CN207413393U - A kind of silane coupling agent low dose synthesizer - Google Patents
A kind of silane coupling agent low dose synthesizer Download PDFInfo
- Publication number
- CN207413393U CN207413393U CN201721392361.0U CN201721392361U CN207413393U CN 207413393 U CN207413393 U CN 207413393U CN 201721392361 U CN201721392361 U CN 201721392361U CN 207413393 U CN207413393 U CN 207413393U
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- China
- Prior art keywords
- reaction kettle
- upper cover
- coupling agent
- silane coupling
- low dose
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Abstract
The utility model discloses a kind of silane coupling agent low dose synthesizers, including reaction kettle, collection device and upper cover, the collection device is screwed onto the lower end of reaction kettle, the upper surface of the reaction kettle offers screw thread circular groove, the upper cover is screwed onto the upper surface of reaction kettle by screw thread circular groove, the upper surface middle of the upper cover is installed with motor, and the lower surface of the upper cover is rotatablely equipped with bull stick, and the upper end of the bull stick is fixedly connected through upper cover with the output terminal of motor.The utility model is simple in sturcture, ingenious in design, in the low dose of synthesis of silane coupling agent, the step of effectively reducing the instrument used, alleviate manual operation, makes building-up process simple and convenient, effectively alleviates work load.
Description
Technical field
The utility model is related to organic silicon monomer synthesizer technical fields, and being specially that a kind of silane coupling agent is low dose of closes
Into device.
Background technology
Silane coupling agent be it is a kind of in the molecule simultaneously containing there are two types of different chemical property groups organo-silicon compound,
There is energy and the chemically combined reactive group of inanimate matter material and the reactive group combined with organic matter materials chemistry simultaneously in molecule
Group, can be used for being surface-treated；This characteristic of silane coupling agent is applied on fiberglass reinforced plastics earliest, makees glass fibers
The surface conditioning agent of dimension makes mechanical performance, electric property and the anti-aging property of fiberglass be greatly improved, in fiberglass
Importance in industry gains public acceptance already；Now, silane coupling agent is low dose of synthesize when, it is complicated for operation, it is necessary to use
Instrument is various, inconvenient to use, for this purpose, we have proposed a kind of silane coupling agent low dose synthesizers.
Utility model content
The purpose of this utility model is to provide a kind of silane coupling agent low dose synthesizer, to solve above-mentioned background skill
The problem of being proposed in art.
To achieve the above object, the utility model provides following technical solution：A kind of low dose of synthesis dress of silane coupling agent
It puts, including reaction kettle, collection device and upper cover, the collection device is screwed onto the lower end of reaction kettle, the upper table of the reaction kettle
Face offers screw thread circular groove, and the upper cover is screwed onto the upper surface of reaction kettle by screw thread circular groove, in the upper surface of the upper cover
Between be installed with motor, the lower surface of the upper cover is rotatablely equipped with bull stick, and the upper end of the bull stick is through upper cover and electricity
The output terminal of machine is fixedly connected, and the side surface of the bull stick is installed with agitating vane, and the lower surface of the bull stick is equipped with
Temperature detector, the upper surface of the motor are equipped with controller, and the upper surface of the controller is equipped with control switch, and controls
Device processed is electrically connected respectively with motor, temperature detector and control switch, and the upper surface of the upper cover offers gas outlet, it is described go out
The upper end of gas port is socketed with balloon, and reaction kettle inner cavity side surface is equipped with heating unit, and heating unit and controller electricity
Connection, the upper surface of the upper cover offer socket, and the left and right sides surface of the socket offers card slot, in the card slot
Be connected with sealing block, the inner surface of the card slot is installed with the first spring, and the other end of the first spring with it is close
Block block is fixedly connected；
The lower surface of the reaction kettle offers discharge port, and the left surface of the discharge port offers mounting groove, the peace
The left side wall of tankage is installed with electromagnetic coil, and electromagnetic coil is electrically connected with the controller, and clamping is slided in the mounting groove
There is dynamic iron core, the left surface of the dynamic iron core is installed with one end of second spring, and the other end of the second spring is fixed
Mounted on the right surface of electromagnetic coil, the right surface of the dynamic iron core is installed with baffle, the right end of the baffle and discharging
The right surface of mouth fits closely, and the inner cavity upper surface of the collection device is equipped with filter tunnel, the upper table of the filter tunnel
Face is equipped with filter paper, and filter paper is fitted closely with filter tunnel.
Preferably, the lower surface of the reaction kettle is installed with flow-guiding bar, lower end and the filter paper phase of the flow-guiding bar
Connect place, and the lower end of discharge port and the side surface joint of flow-guiding bar.
Preferably, the outboard end upper surface of the sealing block is equipped with landslide.
Compared with prior art, the beneficial effects of the utility model are：The utility model is simple in sturcture, ingenious in design, in silane
During coupling agent low dose synthesis, the step of effectively reducing the instrument used, alleviate manual operation, make building-up process simple
It is convenient, effectively alleviate work load.
Description of the drawings
Fig. 1 is the utility model structure diagram；
Fig. 2 is enlarged diagram at a in Fig. 1；
Fig. 3 is enlarged diagram at b in Fig. 1.
In figure：1st, reaction kettle, 101, screw thread circular groove, 102, flow-guiding bar, 103, discharge port, 104, mounting groove, 105, electromagnetism
Coil, 106, second spring, 107, dynamic iron core, 108, baffle, 2, collection device, 21, filter tunnel, 22, filter paper, 3, on
Lid, 301, gas outlet, 302, socket, 303, card slot, the 304, first spring, 305, sealing block, 4, motor, 5, controller, 6,
Control switch, 7, balloon, 8, temperature detector, 9, heating unit, 10, bull stick, 11, agitating vane.
Specific embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out
It clearly and completely describes, it is clear that the described embodiments are only a part of the embodiments of the utility model rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work
All other embodiments obtained shall fall within the protection scope of the present invention.
It please refers to Fig.1, Fig. 2 and Fig. 3, the utility model provides a kind of silane coupling agent low dose synthesizer, including anti-
Kettle 1, collection device 2 and upper cover 3 are answered, the collection device 2 is screwed onto the lower end of reaction kettle 1, and the upper surface of the reaction kettle 1 is opened
Equipped with screw thread circular groove 101, the upper cover 3 is screwed onto the upper surface of reaction kettle 1 by screw thread circular groove 101, makes upper cover 3 and reaction kettle
1 is tightly connected, and the upper surface middle of the upper cover 3 is installed with motor 4, and the lower surface of the upper cover 3 is rotatablely equipped with
Bull stick 10, the upper end of the bull stick 10 are fixedly connected through upper cover 3 with the output terminal of motor 4, and the side surface of the bull stick 10 is consolidated
Dingan County is equipped with agitating vane 11, and motor 4 rotates, and bull stick 10 is driven to rotate, is stirred by agitating vane 11, the bull stick 10
Lower surface temperature detector 8 is installed, detect the temperature in reaction kettle 1, the upper surface of the motor 4 is equipped with controller 5,
The upper surface of the controller 5 is equipped with control switch 6, and controller 5 switchs respectively with motor 4, temperature detector 8 and control
6 electrical connections, the upper surface of the upper cover 3 offer gas outlet 301, and the upper end of the gas outlet 301 is socketed with balloon 7, balloon 7
Cushioning effect is played to the gas of heating expansion in reaction kettle 1, the 1 inner cavity side surface of reaction kettle is equipped with heating unit 9, and
Heating unit 9 is electrically connected with controller 5, controls heater 9 by controller 5, the inner cavity of reaction kettle 1 is heated, described
The upper surface of upper cover 3 offers socket 302, and the left and right sides surface of the socket 302 offers card slot 303, the card slot
Sealing block 305 is connected in 303, the inner surface of the card slot 303 is installed with the first spring 304, and the first bullet
The other end of spring 304 is fixedly connected with sealing block 305, in gas-guide tube or Dropping feeder insertion socket 302, to reaction kettle
Nitrogen is passed through in 1 or reagent is added dropwise；
The lower surface of the reaction kettle 1 offers discharge port 103, and the left surface of the discharge port 103 offers mounting groove
104, the left side wall of the mounting groove 104 is installed with electromagnetic coil 105, and electromagnetic coil 105 is electrically connected with controller 5,
It is slided in the mounting groove 104 and is connected with dynamic iron core 107, the left surface of the dynamic iron core 107 is installed with second spring 106
One end, the other end of the second spring 106 is fixedly mounted on the right surface of electromagnetic coil 105, the right side of the dynamic iron core 107
Surface is installed with baffle 108, and the right end of the baffle 108 is fitted closely with the right surface of discharge port 103, and controller 5 is controlled
Electromagnetic coil 105 processed is powered, and baffle 108 is made to take in mounting groove 104, and the reagent that reaction finishes in reaction kettle 1 is made to pass through discharging
Mouth 103 flows out, and the inner cavity upper surface of the collection device 2 is equipped with filter tunnel 21, the upper surface peace of the filter tunnel 21
Equipped with filter paper 22, and filter paper 22 is fitted closely with filter tunnel 21, and the reagent that discharge port 103 flows out passes through filter tunnel 21
It filters, is flowed into collection device with filter paper 22.
Specifically, the lower surface of the reaction kettle 1 is installed with flow-guiding bar 102, the lower end of the flow-guiding bar 102 with
22 joint of filter paper, and the lower end of discharge port 103 and the side surface joint of flow-guiding bar 102, facilitate filtering.
Specifically, the outboard end upper surface of the sealing block 305 is equipped with landslide, facilitates gas-guide tube and Dropping feeder
It is inserted into socket 302.
Operation principle：During using the utility model, the tetraethoxysilane being disposed, magnesium and iodine are added in into 1 inner cavity of reaction kettle,
Upper cover 3 is screwed onto by screw thread circular groove 101 on reaction kettle 1, by gas-guide tube by being passed through nitrogen in 302 intercalation reaction kettle 1 of socket
Gas discharges air in reaction kettle 1 by gas outlet 301, then 301 upper end of gas outlet is put on balloon 7, extracts gas-guide tube out, leads to
Crossing the first spring 304 and sealing block 305 seals socket 302, by controlling switch 6 and controller 5 that motor 4 is controlled to rotate,
It is stirred by bull stick 10 and agitating vane 11, by controller 5 heating unit 9 is controlled to heat, examined by temperature detector 8
The temperature in reaction kettle 1 is surveyed, temperature is controlled in 180 degree, then chlorocyclohexane is added dropwise by socket 302, after being added dropwise, then
Temperature is controlled at 120 degree, the reaction was continued, and after completion of the reaction, control electromagnetic coil 105 makes baffle 108 take in mounting groove 104,
The magnesium salts of generation is filtered by filter tunnel 21 and filter paper 22, filtrate is collected in collection device 2, and filtered fluid is steamed four
Ethoxysilane and iodine, obtain the crude product of cyclohexyltriethyloxysilane, then crude product is carried out rectification and purification to get to
Yield 97%, the water white transparency cyclohexyltriethyloxysilane of purity 99.5%.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned exemplary embodiment, and
And in the case of the spirit or essential attributes without departing substantially from the utility model, it can realize that this practicality is new in other specific forms
Type.Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this practicality is new
The scope of type is indicated by the appended claims rather than the foregoing description, it is intended that will fall containing in the equivalent requirements of the claims
All changes in justice and scope are embraced therein.Any reference numeral in claim should not be considered as limitation
Involved claim.
Moreover, it will be appreciated that although this specification is described in terms of embodiments, but not each embodiment is only wrapped
Containing an independent technical solution, this description of the specification is merely for the sake of clarity, and those skilled in the art should
Using specification as an entirety, the technical solutions in each embodiment can also be properly combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (3)
1. a kind of silane coupling agent low dose synthesizer, including reaction kettle（1）, collection device（2）And upper cover（3）, feature
It is：The collection device（2）It is screwed onto reaction kettle（1）Lower end, the reaction kettle（1）Upper surface offer screw thread circular groove
（101）, the upper cover（3）Pass through screw thread circular groove（101）It is screwed onto reaction kettle（1）Upper surface, the upper cover（3）Upper surface
Middle is installed with motor（4）, the upper cover（3）Lower surface be rotatablely equipped with bull stick（10）, the bull stick（10）'s
Upper cover is run through in upper end（3）With motor（4）Output terminal be fixedly connected, the bull stick（10）Side surface be installed with paddle
Piece（11）, the bull stick（10）Lower surface temperature detector is installed（8）, the motor（4）Upper surface control is installed
Device（5）, the controller（5）Upper surface be equipped with control switch（6）, and controller（5）Respectively with motor（4）, temperature inspection
Survey device（8）It is switched with control（6）Electrical connection, the upper cover（3）Upper surface offer gas outlet（301）, the gas outlet
（301）Upper end be socketed with balloon（7）, the reaction kettle（1）Inner cavity side surface is equipped with heating unit（9）, and heating unit
（9）With controller（5）Electrical connection, the upper cover（3）Upper surface offer socket（302）, the socket（302）Left and right two
Side surface offers card slot（303）, the card slot（303）Inside it is connected with sealing block（305）, the card slot（303）'s
Inner surface is installed with the first spring（304）, and the first spring（304）The other end and sealing block（305）It is fixed to connect
It connects；
The reaction kettle（1）Lower surface offer discharge port（103）, the discharge port（103）Left surface offer installation
Slot（104）, the mounting groove（104）Left side wall be installed with electromagnetic coil（105）, and electromagnetic coil（105）With control
Device（5）Electrical connection, the mounting groove（104）Interior slip is connected with dynamic iron core（107）, the dynamic iron core（107）Left surface consolidate
Dingan County is equipped with second spring（106）One end, the second spring（106）The other end be fixedly mounted on electromagnetic coil（105）
Right surface, the dynamic iron core（107）Right surface be installed with baffle（108）, the baffle（108）Right end and discharging
Mouthful（103）Right surface fit closely, the collection device（2）Inner cavity upper surface filter tunnel is installed（21）, the mistake
Filter funnel（21）Upper surface filter paper is installed（22）, and filter paper（22）With filter tunnel（21）It fits closely.
2. a kind of silane coupling agent low dose synthesizer according to claim 1, it is characterised in that：The reaction kettle
（1）Lower surface be installed with flow-guiding bar（102）, the flow-guiding bar（102）Lower end and filter paper（22）Joint, and go out
Material mouth（103）Lower end and flow-guiding bar（102）Side surface joint.
3. a kind of silane coupling agent low dose synthesizer according to claim 1, it is characterised in that：The sealing block
（305）Outboard end upper surface be equipped with landslide.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721392361.0U CN207413393U (en) | 2017-10-26 | 2017-10-26 | A kind of silane coupling agent low dose synthesizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721392361.0U CN207413393U (en) | 2017-10-26 | 2017-10-26 | A kind of silane coupling agent low dose synthesizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207413393U true CN207413393U (en) | 2018-05-29 |
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ID=62309880
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721392361.0U Active CN207413393U (en) | 2017-10-26 | 2017-10-26 | A kind of silane coupling agent low dose synthesizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207413393U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110586016A (en) * | 2019-09-29 | 2019-12-20 | 杨苗珍 | Stirring device for industrial compound reaction |
-
2017
- 2017-10-26 CN CN201721392361.0U patent/CN207413393U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110586016A (en) * | 2019-09-29 | 2019-12-20 | 杨苗珍 | Stirring device for industrial compound reaction |
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