
Second stirring rod (10) and arc stirring sheet (12).
5. 6B acid high-efficiency sulfonation according to claim 4 bakes reactor, which is characterized in that the fixinig plate (13) for etc.
Waist right angled triangle.
6. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that second stirring rod (10)
On scraping blade be set to the first scraping blade (11), the first scraping blade (11) and the second stirring rod (10) -60 ° of angles at 45 °.
7. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that first stirring rod (9)
It is stirred axis (7) and is divided into left-half and right half part, the end of left-half is equipped with the second scraping blade (14), in left-half
Portion is equipped with the 3rd scraping blade (15), and the end of right half part is equipped with the 4th scraping blade (16), and the middle part of right half part is equipped with the 5th scraping blade
(17), the second scraping blade (14) and the 4th scraping blade (16) are respectively with the first stirring rod (9) into equal angular angle and direction on the contrary,
Three scraping blades (15) and the 5th scraping blade (17) respectively with the first stirring rod (9) into equal angular angle and direction it is opposite.
8. 6B acid high-efficiency sulfonation according to claim 1 bakes reactor, which is characterized in that the reactor further includes biography
Dynamic device (1), kettle cover (3), A types clamp (4), the outer layer of the autoclave body (6) are provided with chuck (8), and bottom is provided with bottom valve, side
Face is provided with heat conductive oil inlet (20) and conduction oil outlet (5), is provided on the kettle cover (3) into hole (2), thermometer wrap nozzle
(18), feed inlet (19), visor (21), vacuum port (22), drain (23).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720911955.1U CN207446222U (en) | 2017-07-26 | 2017-07-26 | A kind of 6B acid high-efficiency sulfonation bakes reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720911955.1U CN207446222U (en) | 2017-07-26 | 2017-07-26 | A kind of 6B acid high-efficiency sulfonation bakes reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207446222U true CN207446222U (en) | 2018-06-05 |
Family
ID=62247703
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720911955.1U Active CN207446222U (en) | 2017-07-26 | 2017-07-26 | A kind of 6B acid high-efficiency sulfonation bakes reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207446222U (en) |
-
2017
- 2017-07-26 CN CN201720911955.1U patent/CN207446222U/en active Active
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN209530851U (en) | Conducive to the reaction kettle for promoting reaction efficiency | |
| CN208373089U (en) | A kind of production zinc sulfate agitating device | |
| CN206444606U (en) | A kind of multifunctional high pressure collecting agent synthesis reactor | |
| CN207446222U (en) | A kind of 6B acid high-efficiency sulfonation bakes reactor | |
| CN106807311A (en) | A kind of environmental protective type chemical reactor with emission-control equipment | |
| CN205550270U (en) | Synthetic cauldron of former medicine with circulation agitating unit | |
| CN204395941U (en) | New type agitation reactor | |
| CN207385482U (en) | A kind of industrial chemicals stirred autoclave convenient for cleaning | |
| CN108854894A (en) | A kind of stainless steel cauldron | |
| CN207667631U (en) | A kind of composite sterilization algicide compounding kettle | |
| CN208465862U (en) | A kind of highly effective reaction kettle | |
| CN203400714U (en) | Temperature meter jacket of enamel reaction kettle and enamel reaction kettle with same | |
| CN208494232U (en) | A kind of reaction kettle air inlet distributor | |
| CN209173941U (en) | Aqueous Adhesives reaction kettle | |
| CN208771401U (en) | A kind of reaction kettle for furane resins | |
| CN206868216U (en) | Stirred autoclave | |
| CN204865816U (en) | Safe reation kettle | |
| CN207655117U (en) | A kind of concentration kettle for producing sildenafil intermediate | |
| CN209378994U (en) | A kind of reaction kettle for industrial production polyurethane | |
| CN205965566U (en) | Take reation kettle of semicircle arc structure puddler | |
| CN205833171U (en) | A kind of detachable can the reactor of high-efficiency stirring reactant | |
| CN207042487U (en) | A kind of low temperature hydrogenation reactor | |
| CN207899331U (en) | A kind of agitating device | |
| CN204699703U (en) | A kind of polymer stirred autoclave | |
| CN108786684A (en) | A kind of deep-etching reagent reaction kettle |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: No. 228, Mingxin Road, Daqiao Town, Nanhu District, Jiaxing City, Zhejiang Province, 314000 Patentee after: Zhejiang Zhengda New Material Technology Co.,Ltd. Address before: No. 228, Mingxin Road, Daqiao Town, Nanhu District, Jiaxing City, Zhejiang Province, 314000 Patentee before: ZHEJIANG ZHENGDA NEW MATERIALS TECHNOLOGY Co.,Ltd. |