CN207405216U - A kind of vacuum distillation plant of essence calcium continuous production - Google Patents
A kind of vacuum distillation plant of essence calcium continuous production Download PDFInfo
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- CN207405216U CN207405216U CN201721206628.2U CN201721206628U CN207405216U CN 207405216 U CN207405216 U CN 207405216U CN 201721206628 U CN201721206628 U CN 201721206628U CN 207405216 U CN207405216 U CN 207405216U
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- graphite
- distillation
- tower tray
- furnace body
- continuous production
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
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Abstract
The utility model discloses a kind of vacuum distillation plant of smart calcium continuous production, including distillation furnace body, graphite distillation tower tray, electrolytic furnace, condenser, the first vacuum pump being connected with condenser and holding furnace, original fluid container, recycling can；Graphite distillation tower tray is provided outside resistance wire, for heating graphite distillation tower tray；Feed inlet is provided in the middle part of distillation furnace body, electrolytic furnace is connected with feed inlet；Rinse mouth is provided at the top of graphite distillation tower tray, original fluid container is connected with rinse mouth；The upper end of recycling can is connected with the second vacuum pump；Graphite distillation tower tray is made of multiple graphite cakes, and the first from left right side is alternate between adjoining graphite plate sets and form the passage of zigzag, and the graphite cake tilts downwards.The purpose of this utility model is to provide a kind of vacuum distillation plant of smart calcium continuous production, can realize continuous production, reduce production cost.
Description
Technical field
The utility model belongs to non-ferrous metal metallurgy apparatus field, is specially a kind of vacuum distillation of smart calcium continuous production
Device.
Background technology
The existing extraction to calcium alloy product can only be the progress of one stove of a stove, i.e., after the extraction of a stove is completed, will produce
Product and waste residue take out, and add new raw material again.The process cycle of this extracting mode is longer, the variation width of the rate of output of product
Degree is very big, and without continuity, production cost is higher.
Utility model content
The purpose of this utility model be in view of the above problems, provide a kind of vacuum distillation plant of smart calcium continuous production,
It can realize continuous production, reduce production cost.
In order to achieve the above object, the technical solution adopted in the utility model is：Described in distilling furnace body 2, being arranged on
Graphite in distillation furnace body 2 distills tower tray 6, is arranged on what is be connected outside the distillation furnace body 2 with graphite distillation tower tray 6
Electrolytic furnace 1, the condenser 3 for being arranged on 6 upper end of graphite distillation tower tray, the first vacuum pump 7 being connected with the condenser 3 and
It is arranged on the outer holding furnace 4 connected with 6 upper end of graphite distillation tower tray of the distillation furnace body 2, is arranged on the retort
The outer original fluid container 8 connected with 6 top of graphite distillation tower tray of furnace body 2 is arranged on outside the distillation furnace body 2 and the graphite
Distill the recycling can 9 of 6 bottom of tower tray connection；The graphite distillation tower tray 6 is provided outside resistance wire, is steamed for heating the graphite
Evaporate tower tray 6；The middle part of the distillation furnace body 2 is provided with feed inlet, and the electrolytic furnace 1 is connected with the feed inlet；Original fluid container 8
The built-in liquid for being useful for rinsing graphite destilling tower disk 6；The top of the graphite distillation tower tray 6 is provided with rinse mouth, the original
Flow container 8 is connected with the rinse mouth；The upper end of the recycling can 9 is connected with the second vacuum pump 10；The graphite distills tower tray 6
It is made of multiple graphite cakes, the first from left right side is alternate between the adjoining graphite plate sets and form the passage of zigzag, the graphite
Plate tilts downwards.
Further, the bottom for being arranged on the graphite distillation tower tray 6 is further included, and 6 bottom of tower tray is distilled with the graphite
The liquation hearth 5 of portion's connection.
Further, the condenser 3 is use outside as condenser 3 that stainless steel plate liner is graphite.
Further, filter is further included, the condenser 3 is connected by the filter with first vacuum pump 7.
Further, the distillation furnace body 2 is vertical cylinder furnace body.
Further, the stainless steel casing being arranged on outside the distillation furnace body 2 is further included.
Further, the temperature being arranged on the electrolytic furnace 1, graphite distillation tower tray 6 or the condenser 3 is further included
Spend detection device.
Further, further include be arranged on distillation 2 outer wall of furnace body central control unit, the central control unit with
The resistance wire and temperature-detecting device connection, for the fed back values according to the temperature-detecting device, control institute
State the output power of resistance wire.
The beneficial effects of the utility model：The utility model provides a kind of vacuum distillation dress of smart calcium continuous production
It puts, including distillation furnace body, the graphite distillation tower tray being arranged in the distillation furnace body, is arranged on outside the distillation furnace body
The electrolytic furnace that be connected with graphite distillation tower tray, the condenser being arranged at the top of graphite distillation tower tray and the condensation
The vacuum pump and be arranged on the outer holding furnace with being connected at the top of graphite distillation tower tray of the distillation furnace body that device connects, it is described
Graphite distillation tower tray is provided outside resistance wire, and for heating the graphite distillation tower tray, the middle part of the distillation furnace body is set
There is feed inlet, the electrolytic furnace is connected with the feed inlet.
The vacuum distillation plant after it will be electrolysed in calcium alloy addition electrolytic furnace, is distilled by vacuum suck graphite
Tower tray and carry out distillation become calcium steam, into condenser condensation become liquid, be flowed into holding furnace, smart calcium obtained, using true
Empty retort realizes continuous vacuum distillation, continuous charging, reduces vapo(u)rizing temperature, reduce energy consumption, realize continuous life
Production.
The utility model is additionally provided with original fluid container and recycling can, the built-in liquid for being useful for rinsing graphite destilling tower disk of original fluid container
Body, the upper end of recycling can are connected with the second vacuum pump, realize that graphite distills the flushing of tower tray by suction function, facilitate equipment
Maintenance.
The utility model graphite distillation tower tray is made of multiple graphite cakes, the right phase of a first from left between the adjoining graphite plate
Between set and form the passage of zigzag, graphite cake tilts downwards, and the setting of the structure improves the filtering of high-boiling-point impurity
Effect, and facilitate flushing.
Description of the drawings
Fig. 1 is the structure diagram of the utility model.
Label character is expressed as described in figure：1st, electrolytic furnace；2nd, furnace body is distilled；3rd, condenser；4th, holding furnace；5th, liquate
Stove；6th, graphite distillation tower tray；7th, the first vacuum pump；8th, original fluid container；9th, recycling can；10th, the second vacuum pump.
Specific embodiment
In order to enable those skilled in the art to better understand the technical solutions of the present invention, below in conjunction with the accompanying drawings to this reality
Be described in detail with new, the description of this part be only it is exemplary and explanatory, should not be to the scope of protection of the utility model
There is any restriction effect.
As shown in Figure 1, the concrete structure of the utility model is：Including distillation furnace body 2, it is arranged on the distillation furnace body
Graphite in 2 distills tower tray 6, is arranged on the outer electrolytic furnace 1 being connected with graphite distillation tower tray 6 of the distillation furnace body 2, sets
Put the condenser 3 in graphite distillation tower tray 6 upper end, the first vacuum pump 7 for being connected with the condenser 3 and described in being arranged on
The outer holding furnace 4 connect with 6 upper end of graphite distillation tower tray of distillation furnace body 2 is arranged on described distill outside furnace body 2 and institute
It states the original fluid container 8 of 6 top connection of graphite distillation tower tray, be arranged on outside the distillation furnace body 2 and 6 bottom of graphite distillation tower tray
The recycling can 9 of portion's connection；The built-in liquid for being useful for rinsing graphite destilling tower disk 6 of original fluid container 8；Outside the graphite distillation tower tray 6
Resistance wire is provided with, for heating the graphite distillation tower tray 6；The middle part of the distillation furnace body 2 is provided with feed inlet, described
Electrolytic furnace 1 is connected with the feed inlet；The top of graphite distillation tower tray 6 is provided with rinse mouth, the original fluid container 8 with it is described
Rinse mouth connects；The upper end of the recycling can 9 is connected with the second vacuum pump 10；The graphite distillation tower tray 6 is by multiple graphite
Plate forms, and the first from left right side is alternate between the adjoining graphite plate sets and form the passage of zigzag, and the graphite cake is downwards
It tilts.
Preferably, the bottom for being arranged on the graphite distillation tower tray 6 is further included, and 6 bottom of tower tray is distilled with the graphite
The liquation hearth 5 of connection.
Preferably, the condenser 3 is use outside as condenser 3 that stainless steel plate liner is graphite.
Preferably, filter is further included, the condenser 3 is connected by the filter with first vacuum pump 7.
Preferably, the distillation furnace body 2 is vertical cylinder furnace body.
Preferably, the stainless steel casing being arranged on outside the distillation furnace body 2 is further included.
Preferably, the temperature being arranged on the electrolytic furnace 1, graphite distillation tower tray 6 or the condenser 3 is further included
Detection device.
Preferably, the central control unit for being arranged on distillation 2 outer wall of furnace body, the central control unit and institute are further included
Resistance wire and temperature-detecting device connection are stated, for the fed back values according to the temperature-detecting device, described in control
The output power of resistance wire.
After the utility model will be electrolysed in calcium alloy addition electrolytic furnace 1 by liquid contacting methods, pass through vacuum suck graphite
It distills tower tray 6 and carries out distillation and become calcium steam, become liquid into the condensation of condenser 3, be flowed into holding furnace 4, obtain smart calcium,
Using vacuum distillation furnace 2, continuous vacuum distillation, continuous charging are realized, vapo(u)rizing temperature is reduced, reduces energy consumption, realize
Continuous production.
When vacuum distillation plant works, first calcium alloy is added in electrolytic furnace 1 and is electrolysed, then passes through vacuum suck destilling tower
Interior, temperature control is distilled at 600 DEG C -700 DEG C, and liquid calcium becomes calcium steam in destilling tower, is washed by 6 liquid calcium of tower tray
Purification is washed, liquid is condensed into condenser 3, holding furnace 4 is flowed into and obtains smart calcium.
Due to after raw material is distilled, in addition to smart calcium is obtained, also having the impurity such as higher boiling copper, it is necessary to arrange in time
Go out, could not so influence the normal work of graphite distillation tower tray 6.So the vacuum distillation plant, which further includes, is arranged on institute
State the bottom of graphite distillation tower tray 6, and the liquation hearth 5 connected with 6 bottom of graphite distillation tower tray.Most of high-boiling-point impurity
Metal does not vaporize, and is discharged into liquid by the inflow bottom of towe of tower tray 6 liquation hearth 5, condenser 3 passes through filter and vacuum pump phase
Even, armamentarium interface seals, and keeps negative pressure 3000Pa, and the first vacuum pump 7 is connected with the upper end of graphite distillation tower tray 6.
To improve heat transfer efficiency, liquid calcium, the condenser will be faster cooled to from the calcium steam in distillation tower tray 6
3 is use outside as condenser 3 that stainless steel plate liner is graphite.
It distills furnace body 2 and is generally vertical cylinder furnace body.
To improve the structural strength of distillation furnace body 2, the vacuum distillation plant, which further includes, is arranged on the retort stove
Stainless steel casing outside body 2.
Since all parts nearly all have heating unit, and temperature range during work has certain value, to ensure each portion
The operating temperature of part is in the range of normal working temperature, to realize steady production.To monitor a portion of the vacuum distillation plant
The temperature of part, the vacuum distillation plant, which further includes, is arranged on the electrolytic furnace 1, graphite distillation tower tray 6 or the condensation
Temperature-detecting device on device 3.It should be noted that the present invention to the temperature-detecting device and its specific set-up mode not
It is specifically limited, same type of temperature-detecting device can be set on different components, different type can also be set
Temperature-detecting device.
Accurately to control the operating temperature of each component of vacuum distillation plant, the vacuum distillation plant, which further includes, to be arranged on
The central control unit of 2 outer wall of furnace body is distilled, the central control unit is filled with the resistance wire and the temperature detection
Connection is put, for the fed back values according to the temperature-detecting device, controls the output power of the resistance wire.
In conclusion the vacuum distillation plant that the utility model embodiment is provided, by the way that calcium alloy is added in electrolytic furnace
After middle electrolysis, by vacuum suck graphite distill tower tray and carry out distillation become calcium steam, into condenser condensation become liquid,
Holding furnace is flowed into, obtains smart calcium, using vacuum distillation furnace, continuous vacuum distillation, continuous charging is realized, reduces distillation temperature
Degree, reduces energy consumption, realizes continuous production.
It should be noted that herein, term " comprising ", "comprising" or its any other variant are intended to non-row
His property includes, so that process, method, article or equipment including a series of elements not only include those elements, and
And it further includes other elements that are not explicitly listed or further includes as this process, method, article or equipment institute inherently
Element.
Specific case used herein is set forth the principle and embodiment of the utility model, above example
Illustrate to be only intended to help the method and its core concept for understanding the utility model.The above is only the preferred of the utility model
Embodiment, it is noted that due to the finiteness of literal expression, and objectively there are unlimited concrete structure, for this technology
For the those of ordinary skill in field, on the premise of the utility model principle is not departed from, several improvement, retouching can also be made
Or variation, above-mentioned technical characteristic can also be combined in the right way；These improve retouching, variation or combination or not
It is improved that the design of utility model and technical solution are directly applied into other occasions, it is regarded as the protection of the utility model
Scope.
Claims (8)
1. a kind of vacuum distillation plant of essence calcium continuous production, which is characterized in that including distillation furnace body (2), be arranged on institute
State the distillation tower tray of the graphite in distillation furnace body (2) (6), be arranged on the distillation furnace body (2) outside with the graphite destilling tower
The electrolytic furnace (1) of disk (6) connection, the condenser (3) and the condenser (3) for being arranged on described graphite distillation tower tray (6) upper end
Connection the first vacuum pump (7) and be arranged on it is described distillation furnace body (2) outside with the graphite distill tower tray (6) upper end connect
Holding furnace (4), be arranged on the distillation furnace body (2) outside with connected at the top of graphite distillation tower tray (6) original fluid container (8),
It is arranged on the recycling can (9) that the distillation furnace body (2) connects outside with graphite distillation tower tray (6) bottom；In original fluid container (8)
Equipped with for rinsing the liquid of graphite destilling tower disk (6)；The graphite distillation tower tray (6) is provided outside resistance wire, for heating
The graphite distillation tower tray (6)；Be provided with feed inlet in the middle part of distillation furnace body (2), the electrolytic furnace (1) with it is described into
Material mouth connects；Rinse mouth is provided at the top of the graphite distillation tower tray (6), the original fluid container (8) is connected with the rinse mouth；
The upper end of the recycling can (9) is connected with the second vacuum pump (10)；The graphite distillation tower tray (6) is by multiple graphite cake groups
Into the first from left right side is alternate between the adjoining graphite plate sets and form the passage of zigzag, and the graphite cake inclines downwards
Tiltedly.
2. the vacuum distillation plant of a kind of smart calcium continuous production according to claim 1, which is characterized in that further include and set
It puts in the bottom of graphite distillation tower tray (6), and the liquation hearth (5) connected with graphite distillation tower tray (6) bottom.
A kind of 3. vacuum distillation plant of smart calcium continuous production according to claim 2, which is characterized in that the condensation
Device (3) is use outside as condenser (3) that stainless steel plate liner is graphite.
4. the vacuum distillation plant of a kind of smart calcium continuous production according to claim 3, which is characterized in that further included
Filter, the condenser (3) are connected by the filter with first vacuum pump (7).
A kind of 5. vacuum distillation plant of smart calcium continuous production according to claim 4, which is characterized in that the distillation
Furnace body (2) is vertical cylinder furnace body.
6. the vacuum distillation plant of a kind of smart calcium continuous production according to claim 5, which is characterized in that further include and set
Put the stainless steel casing outside in the distillation furnace body (2).
7. the vacuum distillation plant of a kind of smart calcium continuous production according to claim 6, which is characterized in that further include and set
Put the temperature-detecting device on the electrolytic furnace (1), graphite distillation tower tray (6) or the condenser (3).
8. the vacuum distillation plant of a kind of smart calcium continuous production according to claim 7, which is characterized in that further include and set
Put the central control unit in distillation furnace body (2) outer wall, the central control unit and the resistance wire and the temperature
Detection device connects, and for the fed back values according to the temperature-detecting device, controls the output power of the resistance wire.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721206628.2U CN207405216U (en) | 2017-09-19 | 2017-09-19 | A kind of vacuum distillation plant of essence calcium continuous production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721206628.2U CN207405216U (en) | 2017-09-19 | 2017-09-19 | A kind of vacuum distillation plant of essence calcium continuous production |
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| Publication Number | Publication Date |
|---|---|
| CN207405216U true CN207405216U (en) | 2018-05-25 |
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ID=62405997
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721206628.2U Active CN207405216U (en) | 2017-09-19 | 2017-09-19 | A kind of vacuum distillation plant of essence calcium continuous production |
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| Country | Link |
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| CN (1) | CN207405216U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111218559A (en) * | 2018-11-26 | 2020-06-02 | 广东先导稀材股份有限公司 | Melt evaporation device and method |
| CN113265550A (en) * | 2021-04-26 | 2021-08-17 | 鄂尔多斯市欣欣宸瑞高纯材料有限公司 | Vacuum distillation and forming device and method for extracting calcium metal from carbide slag |
-
2017
- 2017-09-19 CN CN201721206628.2U patent/CN207405216U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111218559A (en) * | 2018-11-26 | 2020-06-02 | 广东先导稀材股份有限公司 | Melt evaporation device and method |
| CN113265550A (en) * | 2021-04-26 | 2021-08-17 | 鄂尔多斯市欣欣宸瑞高纯材料有限公司 | Vacuum distillation and forming device and method for extracting calcium metal from carbide slag |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200701 Address after: 410600 212, 2 / F, Zhongchuang building, Sany industrial city, No.1 Sany Road, economic and Technological Development Zone, Changsha City, Hunan Province Patentee after: HUNAN JINMA METALLURGICAL TECHNOLOGY DEVELOPMENT Co.,Ltd. Address before: 425302 Daoxian County, Yongzhou, Hunan, Xian Zi Zhen (the original Yuejin Machinery Factory) Patentee before: HUNAN JINMA YOULIN ENVIRONMENTAL PROTECTION SCIENCE AND TECHNOLOGY Co.,Ltd. |