A kind of three barrels of reaction kettles
Technical field
A kind of chemical reaction container is the utility model is related to, more specifically, it relates to a kind of three barrels of reaction kettles.
Background technology
Reaction kettle is the container of chemical reaction, by the structure design and parameter configuration to container, realizes technological requirement
Heating, evaporation, cooling and low high speed mixture function.Reaction kettle is widely used in oil, chemical industry, rubber, pesticide, fuel, doctor
The fields such as medicine, food.
At present, notification number is that the Chinese utility model patent of CN205700483U discloses a kind of porous media catalytic reaction
Twin-tub reaction kettle, it include reaction kettle body, be used to support the reaction kettle stent of reaction kettle, to be arranged on reaction kettle intrinsic
Reaction kettle sleeve, the spherical porous medium and blender being positioned in reaction kettle sleeve;Blender includes servomotor, agitating shaft
And agitating paddle;Agitating paddle is located in reaction kettle sleeve.Reaction mass is entered in reaction kettle sleeve by feed pipe, and and reaction kettle
Spherical porous media contact in sleeve accelerates reaction, as the material in feed pipe constantly enters in reaction kettle sleeve, reaction
Flowed into after material spill-over in kettle sleeve and the second secondary response is carried out in autoclave body, discharged after completion of the reaction from discharge nozzle.
But the feed inlet of above-mentioned twin-tub reaction kettle is located above reaction kettle sleeve, reactive material flows into reaction kettle set from top
In cylinder, overflowed after the reactant in reaction kettle sleeve is full of, just flow into unreacted material because of reaction kettle from feed inlet at this time
Sleeve spill-over and can not all flow into reaction kettle sleeve, a part can overflow into reaction kettle body together with the material of spilling
In, so as to the reaction speed between reactive material can not be made slow, cause reaction efficiency low with spherical porous media contact.
Utility model content
In view of the deficienciess of the prior art, the utility model lies in that a kind of three barrels of reaction kettles are provided, having makes ball-type more
Hole medium comes into full contact with more materials and improves the effect of reaction efficiency.
To achieve the above object, the utility model provides following technical solution:A kind of three barrels of reaction kettles, including autoclave body,
It is in the blender and setting being coaxially disposed to be placed on the chuck on the outside of autoclave body, the sleeve being fixedly connected on inside autoclave body and sleeve
Feed pipe at the top of autoclave body, the autoclave body bottom are equipped with the discharge nozzle tilted down, and the feed pipe at least two is described
Spherical porous medium is equipped with sleeve, guide cylinder is provided with the sleeve, the guide cylinder inner bottom is leaned on sleeve inner
One end connection of nearly bottom, the guide cylinder upper end are higher than the upper end of sleeve, and described feed pipe one end is equipped with feed inlet, it is described into
Material mouth is located above guide cylinder, and the blender is placed in guide cylinder.
By using above-mentioned technical proposal, when material is flowed into guide cylinder from feed pipe, then from guide cylinder inner bottom stream
To sleeve inner bottom, because of upper end of the guide cylinder upper end higher than sleeve, when material is overflowed because of overfill in reaction sleeve, guide cylinder
Do not filled by material also, material is flowed into sleeve inner bottom from guide cylinder, and sleeve upper end is flowed to from sleeve inner bottom
And overflow, make more materials and spherical porous media contact, accelerate reaction speed, the reaction efficiency of raising.
The utility model is further arranged to:The guide cylinder both ends open and with sleeve in being coaxially disposed, the guiding
Gap is left with sleeve inner bottom in cylinder bottom.
By using above-mentioned technical proposal, material in guide cylinder can be through from the gap location stream between the good sleeve of guide cylinder
Enter in sleeve, make guiding barrel structure simpler, manufacture is more convenient.
The utility model is further arranged to:The blender includes being arranged at motor, one end and the motor at the top of autoclave body
The agitating shaft of main shaft connection and the agitating vane for being fixedly connected on agitating shaft, the agitating vane are spiral to stir rotational axis direction
Downwards.
By using above-mentioned technical proposal, when agitating paddle is rotated with agitating shaft, agitating paddle will make in reaction sleeve
Material is subject to upward power, and material overall flow direction is downward, and agitation material makes material relative flow, makes what material mixed
More fully, the reaction speed of quickening.
The utility model is further arranged to:The sleeve bottom is equipped with the convex block of cone, and the convex block is in sleeve
It is coaxially disposed.
By using above-mentioned technical proposal, the conical surface contact backward current of the material to flow downward and convex block to guide cylinder and
Gap between sleeve bottom end inner wall, makes the outflow guide cylinder that material is orderly, has opened the effect of water conservancy diversion.
The utility model is further arranged to:The sleeve bottom is equipped with opening, and the sleeve bottom is equipped with to open and close and is open
Inner cover, the inner cover and convex block are in being fixedly connected, and the inner cover lower end is fixedly connected with connecting rod, and the connecting rod lower end passes through kettle
Body bottom and with autoclave body in being slidably connected.
By using above-mentioned technical proposal, after reaction, inner cover can be dismantled down by connecting rod outside reaction kettle
Come, inner cover can be opened and draw off the material in sleeve, flow in autoclave body from opening, then drawn off from discharge nozzle, easy-unloading.
The utility model is further arranged to:The inner cover is equipped with screw thread in cylinder and side wall, the opening for it is interior
Cover the threaded hole being threadedly coupled.
By using above-mentioned technical proposal, inner cover can be disassembled by rotating inner cover, that is, reach the purpose of sealing
Removed and installed again easy to inner cover.
The utility model is further arranged to:The connecting rod bottom is equipped with turntable.
By using above-mentioned technical proposal, more labour-saving pivot link, make inner cover dismounting more laborsaving.
The utility model is further arranged to:The spherical porous medium is arranged in guide cylinder, is leaned in the guide cylinder
One end of nearly bottom is fixedly connected with filter screen, and the filter screen mesh is more than spherical porous medium.
By using above-mentioned technical proposal, in order to avoid spherical porous medium is drawn off from opening.
The utility model is further arranged to:The guide cylinder upper end is equipped with pull rod, the pull rod away from guide cylinder one
End is fixedly connected at the top of autoclave body.
By using above-mentioned technical proposal, guide cylinder is fixedly connected at the top of autoclave body, will not interfere with the flowing of material.
In conclusion the utility model has the advantages that:
One:More materials is more come into full contact with spherical porous medium, make material reaction more abundant, accelerate
Reaction speed, improves reaction efficiency;
Secondly:Inner cover dismounting is more convenient laborsaving, makes discharging more convenient, and operation is simpler.
Brief description of the drawings
Fig. 1 is the stereogram of the present embodiment;
Fig. 2 is the profile that the present embodiment is used to show internal structure.
Reference numeral:1st, autoclave body;11st, feed pipe;111st, feed inlet;12nd, discharge nozzle;2nd, chuck;21st, water inlet;22nd, go out
The mouth of a river;3rd, stent;4th, blender;41st, motor;42nd, agitating shaft;43rd, agitating vane;5th, sleeve;51st, it is open;52nd, convex block;53、
Connecting rod;54th, turntable;55th, inner cover;56th, connecting rod;6th, guide cylinder;61st, filter screen;62nd, pull rod.
Embodiment
The utility model is described in further detail below in conjunction with attached drawing.
A kind of three barrels of reaction kettles, as shown in Figure 1, including autoclave body 1, being used to support the stent 3 of autoclave body 1 and being placed on autoclave body 1
The chuck 2 in outside, wherein stent 3 are fixedly connected on the lower section of chuck 2, and 2 lower end of chuck is equipped with water inlet 21, and the upper end of chuck 2 is set
There is water outlet 22, by the water flowing into chuck 2 of water inlet 21, the temperature inside temperature indirect control autoclave body 1 by controlling water.
As shown in Fig. 2, reaction kettle is further included with autoclave body 1 is in the sleeve 5 being coaxially disposed, is arranged at two, the top of autoclave body 1
Feed pipe 11 and it is placed in sleeve 5 and the guide cylinder 6 of both ends open 51, use is circumferentially between its middle sleeve 5 and autoclave body 1
In the connecting rod 56 of fixes sleeve 5;For guide cylinder 6 with sleeve 5 in being coaxially disposed, 6 upper end of guide cylinder is circumferentially fixed to be connected with four
Pull rod 62,62 upper end of pull rod are fixedly connected on 6 upper end inner wall of autoclave body, are left between 5 inner bottom surface of 6 bottom of guide cylinder and sleeve
Gap, 6 top of guide cylinder are higher than the top of sleeve 5, spherical porous medium are housed in guide cylinder 6;6 lower end of guide cylinder is internally provided with
Filter screen 61, the mesh on filter screen 61 is less than spherical porous medium, to stop spherical porous medium, protects spherical porous medium
Stay in guide cylinder 6.
11 one end of feed pipe is equipped with feed inlet 111, and feed pipe 11 is bent close to 111 one end of feed inlet into guide cylinder 6;
During charging, material flows into reaction kettle from feed pipe 11, is flowed downwardly into from feed inlet 111 in guide cylinder 6, then from 6 bottom of guide cylinder
Gap between 5 bottom of sleeve is flowed in sleeve 5, because 6 top of guide cylinder is higher than the top of sleeve 5, so that when thing in sleeve 5
Material because overfill overflows when, guide cylinder 6 is not filled also by material, and material is from inflow 5 inner bottom of sleeve of guide cylinder 6, and from set
5 inner bottoms of cylinder are flowed to 5 upper end of sleeve and then overflowed into inside autoclave body 1, make material as much as possible and spherical porous Jie
Matter comes into full contact with, and the reaction speed of quickening, improves reaction efficiency.
In order to make the orderly flowing of the material in guide cylinder 6, the convex block 52 of taper is equipped with 5 bottom of sleeve, opens guiding
The effect of shunting.After the completion of reaction, in order to which the material in sleeve 5 can be discharged, opening 51 is equipped with 5 bottom of sleeve, and
5 bottom thread of sleeve is connected with the inner cover 55 for opening and closing opening 51, and the upper end of inner cover 55 is fixedly connected on the bottom of convex block 52, both
In being integrally formed.55 lower end of inner cover is fixedly connected with connecting rod 53, and 53 lower end of connecting rod passes through 1 bottom of autoclave body;During discharging, pivot link
53 drive inner covers 55 rotate, and inner cover 55 are dismantled from 5 bottom of sleeve, so that opening 51 is opened, the material in sleeve 5 flows to kettle
In body 1, flowed out afterwards from discharge nozzle 12;It is more laborsaving during in order to rotate connecting rod 53, in the one end of connecting rod 53 away from inner cover 55
Equipped with turntable 54.
In order to make to be come into full contact between material, reaction kettle is further included with autoclave body 1 in the blender 4 being coaxially disposed, stirring
Device 4 includes being fixedly connected on the motor 41 at the top of autoclave body 1, one end and the agitating shaft 42 for being connected the connection of 41 main shaft of motor and fixed company
The agitating vane 43 of agitating shaft 42 is connected to, wherein agitating shaft 42 is arranged in guide cylinder 6, and agitating vane 43 and agitating shaft 42 are neither
Contacted with filter screen 61.Agitating vane 43 is with 42 rotation direction downward spiral of agitating shaft, when agitating vane 43 is with agitating shaft 42
During rotation, agitating vane 43 will make the material in sleeve 5 be subject to upward power, and material totally flows to from top to bottom, stir thing
Material makes material form relative flow, material is mixed more abundant, the reaction speed of quickening.
Specific working mode:Convey different materials from two feed pipes 11 to enter in guide cylinder 6, both are stirred
Two kinds of materials of effect that blade 43 stirs mix and start to react, and with the spherical porous media contact in guide cylinder 6 to add
Speed reaction.Material is set to form relative flow in guide cylinder 9 because agitating vane 43 rotates, material and spherical porous media contact are more
Add fully.Material is subject to the effect of convex block 52, to 5 both sides olderly flowage of sleeve, and passes through 5 bottom of 6 lower end of guide cylinder and sleeve
Gap outflow guide cylinder 6 between inner wall, into sleeve 5;Because 6 upper end of guide cylinder is higher than the upper end of sleeve 5, when in sleeve 5
Material because overfill overflow when, guide cylinder 6 is not filled also by material;After the completion of reaction fully, rotating turntable 54 makes 53 turns of connecting rod
Dynamic, connecting rod 53 drives inner cover 55 to rotate, and inner cover 55 is dismantled from 5 bottom of sleeve, so that opening opening 51 makes material in sleeve 5
Flow in autoclave body 1, flowed out afterwards from discharge nozzle 12.
This specific embodiment is only explanation to the utility model, it is not the limitation to the utility model, ability
Field technique personnel as needed can make the present embodiment the modification of no creative contribution after this specification is read, but
As long as all protected in the right of the utility model be subject to Patent Law.