CN207324765U - A kind of solid-liquid hybrid reactor - Google Patents
A kind of solid-liquid hybrid reactor Download PDFInfo
- Publication number
- CN207324765U CN207324765U CN201720565294.1U CN201720565294U CN207324765U CN 207324765 U CN207324765 U CN 207324765U CN 201720565294 U CN201720565294 U CN 201720565294U CN 207324765 U CN207324765 U CN 207324765U
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- catalyst
- solid
- solids
- barrel
- reaction kettle
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Abstract
The utility model discloses a kind of solid-liquid hybrid reactor, including cooling jacket, reaction kettle body, catalyst chuck and solids barrel, the reaction kettle body upper end is welded with solids barrel, motor is installed at the top of the solids barrel, the shaft of motor connects rotation axis by shaft coupling, and rotation axis is vertically arranged in solids barrel；The solids barrel bottom is threadedly coupled end of thread capping；The solids barrel bottom inner portion is welded with loading plate, some screen holes are evenly equipped with loading plate, it is described, filter screen is installed on solids barrel side wall on the upside of loading plate, improve the dissolution velocity of solid material, avoid the occurrence of the phenomenon of precipitated and separated, undissolvable large granular materials are screened out by filter screen, then pass through screen holes and fall into storage slag chamber, realize the abundant dissolving of solid material, residue easy to collect, avoid residue fall into reaction after feed liquid in influence product quality, improve the efficiency and effect of solid-liquid hybrid reaction.
Description
Technical field
Technical field of chemical is the utility model is related to, is specifically a kind of solid-liquid hybrid reactor.
Background technology
Chemical reaction kettle is commonly used reaction unit in chemical industry production, be typically provided with reaction kettle agitating shaft and
Agitating paddle, is rotated by agitating shaft and drives agitating paddle to be stirred mixing to material, make material in the state of uniformly mixed into
Row reaction.But usually common chemical reaction kettle only possesses an agitating shaft, leans on the material of proximal wall or bottom cannot in autoclave body
It is stirred paddle to involve, causes material to mix non-uniform situation and occur, prevent material from fully being reacted.Especially solids
When material is reacted with liquid feed liquid, often due to solid material particle is too big, cause short time solid material and liquid feed liquid
It is difficult to fully dissolving reaction；And the impurity not reacted in solid material will be blended in feed liquid, seriously affect product
Quality；When adding catalyst quickening reaction, catalyst is added in reaction kettle, and after reaction, catalyst may be with feed liquid one
With discharge, product quality is influenced, and catalyst is difficult to separate from feed liquid, adds the complexity of chemical reaction.
Utility model content
It is proposed in the above background technology to solve the purpose of this utility model is to provide a kind of solid-liquid hybrid reactor
Problem.
To achieve the above object, the utility model provides following technical solution：
A kind of solid-liquid hybrid reactor, including cooling jacket, reaction kettle body, catalyst chuck and solids barrel, institute
State reaction kettle body upper end and be welded with solids barrel, motor is installed at the top of the solids barrel, the shaft of motor passes through
Shaft coupling connects rotation axis, and rotation axis is vertically arranged in solids barrel；The solids barrel bottom is threadedly coupled screw thread
End seal lid；The solids barrel bottom inner portion is welded with loading plate, and some screen holes are evenly equipped with loading plate, described, carrying
Filter screen is installed on the solids barrel side wall on the upside of plate, Disintegrating knife is installed in the rotation axis above the loading plate；
The rotation axis bottom sequentially passes through loading plate and connects dispersion impeller with the upper through hole of end of thread capping, and dispersion impeller covers it with the end of thread
Between rotation axis on be welded with agitating vane；Catalyst folder is fixedly connected with the outside of the intrinsic solids barrel of reaction kettle
Set, the catalyst chuck upper end connect catalyst adding tube, some water conservancy diversion through holes, water conservancy diversion are equipped with the outside of the catalyst chuck
The aperture of through hole is less than the particle diameter of catalyst in catalyst storage chamber；The reaction kettle body upper end is welded with offgas outlet and liquid
Feed liquid adding tube.
As further program of the utility model：Solids barrel side connection solid above the reaction kettle body
Material adding tube.
As further program of the utility model：The internal thread of the end of thread capping inner wall and solids barrel bottom
The external screw thread connection of the mouth of pipe.
As further program of the utility model：Enclosed in solids barrel between loading plate and the end of thread capping
Into storage slag chamber.
As further program of the utility model：The aperture of the filter screen is less than the aperture of screen holes.
As further program of the utility model：The dispersion impeller is arranged on the top of discharge nozzle, and discharge nozzle is welded on
The bottom of reaction kettle body.
As further program of the utility model：Catalyst storage chamber, catalyst storage chamber are set in the catalyst chuck
Connected by through hole on filter screen with solids barrel internal cavity.
As further program of the utility model：Some water conservancy diversion through holes are equipped with the outside of the catalyst chuck, water conservancy diversion leads to
The aperture in hole is less than the particle diameter of catalyst in catalyst storage chamber.
As further program of the utility model：The reaction kettle body exterior is equipped with cooling jacket, under cooling jacket
End connection cold water inlet pipe, cooling jacket upper end connection cold water outlet pipe, the cooling jacket outside are welded with supporting rack.
Compared with prior art, the beneficial effects of the utility model are：A kind of solid-liquid hybrid reactor, structure letter
Single, easy to operate, the addition of easy solid material, catalyst and liquid feed liquid, the cooling jacket effect that cools is good, in powder
Broken blade improves upper crushing material on loading plate, crushing rear material and the chemical industry feed liquid mixed dissolution flowed into through filter screen
The dissolution velocity of solid material, under catalyst effect, solid material fully reacts with liquid, feed liquid entrance after reaction
In reaction kettle body, under the stirring of agitating vane and dispersion impeller, the phenomenon of precipitated and separated is avoided the occurrence of, it is impossible to big of dissolving
Grain material is screened out by filter screen, is then passed through screen holes and is fallen into storage slag chamber, realizes the abundant dissolving of solid material, and residue is easy to receive
Collection, avoid residue fall into reaction after feed liquid in influence product quality, improve the efficiency and effect of solid-liquid hybrid reaction.
Brief description of the drawings
Fig. 1 is the structure diagram of the utility model.
Fig. 2 is the structure diagram of catalyst chuck in the utility model.
In figure：1- cold water inlet pipe, 2- discharge nozzles, 3- dispersion impellers, 4- agitating vanes, 5- cooling jackets, 6- reaction kettles body,
7- supporting racks, 8- water conservancy diversion through hole, 9- cold water outlet pipe, 10- catalyst chuck, 11- offgas outlets, 12- catalyst adding tube, 13-
Solids barrel, 14- motors, 15- rotation axis, 16- solid materials adding tube, 17- liquid feed liquids adding tube, 18- filter screens,
19- Disintegrating knifes, 20- catalyst storage chamber, 21- loading plates, the capping of the 22- ends of thread, 23- storage slags chamber, 24- screen holes.
Embodiment
The following is a combination of the drawings in the embodiments of the present utility model, and the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describe, it is clear that the described embodiments are only a part of the embodiments of the utility model, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are without making creative work
All other embodiments obtained, shall fall within the protection scope of the present invention.
Please refer to Fig.1~2, in the utility model embodiment, a kind of solid-liquid hybrid reactor, including cooling jacket 5, reaction
Kettle body 6, catalyst chuck 10 and solids barrel 13,6 upper end of reaction kettle body are welded with solids barrel 13, reaction
13 side of the solids barrel connection solid material adding tube 16 of the top of kettle body 6, the addition of easy solid chemical material is described
The top of solids barrel 13 is provided with motor 14, and the shaft of motor 14 connects rotation axis 15 by shaft coupling, and rotation axis 15 is vertical
It is arranged in solids barrel 13；13 bottom of solids barrel is threadedly coupled end of thread capping 22, and the end of thread is covered in 22
The internal thread of wall is connected with the external screw thread of the 13 bottom mouth of pipe of solids barrel, facilitates the dismounting of end of thread capping 22；The solid
13 bottom inner portion of material barrel is welded with loading plate 21, and some screen holes 24, the loading plate 21 and spiral shell are evenly equipped with loading plate 21
Storage slag chamber 23 is surrounded in solids barrel 13 between line end seal lid 22, is pacified on 13 side wall of solids barrel of the upside of loading plate 21
Equipped with filter screen 18, the aperture of the filter screen 18 is less than the aperture of screen holes 24, the rotation axis 15 of the top of loading plate 21
On Disintegrating knife 19 is installed.
15 bottom of rotation axis sequentially passes through loading plate 21 and connects dispersion impeller 3 with through hole in end of thread capping 22, disperses
Agitating vane 4 is welded with rotation axis 15 between disk 3 and end of thread capping 22, the dispersion impeller 3 is arranged on the upper of discharge nozzle 2
Side, discharge nozzle 2 are welded on the bottom of reaction kettle body 6；Rotation axis 15 drives agitating vane 4 and dispersion impeller 3 to rotate, agitating vane
4 and dispersion impeller 3 to 6 internalization labor and materials liquid of reaction kettle body stir, avoid the occurrence of the phenomenon of precipitated and separated, cause in feed liquid into branch
Divide uneven influence product quality.
The outside of solids barrel 13 in the reaction kettle body 6 is fixedly connected with catalyst chuck 10, catalyst chuck 10
Catalyst storage chamber 20 is inside set to, catalyst storage chamber 20 is connected by through hole on filter screen 18 with 13 internal cavity of solids barrel, institute
10 upper end of catalyst chuck connection catalyst adding tube 12 is stated, catalyst adding tube 12 is easy to catalyst being added to catalyst storage
In chamber 20, the outside of catalyst chuck 10 is equipped with some water conservancy diversion through holes 8, and the aperture of water conservancy diversion through hole 8 is less than catalyst storage chamber 20
The particle diameter of interior catalyst.
6 upper end of reaction kettle body is welded with offgas outlet 11 and liquid feed liquid adding tube 17,11 convenience of offgas outlet
The gas produced in chemical reaction is discharged, is handled easy to further collection, 17 convenient purification labor and materials liquid of liquid feed liquid adding tube
Addition.
After solid chemical material is added in solids barrel 13, material falls on loading plate 21,14 energization work of motor
Making driving rotation axis 15 drives Disintegrating knife 19 to rotate at a high speed, and Disintegrating knife 19 is to going up crushing material on loading plate 21, after crushing
Material with through filter screen 18 flow into chemical industry feed liquid mixed dissolution, then flowed outwardly from filter screen 18, it is impossible to dissolving it is big
Granule materials are screened out by filter screen 18, are then passed through screen holes 24 and are fallen into storage slag chamber 23, realize the abundant dissolving of solid material, residual
Slag easy to collect, avoid residue fall into reaction after feed liquid in influence product quality.
The outside of reaction kettle body 6 is equipped with cooling jacket 5,5 lower end of cooling jacket connection cold water inlet pipe 1, cooling jacket 5
Upper end connection cold water outlet pipe 9, the outside of cooling jacket 5 are welded with supporting rack 7, facilitate the installation of reaction kettle body 6.
It is obvious to a person skilled in the art that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and
And in the case of the spirit or essential attributes without departing substantially from the utility model, it can realize that this practicality is new in other specific forms
Type., it is necessary to illustrate in the description of this specification, unless otherwise clearly defined and limited, term " setting ", " connected "
And " connection " should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected, or it is integrally connected；Can be with
It is to be connected directly, can also be indirectly connected by intermediary, can is the connection inside two elements.For the general of this area
For logical technical staff, the concrete meaning of above-mentioned term in the present invention can be understood with concrete condition.
Therefore, in all respects, the present embodiments are to be considered as illustrative and not restrictive, this
The scope of utility model is indicated by the appended claims rather than the foregoing description, it is intended that will fall equally in claim
All changes in the implication and scope of part are embraced therein.Any reference numeral in claim should not be regarded
To limit involved claim.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical solution, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (9)
1. a kind of solid-liquid hybrid reactor, including cooling jacket (5), reaction kettle body (6), catalyst chuck (10) and solids
Barrel (13), it is characterised in that reaction kettle body (6) upper end is welded with solids barrel (13), the solids barrel
(13) top is provided with motor (14), and the shaft of motor (14) connects rotation axis (15) by shaft coupling, and rotation axis (15) is vertical
It is arranged in solids barrel (13)；Solids barrel (13) bottom is threadedly coupled end of thread capping (22)；The solid
Material barrel (13) bottom inner portion is welded with loading plate (21), and some screen holes (24) are evenly equipped with loading plate (21), described, carrying
Filter screen (18) is installed, the rotation axis above the loading plate (21) on solids barrel (13) side wall on the upside of plate (21)
(15) Disintegrating knife (19) is installed on；Rotation axis (15) bottom sequentially passes through loading plate (21) and end of thread capping (22)
Upper through hole connection dispersion impeller (3), dispersion impeller (3) and the end of thread cover and are welded with agitating vane in the rotation axis (15) between (22)
(4)；Catalyst chuck (10), the catalyst are fixedly connected with the outside of solids barrel (13) in the reaction kettle body (6)
Chuck (10) upper end connection catalyst adding tube (12), catalyst chuck (10) outside are equipped with some water conservancy diversion through holes (8), lead
The aperture of recirculation hole (8) is less than the particle diameter of catalyst storage chamber (20) interior catalyst；Reaction kettle body (6) upper end is welded with tail
Gas exports (11) and liquid feed liquid adding tube (17).
2. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that above the reaction kettle body (6)
Solids barrel (13) side connection solid material adding tube (16).
3. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that the end of thread covers (22) inner wall
Internal thread be connected with the external screw thread of solids barrel (13) bottom mouth of pipe.
4. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that the loading plate (21) and the end of thread
Storage slag chamber (23) is surrounded in solids barrel (13) between capping (22).
5. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that the aperture of the filter screen (18) is small
In the aperture of screen holes (24).
6. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that the dispersion impeller (3) is arranged on out
The top of expects pipe (2), discharge nozzle (2) are welded on the bottom of reaction kettle body (6).
7. a kind of solid-liquid hybrid reactor according to claim 1, it is characterised in that set in the catalyst chuck (10)
For catalyst storage chamber (20), catalyst storage chamber (20) is connected by through hole on filter screen (18) and solids barrel (13) internal cavity
It is logical.
8. a kind of solid-liquid hybrid reactor according to claim 7, it is characterised in that on the outside of the catalyst chuck (10)
Equipped with some water conservancy diversion through holes (8), the aperture of water conservancy diversion through hole (8) is less than the particle diameter of catalyst storage chamber (20) interior catalyst.
9. a kind of solid-liquid hybrid reactor according to claim 7, it is characterised in that the reaction kettle body (6) is exterior
Equipped with cooling jacket (5), cooling jacket (5) lower end connection cold water inlet pipe (1), cooling jacket (5) upper end connection cold water outlet pipe
(9), it is welded with supporting rack (7) on the outside of the cooling jacket (5).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720565294.1U CN207324765U (en) | 2017-05-21 | 2017-05-21 | A kind of solid-liquid hybrid reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720565294.1U CN207324765U (en) | 2017-05-21 | 2017-05-21 | A kind of solid-liquid hybrid reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207324765U true CN207324765U (en) | 2018-05-08 |
Family
ID=62376398
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720565294.1U Expired - Fee Related CN207324765U (en) | 2017-05-21 | 2017-05-21 | A kind of solid-liquid hybrid reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207324765U (en) |
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109364858A (en) * | 2018-11-27 | 2019-02-22 | 杨迪忠 | A kind of safe solid-liquid reaction kettle of chemical industry |
| CN110339799A (en) * | 2019-07-24 | 2019-10-18 | 刘路丹 | A kind of reaction kettle for multi-phase material reaction |
| CN111821932A (en) * | 2020-07-15 | 2020-10-27 | 中国科学院上海有机化学研究所 | Continuous preparation device and preparation method of trialkyl phosphine oxide |
| CN112642367A (en) * | 2020-12-09 | 2021-04-13 | 湖北富奕达电子科技有限公司 | Reaction kettle for preparing aluminum dihydrogen phosphate from foil process waste residues and process method thereof |
| WO2021143904A1 (en) * | 2020-01-18 | 2021-07-22 | 冯三林 | Crosslinking agent and preparation thereof |
| CN113562783A (en) * | 2021-07-30 | 2021-10-29 | 福建常青新能源科技有限公司 | Preparation method of nickel sulfate solution |
| CN117326720A (en) * | 2023-09-15 | 2024-01-02 | 河北彩客新材料科技股份有限公司 | Phthalic anhydride chlorination wastewater treatment and recycling device and method |
| CN117482879A (en) * | 2023-12-29 | 2024-02-02 | 陕西红十月发展有限公司 | Mixing kettle for producing antifreeze fluid and production process thereof |
-
2017
- 2017-05-21 CN CN201720565294.1U patent/CN207324765U/en not_active Expired - Fee Related
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109364858A (en) * | 2018-11-27 | 2019-02-22 | 杨迪忠 | A kind of safe solid-liquid reaction kettle of chemical industry |
| CN110339799A (en) * | 2019-07-24 | 2019-10-18 | 刘路丹 | A kind of reaction kettle for multi-phase material reaction |
| WO2021143904A1 (en) * | 2020-01-18 | 2021-07-22 | 冯三林 | Crosslinking agent and preparation thereof |
| CN111821932A (en) * | 2020-07-15 | 2020-10-27 | 中国科学院上海有机化学研究所 | Continuous preparation device and preparation method of trialkyl phosphine oxide |
| CN112642367A (en) * | 2020-12-09 | 2021-04-13 | 湖北富奕达电子科技有限公司 | Reaction kettle for preparing aluminum dihydrogen phosphate from foil process waste residues and process method thereof |
| CN113562783A (en) * | 2021-07-30 | 2021-10-29 | 福建常青新能源科技有限公司 | Preparation method of nickel sulfate solution |
| CN117326720A (en) * | 2023-09-15 | 2024-01-02 | 河北彩客新材料科技股份有限公司 | Phthalic anhydride chlorination wastewater treatment and recycling device and method |
| CN117326720B (en) * | 2023-09-15 | 2024-04-05 | 河北彩客新材料科技股份有限公司 | Phthalic anhydride chlorination wastewater treatment and recycling device and method |
| CN117482879A (en) * | 2023-12-29 | 2024-02-02 | 陕西红十月发展有限公司 | Mixing kettle for producing antifreeze fluid and production process thereof |
| CN117482879B (en) * | 2023-12-29 | 2024-03-12 | 陕西红十月发展有限公司 | Mixing kettle for producing antifreeze fluid and production process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200117 Address after: 210000 fine chemical industry park, Hai'an Development Zone, Nantong City, Jiangsu Province (Nanyang Village, Chengdong town) Patentee after: NANTONG HONGSHEN CHEMICAL Co.,Ltd. Address before: 510000 Guangzhou High-tech Industrial Development Zone Science Avenue 231, 233 Skirt Building B1B2, 1st, 2nd, 3rd and 4th floors Patentee before: BOAO ZONGHENG NETWORK TECHNOLOGY Co.,Ltd. Effective date of registration: 20200117 Address after: 510000 Guangzhou High-tech Industrial Development Zone Science Avenue 231, 233 Skirt Building B1B2, 1st, 2nd, 3rd and 4th floors Patentee after: BOAO ZONGHENG NETWORK TECHNOLOGY Co.,Ltd. Address before: 362000 Fujian Taiwanese investment zone of Quanzhou City Dong Yuan Zhen Jin Feng Cun Hai Qi Wei No. 9 Patentee before: Huang Yanping |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180508 |