CN207407680U - A kind of electromagnetic suspension water jacketed copper crucible - Google Patents

A kind of electromagnetic suspension water jacketed copper crucible Download PDF

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Publication number
CN207407680U
CN207407680U CN201721426223.XU CN201721426223U CN207407680U CN 207407680 U CN207407680 U CN 207407680U CN 201721426223 U CN201721426223 U CN 201721426223U CN 207407680 U CN207407680 U CN 207407680U
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CN
China
Prior art keywords
crucible
copper
melt
copper mold
electromagnetic suspension
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Expired - Fee Related
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CN201721426223.XU
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Chinese (zh)
Inventor
燕云程
黄蓓
覃乃领
卿培林
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Baise University
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Baise University
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Publication of CN207407680U publication Critical patent/CN207407680U/en
Expired - Fee Related legal-status Critical Current
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Abstract

The utility model discloses a kind of electromagnetic suspension water jacketed copper crucible, it is related to the smelting equipment field of metal or alloy.Including crucible body, induction coil, copper mold, compaction plug and rubber pad, induction coil is arranged on the copper mold intracavitary of crucible body around crucible body top, copper mold and passes through compaction plug and rubber pad is fixed and anti-gas-leak;Melt high-cleanness can be made to avoid melt contamination by the utility model smelting metal or alloy;Electromagnetic suspension water jacketed copper crucible prepares sample or bar can be to avoid sample or the unicity of bar cross section;Sample or bar crystal grain prepared by electromagnetic suspension water jacketed copper crucible is tiny, improves the mechanical property of material.

Description

A kind of electromagnetic suspension water jacketed copper crucible
Technical field
The utility model is related to the smelting equipments of metal or alloy, particularly a kind of electromagnetic suspension water jacketed copper crucible.
Background technology
Usually in atmospheric environment, the melting in ceramic crucible, such melting mode is made pottery for the melting of metal or alloy Porcelain crucible is likely to contaminated melt, and certain difficulty is brought to the purified treatment of later stage melt;Melt may be used also in atmospheric environment Oxidation and the scaling loss of bath composition can be caused, certain difficulty is brought for accurate Composition Control, in view of this, to reduce or keeping away Exempt from melt contamination, developed the following technology.
Light suspension technology can also avoid melt contamination, and light suspension technology is by the use of halogen lamp as heat source, utilizes filament The light that neighbouring concave mirror sends filament focuses on and a bit, and bar melts at this point, then with certain speed mover bar Material, it becomes possible to form the sample of directional solidification, such sample is it is difficult to ensure that the glacing flatness of surfacing and sample.
The principle of electron beam directional solidification is the high energy electron bombardment Surface of Rod Bar of electron gun transmitting, and the kinetic energy of electronics converts For thermal energy, make its small range zone melting in gun alignment, molten metal melt is in the effect of gravity and surface tension It is lower to keep balance, during electron gun is moved to top from the bottom of bar, the Quench copper of melt one-way heat conduction to bottom, So that directionally solidifying from bottom to top for melt, eventually forms sample.During electron beam directional solidification, melt Balance is kept under gravity and surface tension effects, therefore specimen shape is simple, size is small, surface irregularity;Especially electron beam Generation need high vacuum, then the element of high saturated vapour pressure is readily volatilized, be easy to cause ingredient inaccuracy.
Czochralski directional solidifications in water jacketed copper crucible, the principle of the technology is that induction coil generates electromagnetic field, electricity Magnetic field transmission divides the water jacketed copper crucible gap of valve to act on the metal or alloy in copper crucible, and metal or alloy is in electromagnetic field effect Under, generate inductive loop, inductive loop generates Joule heat in metal or alloy makes material melt to form melt, melt equipped with Under the draw bar of seed crystal, the directional solidification growth of real material, this method can realize the free of contamination directional solidification of melt, but It is during solidification, melt is constantly reduced, and the speed of growth is difficult to control.The specimen shape made is simple, surface irregularity.
Electromagnetic cold crucible directional solidification, the fusing principle of the technology are solidifying with the Czochralski orientations in water jacketed copper crucible Solid fusing principle it is identical, but the raw material of Czochralski directional solidifications is first in the crucible, and electromagnetic cold crucible orientation is solidifying Solid raw material for suspension charge bar, when the melt in crucible reaches a certain amount of, allow fuel rod and pumping rod with certain rate It is moved downward than (ensureing that the melt volume in crucible is constant).Under the traction of pumping rod, sample immerses Ga-In liquid billons In, under the pressure cooling effect of liquid alloy, unidirectional heat dissipation is realized, so as to achieve the purpose that directional solidification.It is prepared by this method During sample, there is high-temperature fusant in one end of sample, and the other end has the liquid alloy of cooling, and temperature gradient is larger, is given birth in fair speed When long, melt easily extinguishes, and causes the failure of an experiment, and liquid alloy is likely to pollution sample.The melt that above method obtains More clean, the method for crystal grain refinement is including as follows.
First, deformation process method, this method be using the plastic deformation process of material and the recrystallization of material or phase transformation come Control the size of crystal grain.This method will could be implemented after sample shaping.
2nd, physical field refinement technology, this method directly act on melt using physical field, are controlled during solidification solidifying Gu tissue, crystal grain thinning.The technology includes three aspects to the processing of melt:1) pulsed current annealing;2) magnetic field is handled;3) surpass Sonicated.
3rd, mechanical refinement method, this method are to promote the formation of nucleus in melt using mechanical agitation or effect of vibration, Dendrite is broken, and increases nucleus, so as to achieve the purpose that refinement.
4th, grain refiner method, this method are to add in grain refiner to melt, and melt is different after grain refiner adds in Matter forming core number increases, so as to achieve the purpose that crystal grain thinning.
5th, modifying-refining method, Metamorphism treatment are to add in alterant in the melt, by alterant during solidification The variation of pattern or performance and influence the process of crystal growth.
6th, method for quick cooling, theory and practice research show to be quickly cooled down to improve forming core rate and inhibit atom and expand It dissipates.The raising of forming core rate represents that the nucleus number formed in the unit interval is more;Inhibit atoms permeating, represent the diffusion of atom Rate is slack-off, and crystal grain is grown up slack-off in the unit interval, this means that the crystal grain formed after solidification is tiny.Electromagnetic suspension water-cooled copper Crucible is equipped with copper mold, and for melt under the pressure cooling effect of copper mold, solidification forms the tiny tissue of crystal grain.According to Hall-Petch Formula, the tiny material of crystal grain, mechanical property are more excellent.
The content of the invention
The goal of the invention of the utility model is, in view of the above-mentioned problems, providing a kind of electromagnetic suspension water jacketed copper crucible, to pass through electricity Magnetic suspension water jacketed copper crucible smelting metal or alloy can make melt high-cleanness to avoid melt contamination;Electromagnetic suspension water-cooled copper earthenware Crucible prepares sample or bar can be to avoid sample or the unicity of bar cross section;Sample prepared by electromagnetic suspension water jacketed copper crucible Or bar crystal grain is tiny, improves the mechanical property of material.
In order to achieve the above objectives, technical solution is used by the utility model:Including
Crucible body, shape is cylindrical, and its upper part divides valve including several by the crucible of circle distribution, and crucible divides valve group Into the melt cavity of upward opening;Crucible has valve seam between dividing valve, and the valve seam is filled with heat safe insulating materials;Crucible sheet Body lower part is provided with downwardly open cylindrical, copper die cavity, and cylindrical, copper die cavity lower part is provided with internal thread;Crucible body cylinder Several water cooling through holes for being used to lead to up and down are provided in wall, two adjacent water cooling through hole tops connect and lower end connects respectively Water inlet pipe and outlet pipe;Melt cavity bottom is provided with a melt through hole, melt through hole connection copper mold chamber and melt cavity;
Induction coil is looped around and several divides valve outer surface by the crucible of circle distribution;
Copper mold, in the cylindrical, copper die cavity of crucible body, the semicolumn mould that is fitted closely including two, in copper mold The sample aperture being coaxial therewith is provided with, the sample aperture top is connected with melt through hole, sample aperture lower end face closure;Copper mold Bottom is provided with the anti-blocking chamber being coaxial therewith, and anti-blocking chamber connect with sample aperture by several pumping curved holes, the curved hole of the pumping and The sample aperture lower sides connection;And
Compaction plug, it is cylindrical, it is arranged below copper mold, compaction plug upper surface is provided with and copper mold chamber lower internal thread The external screw thread boss to match is coaxially arranged with inside compaction plug and is used to logical aspirating hole up and down.
Based on said structure:Heat safe insulating materials is filled between valve seam, alternating electromagnetic field can be allowed to enter through valve seam In crucible, raw material and melt are acted on, vortex can be generated in entire crucible cross section to avoid electromagnetic field.Melt through hole is molten Body enters the unique passage of copper mold.Each crucible divides valve all water cooling through holes to cool down, and cooling water is from inlet opening into then from water outlet Hole is flowed out, and crucible forces cooling copper crucible during operation, takes away the heat for passing to copper crucible of melt, avoids copper crucible temperature High or fusing is spent, while water cooling can take away copper mold heat, make sample rapid shaping.When vacuumizing, the gas of sample aperture leads to It crosses and is evacuated curved hole and is pumped.Being evacuated curved hole and anti-blocking chamber can prevent melt to be directly entered the aspirating hole of compaction plug, cause to be evacuated Hole plug;Aspirating hole is connected with air exhauster.
During entire crucible work, raw material is placed in melt cavity, and induction coil generates alternating electromagnetic field and acted on through valve seam In raw material, raw material generates inductive loop, generates Joule heat, and so as to which melt raw material forms melt, melt is in inert gas shielding Micro-positive pressure environment in, under the action of electromagnetic push, melt is in suspended state or is in melt cavity and soft connect melt The state of touching, electromagnetic stirring force are uniform by bath composition.After keeping the temperature a period of time, the air exhauster being connected with aspirating hole starts pumping very Sky, and the power supply of induction coil is closed, stop heating, melt is inhaled into the sample aperture of copper mold by melt through hole in melt cavity In, under the pressure cooling effect of copper mold, solidification forms the tiny sample of tissue, crystal grain.After cooling, compaction plug is unscrewed, is taken out Copper mold, then separated copper mold, takes out sample.
Further, the crucible divides valve top to be wound using insulating tape.
Advantageous effect using above-mentioned further scheme is:After valve seam fills in high temperature insulating material, with insulating cement high Warm insulating materials is enclosed in valve seam, then winds crucible top with insulating tape, can increase the radial strength of crucible.
Further, the crucible body lower face is provided with gasket with the outer faying face of the compaction plug.
Advantageous effect using above-mentioned further scheme is:When can prevent pumping with exhaust blower, crucible body lower face With faying face gas leakage outside compaction plug.
Further, the cross-sectional shape of sample aperture is circular or rectangle.
Advantageous effect using above-mentioned further scheme is:By the sample aperture of different cross section, different cut can be produced The sample in face.
Further, the copper mold outer diameter is identical with the cylindrical, copper die cavity internal diameter, the copper mold length and the copper Die cavity height is identical.
Advantageous effect using above-mentioned further scheme is:Copper mold can combine closely in copper mold intracavitary, and sample aperture side is split Head is not in gap, and sample side wall will not generate redundancy.
Further, the melt cavity bottom is provided with to recessed arc.
Advantageous effect using above-mentioned further scheme is:Melt is formed in bottom to be assembled, and is easily absorbed style hole It is interior.
Due to the adoption of the above technical scheme, the utility model has the advantages that:
1. the utility model electromagnetic suspension water jacketed copper crucible smelting metal or alloy can pass through electromagnetism to avoid melt contamination The melt that the melting of suspension water jacketed copper crucible is formed has high cleanliness factor.
2. the Czochralski in the utility model relatively light suspension method, electron beam directional solidification method and water jacketed copper crucible Bar prepared by directional solidification, cross-sectional shape is single, is approximately cylindrical substantially, and prepared by electromagnetic suspension water jacketed copper crucible Bar can prepare bar of the cross section for circular, rectangle or square etc. according to the shape of copper mold.
3. the Czochralski in the utility model relatively light suspension method, electron beam directional solidification method and water jacketed copper crucible Surface of Rod Bar prepared by directional solidification lacks constraint, the specimen surface out-of-flatness of preparation, and electromagnetic suspension water jacketed copper crucible is molten Body shapes in copper mold, and copper mold has effect of contraction to bath surface, can prepare the bar of surfacing.
4. the melt of the utility model electromagnetic suspension water jacketed copper crucible solidifies formation, shape under the pressure cooling effect of copper mold Into solidified structure it is tiny, excellent in mechanical performance, this is not available for common forging type
Description of the drawings
Fig. 1 is the utility model section view.
Fig. 2 is the utility model crucible body top view.
Fig. 3 is the utility model semicolumn mould front view.
Fig. 4 is the utility model compaction plug sectional view
In attached drawing, 1- crucible bodies, 2- induction coils, 3- copper molds, 4- compaction plugs, 5- rubber pads, 6- insulating tapes, 7- melt Body, 11- crucibles divide valve, 12- melts cavity, 13- copper molds chamber, 14- internal threads, 15- water coolings through hole, 16- melts through hole, 31- half Cylinder mold, 32- sample apertures, the anti-blocking chambers of 33-, 34- are evacuated curved hole, 41- external screw threads boss, 42- aspirating holes.
Specific embodiment
The specific implementation of invention is further illustrated below in conjunction with attached drawing.
As shown in Figure 1, a kind of electromagnetic suspension water jacketed copper crucible, including crucible body 1, induction coil 2, copper mold 3, compaction plug 4th, rubber pad 5 and insulating tape 6, induction coil 2 are arranged on the copper mold chamber 13 of crucible body 1 around 1 top of crucible body, copper mold 3 Interior and pass through compaction plug 4 and rubber pad 5 is fixed and anti-gas-leak, the crucible in crucible body 1 divides 11 top of valve to be twined using insulating tape 6 Around.
As shown in Fig. 2, 1 shape of crucible body is cylindrical, its upper part divides valve 11 including eight valves by the crucible of circle distribution, Crucible divides the melt cavity 12 that valve 11 forms upward opening;Crucible has valve seam between dividing valve 11, and the valve seam is filled with high temperature resistant Insulating materials;1 lower part of crucible body is provided with downwardly open cylindrical, copper die cavity 13, and 13 lower part of cylindrical, copper die cavity is set There is internal thread 14;About eight groups are provided in 1 cylindrical wall of crucible body and is used to logical water cooling through hole 15, adjacent two water cooling through holes 15 tops connect and lower end is connected respectively with the outlet pipe of water inlet pipe;12 bottom of melt cavity is provided with a melt through hole 16, melts Body through hole 16 connects copper mold chamber 13 and melt cavity 12;12 bottom of melt cavity is provided with to recessed arc.
As shown in figure 3, copper mold 3 includes two semicolumn moulds 31 fitted closely, the examination being coaxial therewith is provided in copper mold 3 Sample hole 32,32 top of sample aperture are connected with melt through hole 16, the 32 lower end face closure of sample aperture;3 bottom of copper mold is set There is the anti-blocking chamber 33 being coaxial therewith, anti-blocking chamber 33 is connected with sample aperture 32 by two curved holes 34 of pumping, the curved hole 34 of pumping It is connected with 32 lower sides of sample aperture;3 outer diameter of copper mold is identical with 13 internal diameter of cylindrical, copper die cavity, the copper mold 3 length are identical with 13 height of copper mold chamber;And
Cylindrical such as Fig. 4 compaction plugs, 4 upper surface of compaction plug is provided with and 13 lower internal thread of copper mold chamber, 14 phase The external screw thread boss 41 matched somebody with somebody is coaxially arranged with inside compaction plug 4 and is used to logical aspirating hole 42 up and down.
During work, raw material is placed in melt cavity 12, and induction coil 2 generates alternating electromagnetic field and acts on original through valve seam Material, raw material generate inductive loop, generate Joule heat, and so as to which melt raw material forms melt 7, melt 7 is in inert gas shielding In micro-positive pressure environment, under the action of electromagnetic push, melt 7 is in suspended state or is in soft with melt cavity 12 melt 7 Contact condition, electromagnetic stirring force are uniform by 7 ingredient of melt.After keeping the temperature a period of time, the air exhauster being connected with aspirating hole 42 starts It vacuumizes, and closes the power supply of induction coil 2, stop heating, melt 7 leads to 16 holes by melt and is inhaled into copper in melt cavity 12 In the sample aperture 32 of mould 3, cooling water enters from 15 water inlet of water cooling through hole, and water outlet outflow forces cooling copper mold 3, makes sample The solidification of melt 7 in hole 32 forms the tiny sample of tissue, crystal grain.After cooling, compaction plug 4 is unscrewed, takes out copper mold 3, Ran Houfen Copper mold 3 is opened, takes out sample.
Above description is the detailed description for the preferable possible embodiments of the utility model, but embodiment is not limited to The patent claim of the utility model, the equal variation or modification completed under the technical spirit suggested by all the utility model Change, should all belong to the utility model and cover the scope of the claims.

Claims (6)

1. a kind of electromagnetic suspension water jacketed copper crucible, it is characterised in that:Including
Crucible body, shape is cylindrical, its upper part include it is several divide valve by the crucible of circle distribution, crucible divide valve form to The melt cavity of upper opening;Crucible has valve seam between dividing valve, and the valve seam is filled with heat safe insulating materials;Under crucible body Portion is provided with downwardly open cylindrical, copper die cavity, and cylindrical, copper die cavity lower part is provided with internal thread;In crucible body cylindrical wall Several water cooling through holes for being used to lead to up and down are provided with, two adjacent water cooling through hole tops connect and lower end connects water inlet respectively Pipe and outlet pipe;Melt cavity bottom is provided with a melt through hole, melt through hole connection copper mold chamber and melt cavity;
Induction coil is looped around and several divides valve outer surface by the crucible of circle distribution;
Copper mold, in the cylindrical, copper die cavity of crucible body, the semicolumn mould that is fitted closely including two is set in copper mold There is the sample aperture being coaxial therewith, the sample aperture top is connected with melt through hole, sample aperture lower end face closure;Copper mold bottom Be provided with the anti-blocking chamber being coaxial therewith, anti-blocking chamber connect with sample aperture by several pumping curved holes, it is described be evacuated curved hole with it is described Sample aperture lower sides connect;And
Compaction plug, it is cylindrical, it is arranged below copper mold, compaction plug upper surface is provided with and copper mold chamber lower internal thread phase The external screw thread boss matched somebody with somebody is coaxially arranged with inside compaction plug and is used to logical aspirating hole up and down.
2. a kind of electromagnetic suspension water jacketed copper crucible according to claim 1, it is characterised in that:The crucible divides valve top to adopt It is wound with insulating tape.
3. a kind of electromagnetic suspension water jacketed copper crucible according to claim 1, it is characterised in that:The crucible body lower face Faying face outside the compaction plug is provided with gasket.
4. a kind of electromagnetic suspension water jacketed copper crucible according to claim 1, it is characterised in that:The cross-sectional shape of sample aperture For circular or rectangle.
5. a kind of electromagnetic suspension water jacketed copper crucible according to claim 1, it is characterised in that:The copper mold outer diameter and described Cylindrical, copper die cavity internal diameter is identical, and the copper mold length is identical with the copper mold chamber height.
6. a kind of electromagnetic suspension water jacketed copper crucible according to claim 1, it is characterised in that:The melt cavity bottom is set It is equipped with to recessed arc.
CN201721426223.XU 2017-10-31 2017-10-31 A kind of electromagnetic suspension water jacketed copper crucible Expired - Fee Related CN207407680U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107677126A (en) * 2017-10-31 2018-02-09 百色学院 A kind of electromagnetic suspension water jacketed copper crucible

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107677126A (en) * 2017-10-31 2018-02-09 百色学院 A kind of electromagnetic suspension water jacketed copper crucible
CN107677126B (en) * 2017-10-31 2023-09-19 百色学院 Electromagnetic suspension water-cooled copper crucible

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180525

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