CN207347173U - A kind of graphene prepares oxidation pond - Google Patents

A kind of graphene prepares oxidation pond Download PDF

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Publication number
CN207347173U
CN207347173U CN201721367204.4U CN201721367204U CN207347173U CN 207347173 U CN207347173 U CN 207347173U CN 201721367204 U CN201721367204 U CN 201721367204U CN 207347173 U CN207347173 U CN 207347173U
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CN
China
Prior art keywords
main body
head cover
oxidation pond
decelerating motor
heater
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201721367204.4U
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Chinese (zh)
Inventor
朱洋
邵蓉
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Nanjing Xuyurui Material Technology Co Ltd
Original Assignee
Nanjing Xuyurui Material Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
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Priority to CN201721367204.4U priority Critical patent/CN207347173U/en
Application granted granted Critical
Publication of CN207347173U publication Critical patent/CN207347173U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of graphene to prepare oxidation pond, including main body and head cover, the head cover is installed at the upper port of main body, the upper surface of the head cover is installed with decelerating motor, the decelerating motor is rotatably connected to shaft straight down, the top of the shaft is installed with stirring fan, the head cover offers feed inlet and air outlet pipe respectively in the both sides positioned at decelerating motor, the inner wall of the main body is equipped with erosion resistant coating, the side wall of the main body embeds installation having heaters, the main body is provided with temperature sensor being embedded positioned at the top of heater, the bottom of the main body is provided with cooling block, cooling tube is provided with the inner cavity of the cooling block.This utility model is skillfully constructed, the temperature of insulation can be freely adjusted, while the reaction solution in oxidation pond can also be cooled down, and the irritative gas produced in preparation process can be sent in the exhaust treatment system of outside, purified treatment is carried out, and corrosion resistance is good.

Description

A kind of graphene prepares oxidation pond
Technical field
Graphene processing correlative technology field is the utility model is related to, is specially that a kind of graphene prepares oxidation pond.
Background technology
A kind of new carbon material of the graphene as superior performance, widely applies to electronic device field, is making During making graphene, typically aoxidized by graphite with strong acid, then through reduction, so that graphene is obtained, in the process of preparation It is middle to need to carry out it insulation reaction in multiple stages, and cooling, it is therefore desirable to design a kind of graphene and prepare oxidation pond.
Utility model content
The purpose of this utility model is to provide a kind of graphene to prepare oxidation pond, to solve to propose in above-mentioned background technology The problem of.
To achieve the above object, the utility model provides following technical solution:A kind of graphene prepares oxidation pond, including master Body and head cover, the head cover are installed at the upper port of main body, and the upper surface of the head cover is installed with decelerating motor, described Decelerating motor is rotatably connected to shaft straight down, and the top of the shaft is installed with stirring fan, and the head cover is in place Feed inlet and air outlet pipe are offered respectively in the both sides of decelerating motor, and the inner wall of the main body is equipped with erosion resistant coating, the main body Side wall embed installation having heaters, the main body is provided with temperature sensor being embedded positioned at the top of heater, the master The bottom of body is provided with cooling block, and cooling tube is provided with the inner cavity of the cooling block, is set in the bottom side of the wall of the main body There are water inlet and water outlet, connected between the water inlet and water outlet by cooling tube, the bottom of the main body is provided with Two discharge ports, embed on the lateral wall of the main body and are provided with control panel, and the decelerating motor and heater are and chain of command Plate is electrically connected, and the exterior bottom of the main body is fixedly welded with support feet.
Preferably, the erosion resistant coating uses polytetrafluoroethylene (PTFE) material.
Preferably, the middle-end of the main body is provided with the first discharge port.
Preferably, the cooling tube is connected with external cooling device.
Preferably, the heater is resistance heater or electromagnetic heater.
Compared with prior art, the beneficial effects of the utility model are:The design of this utility model is reasonable, is skillfully constructed, energy It is enough free to adjust the temperature of insulation reaction, while the reaction solution in oxidation pond can also be cooled down, and can will be The irritative gas produced in preparation process is sent in the exhaust treatment system of outside, is carried out purified treatment, environment is not made Into pollution, and corrosion resistance is good, and detects the actual temp in oxidation pond in real time, is worked accordingly easy to staff Adjustment.
Brief description of the drawings
Fig. 1 is the utility model structure diagram;
Fig. 2 is the utility model main body sectional view.
In figure:1 main body, 2 head covers, 3 decelerating motors, 4 stirring fans, 5 shafts, 6 feed inlets, 7 air outlet pipes, 8 control panels, 9 Support feet, 10 heaters, 11 cooling blocks, 12 cooling tubes, 13 water outlets, 14 water inlets, 15 first discharge ports, 16 second dischargings Mouth, 17 temperature sensors, 18 erosion resistant coatings.
Embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work All other embodiments obtained, shall fall within the protection scope of the present invention.
In the description of the utility model, it is necessary to explanation, the side of the instruction such as term " vertical ", " on ", " under ", " level " Either position relationship is based on orientation shown in the drawings or position relationship for position, is for only for ease of this practicality of description and simplification is retouched State, rather than instruction either implies that signified device or element must have specific orientation, with specific azimuth configuration with Operation, therefore it is not intended that limitation to the utility model.In addition, " first ", " second ", " the 3rd ", " the 4th " are only used for Purpose is described, and it is not intended that instruction or hint relative importance.
In the description of the utility model, it is also necessary to which explanation, " sets unless otherwise clear and definite regulation and limitation, term Put ", " installation ", " connected ", " connection " should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, Or be integrally connected, can mechanically connect or be electrically connected, can be directly connected to or by middle matchmaker It is situated between and is connected, can is the connection inside two elements.For the ordinary skill in the art, can be as the case may be Understand concrete meaning of the above-mentioned term in the utility model.
- 2 are please referred to Fig.1, the utility model provides a kind of technical solution:A kind of graphene prepares oxidation pond, including main body 1 With head cover 2, the head cover 2 is installed at the upper port of main body 1, and the middle-end of the main body 1 is provided with the first discharge port 15, is easy to By outside the graphene oxide suspension discharge main body 1 for reacting generation, the upper surface of the head cover 2 is installed with decelerating motor 3, The decelerating motor 3 is rotatably connected to shaft 5 straight down, and the top of the shaft 5 is installed with stirring fan 4 so that Powdered graphite can offer feed inlet respectively with the sufficient haptoreaction of strong acid, the head cover 2 positioned at the both sides of decelerating motor 3 6 and air outlet pipe 7, the inner wall of the main body 1 is equipped with erosion resistant coating 18, and the erosion resistant coating 18 uses polytetrafluoroethylene (PTFE) material, resistance to strong Acid corrosion, resistance, the side wall of the main body 1 embed installation having heaters 10, and the heater 10 is resistance heater or electricity Magnetic heater, is heated using electrically heated mode, and easy to control and adjust, the main body 1 is positioned at the upper of heater 10 Side is embedded to be provided with temperature sensor 17, and the moment detects the reaction temperature of 1 reaction mixture of main body, works to insulation reaction Great convenience is brought, the bottom of the main body 1 is provided with cooling block 11, cooling tube is provided with the inner cavity of the cooling block 11 12, the cooling tube 12 is connected with external cooling device, easy to carry out heat exchange with the external world, accelerates reaction readily cooling speed Rate, is provided with water inlet 14 and water outlet 13 in the bottom side of the wall of the main body 1, leads between the water inlet 14 and water outlet 13 Supercooling pipe 12 connects, and the bottom of the main body 1 is provided with the second discharge port 16, and installation is embedded on the lateral wall of the main body 1 There is control panel 8, the decelerating motor 3 and heater 10 are electrically connected with control panel 8, and the exterior bottom of the main body 1 is consolidated Surely support feet 9 is welded with, the design of this utility model is reasonable, is skillfully constructed, can freely adjust the temperature of insulation reaction, at the same time Reaction solution in oxidation pond can also be cooled down, and the irritative gas produced in preparation process can be sent to In exterior exhaust treatment system, purified treatment is carried out, environment is not polluted, while corrosion resistance is good, and detect in real time Specific temperature in oxidation pond, corresponding work adjustment is carried out easy to staff.
Operation principle:Reactant is imported in main body 1 successively by feed inlet 6, decelerating motor is controlled by control panel 8 3 and heater 10, the reactant in main body 1 is heated, stirs reaction so that powdered graphite easily fully connects with strong acid Reaction is touched, and the irritative gas produced in reaction process is imported into the exhaust treatment system of outside by air outlet pipe 7, no The working environment of surrounding is polluted, and 17 moment of temperature sensor detects the temperature of reaction mixture, easy to work Personnel carry out work adjustment, and can be connected by cooling tube 12 with exterior cooling system, to the mixture after reaction into Row cools, and improves its cooling effectiveness, substantially reduces the manufacturing cycle of graphene.
While there has been shown and described that the embodiment of the utility model, for the ordinary skill in the art, It is appreciated that these embodiments can be carried out with a variety of changes in the case where not departing from the principle of the utility model and spirit, repaiied Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.

Claims (5)

1. a kind of graphene prepares oxidation pond, including main body(1)And head cover(2), it is characterised in that:The head cover(2)It is installed on Main body(1)Upper port at, the head cover(2)Upper surface be installed with decelerating motor(3), the decelerating motor(3)Turn The dynamic shaft being connected with straight down(5), the shaft(5)Top be installed with stirring fan(4), the head cover(2) Positioned at decelerating motor(3)Both sides offer feed inlet respectively(6)And air outlet pipe(7), the main body(1)Inner wall be equipped with it is anti- Rotten layer(18), the main body(1)Side wall embed installation having heaters(10), the main body(1)Positioned at heater(10)'s Top, which embeds, is provided with temperature sensor(17), the main body(1)Bottom be provided with cooling block(11), the cooling block(11) Inner cavity in be provided with cooling tube(12), the main body(1)Bottom side of the wall on be provided with water inlet(14)And water outlet(13), The water inlet(14)With water outlet(13)Between pass through cooling tube(12)Connection, the main body(1)Bottom be provided with second Discharge port(16), the main body(1)Lateral wall on embed control panel is installed(8), the decelerating motor(3)And heater (10)And control panel(8)It is electrically connected, the main body(1)Exterior bottom be fixedly welded with support feet(9).
2. a kind of graphene according to claim 1 prepares oxidation pond, it is characterised in that:The erosion resistant coating(18)Using poly- Tetrafluoroethene material.
3. a kind of graphene according to claim 1 prepares oxidation pond, it is characterised in that:The main body(1)Middle-end set It is equipped with the first discharge port(15).
4. a kind of graphene according to claim 1 prepares oxidation pond, it is characterised in that:The cooling tube(12)With it is external Cooling device connects.
5. a kind of graphene according to claim 1 prepares oxidation pond, it is characterised in that:The heater(10)For resistance Heater or electromagnetic heater.
CN201721367204.4U 2017-10-23 2017-10-23 A kind of graphene prepares oxidation pond Expired - Fee Related CN207347173U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721367204.4U CN207347173U (en) 2017-10-23 2017-10-23 A kind of graphene prepares oxidation pond

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721367204.4U CN207347173U (en) 2017-10-23 2017-10-23 A kind of graphene prepares oxidation pond

Publications (1)

Publication Number Publication Date
CN207347173U true CN207347173U (en) 2018-05-11

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108793132A (en) * 2018-07-28 2018-11-13 赣州市兴顺辉科技有限公司 It is a kind of can be to graphene preparation oxidation pond that irritant gas is handled

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108793132A (en) * 2018-07-28 2018-11-13 赣州市兴顺辉科技有限公司 It is a kind of can be to graphene preparation oxidation pond that irritant gas is handled

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180511

Termination date: 20181023

CF01 Termination of patent right due to non-payment of annual fee