CN207318425U - A kind of waste liquid recovery apparatus for liquid chromatogram - Google Patents
A kind of waste liquid recovery apparatus for liquid chromatogram Download PDFInfo
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- CN207318425U CN207318425U CN201721389086.7U CN201721389086U CN207318425U CN 207318425 U CN207318425 U CN 207318425U CN 201721389086 U CN201721389086 U CN 201721389086U CN 207318425 U CN207318425 U CN 207318425U
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- waste liquid
- solvent bottle
- recovery apparatus
- filter mechanism
- autosampler
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Abstract
The utility model discloses a kind of waste liquid recovery apparatus for liquid chromatogram, its structure includes detector, devil liquor recovery filter mechanism, delivery pipe, autosampler, quaternary pump, vacuum degassing machine, solvent bottle, solvent bottle case, automatic injector, column oven, supporting rod, support pad, the devil liquor recovery filter mechanism is by engine base, spring, water outlet, beam ring, dust cover, water inlet, filter screen plate, upper weight, vibration body, vibration motor, lower heavy punch forms, the utility model realizes a kind of waste liquid recovery apparatus for liquid chromatogram by being provided with devil liquor recovery filter mechanism, easily unwanted waste liquid is transported to when in use in devil liquor recovery filter mechanism by high speed vibration to realize pollution separation and then say that harmful substance is isolated in device, therefore not only beneficial to environmental protection but also multinomial cumbersome process had been eliminated.
Description
Technical field
The utility model is a kind of waste liquid recovery apparatus for liquid chromatogram, belongs to waste liquid recovery apparatus field.
Background technology
Liquid chromatogram is a kind of separation and analytical technology, its main feature is that using liquid as mobile phase, stationary phase can have more
Kind form, such as paper, thin plate and packed bed, is in order to distinguish various methods during chromatographic technique develops, according to stationary phase
Form generate respective name, such as paper chromatography, thin-layer chromatography and column liquid chromatographic, the mobile phase of classical liquid chromatogram be according to
By gravity slowly through chromatographic column, therefore the granularity of stationary phase can not possibly be too small, and the sample after separation is after being graded collection
Analyzed again so that not only low separation efficiency, analyze speed are slow for classical liquid chromatogram, but also operation is also more complicated, directly
The high-effective fixed phase that granularity is less than is developed to the 1960s, and has used high pressure pump and self registering detection
Device, the shortcomings that overcoming classical liquid chromatogram, develops into high performance liquid chromatography, also referred to as high pressure liquid chromatography.
Prior art discloses Application No.：A kind of devil liquor recovery for liquid chromatogram of CN201510869987.5 fills
Put the invention and be related to a kind of quick waste liquid recovery apparatus, belong to devil liquor recovery technical field, a kind of quick waste liquid recovery apparatus, bag
Knockout drum and the recycling being connected with the knockout drum are included, cooling device is provided between the knockout drum and the recycling can,
Agitating device and heating unit are respectively arranged with inside and outside the knockout drum, it is characterised in that under the agitating device in the knockout drum
It is in netted that side, which is provided with the heat-conducting part for separating top tank structure and being connected, the heat-conducting part, hole is distributed with above, which returns
Receiving apparatus is swift to operate, has saved time cost, but prior art construction is simple, is traditionally used for the devil liquor recovery of liquid chromatogram
Device is largely served only for the accumulation for not having timely processing to cause harmful substance for recycling waste water, be not equipped with recycling and
The device that can be disposed waste liquid at the same time, therefore cause workload increase cumbersome using program.
Utility model content
In view of the deficienciess of the prior art, the utility model aim is to provide a kind of devil liquor recovery for liquid chromatogram
Device, prior art construction is simple to solve, be traditionally used for liquid chromatogram waste liquid recovery apparatus be largely served only for for
Recycling waste water does not have the accumulation that timely processing causes harmful substance, since the dress that is not equipped with recycling and can dispose waste liquid at the same time
The problem of putting, therefore causing workload increase to use program cumbersome.
To achieve these goals, the utility model is to realize by the following technical solutions：One kind is used for liquid phase color
The waste liquid recovery apparatus of spectrum, its structure include detector, devil liquor recovery filter mechanism, delivery pipe, autosampler, quaternary pump,
Vacuum degassing machine, solvent bottle, solvent bottle case, automatic injector, column oven, supporting rod, support pad, the detector are connected by bolt
It is connected to below column oven, the column oven is located at below autosampler, and the automatic injector is automatic by being mechanically connected to
Injector inner right side, for the autosampler by being electrically connected to below quaternary pump, the quaternary pump, which runs through, is connected to vacuum
Below degasser, the vacuum degassing machine is located at below solvent bottle, and the solvent bottle case is welded in above quaternary pump, and the liquid returns
Filter mechanism is received through being connected on the left of delivery pipe, the support pad is nested in below supporting rod, and the supporting rod is connected by screw thread
It is connected to below detector, the devil liquor recovery filter mechanism is by engine base, spring, water outlet, beam ring, dust cover, water inlet, filter
Dropbox, upper weight, vibration body, vibration motor, lower heavy punch, the engine base are welded in below lower heavy punch, and the spring passes through screw
It is connected to above engine base, the water outlet is welded in spring upper left, and the beam ring is welded in below dust cover, described anti-
The lid that is covered with dust passes through screw connection above beam ring, and for the water inlet through being connected on the left of detector, the lower heavy punch passes through spiral shell
Tether and be connected to below vibration motor, the filter screen plate is nested in above weight, and the upper weight is by through being connected to vibrations
Above motor, the vibration motor is located among vibration body left side, and the vibration body is welded in inside spring both sides.
Further, the delivery pipe, which runs through, is connected on the left of detector.
Further, the solvent bottle is positioned over solvent bottle case upper interior.
Further, the column oven is in same vertical plane with autosampler and is mutually perpendicular to.
Further, the solvent bottle case is parallel to each other with solvent bottle in same level.
Further, the solvent bottle case is about 50-60cm.
Further, the supporting rod material is unlikely to deform supporting rod for clad aluminum its material is firm.
Beneficial effect
The utility model realizes a kind of waste liquid recovery apparatus for liquid chromatogram and is filtered by being provided with devil liquor recovery
Mechanism, is easily transported to unwanted waste liquid in devil liquor recovery filter mechanism realizes pollution by high speed vibration when in use
Separate and then say that harmful substance is isolated in device, therefore not only beneficial to environmental protection but also eliminated multinomial cumbersome process.
Brief description of the drawings
Upon reading the detailed description of non-limiting embodiments with reference to the following drawings, other spies of the utility model
Sign, objects and advantages will become more apparent upon：
Fig. 1 is a kind of structure diagram of waste liquid recovery apparatus for liquid chromatogram of the utility model；Fig. 2 is this reality
With a kind of structure diagram of new waste liquid recovery apparatus section for liquid chromatogram；
Fig. 3 is the structure diagram of the utility model devil liquor recovery filter mechanism.
In figure：Detector -1, devil liquor recovery filter mechanism -2, delivery pipe -3, autosampler -4, quaternary pump -5, vacuum
Degasser -6, solvent bottle -7, solvent bottle case -8, automatic injector -9, column oven -10, supporting rod -11, support pad -12, engine base -
201st, spring -202, water outlet -203, beam ring -204, dust cover -205, water inlet -206, filter screen plate -207, upper weight -
208th, vibration body -209, vibration motor -210, lower heavy punch -211.
Embodiment
To make the technical means, creative features, achievable purpose and effectiveness that the utility model is realized easy to understand, below
With reference to embodiment, the utility model is expanded on further.
- Fig. 2 is please referred to Fig.1, the utility model provides a kind of waste liquid recovery apparatus for liquid chromatogram：Its structure includes
It is detector 1, devil liquor recovery filter mechanism 2, delivery pipe 3, autosampler 4, quaternary pump 5, vacuum degassing machine 6, solvent bottle 7, molten
Agent bottle case 8, automatic injector 9, column oven 10, supporting rod 11, support pad 12, the detector 1 are bolted to column oven
10 lower sections, the column oven 10 are located at the lower section of autosampler 4, and the automatic injector 9 is by being mechanically connected to auto injection
Device inner right side, by being electrically connected to the lower section of quaternary pump 5, the quaternary pump 5 takes off through being connected to vacuum the autosampler 4
The lower section of mechanism of qi 6, the vacuum degassing machine 6 are located at the lower section of solvent bottle 7, and the solvent bottle case 8 is welded in the top of quaternary pump 5, described
Liquid recycling filter mechanism 2 is nested in the lower section of supporting rod 11, the supporting rod through the left side of delivery pipe 3, the support pad 12 is connected to
11 are threadingly attached to the lower section of detector 1, the devil liquor recovery filter mechanism 2 by engine base 201, spring 202, water outlet 203,
It is beam ring 204, dust cover 205, water inlet 206, filter screen plate 207, upper weight 208, vibration body 209, vibration motor 210, lower heavy
Hammer 211, the engine base 201 are welded in the lower section of lower heavy punch 211, the spring 202 by screw connection above engine base 201, institute
State water outlet 203 and be welded in 202 upper left of spring, the beam ring 204 is welded in the lower section of dust cover 205, the dust seal
For lid 205 by screw connection above beam ring 204, the water inlet 206, which runs through, is connected to the left side of detector 1, the lower heavy punch
211 are bolted to the lower section of vibration motor 210, and the filter screen plate 207 is nested in the top of weight 208, the upper weight
208 by the way that through being connected to above vibration motor 210, the vibration motor 210 is located among the left side of vibration body 209, the shake
Kinetoplast 209 is welded in inside 202 both sides of spring, and the delivery pipe 3, which runs through, is connected to the left side of detector 1, the solvent bottle 7
8 upper interior of solvent bottle case is positioned over, the column oven 10 is in same vertical plane with autosampler 4 and is mutually perpendicular to, described
Solvent bottle case 8 is parallel to each other with solvent bottle 7 in same level, and the solvent bottle case 8 is about 50-60cm, the supporting rod
11 materials are unlikely to deform supporting rod 11 for clad aluminum its material is firm.
The optimization of the series quaternary pump of 5 Agilent of quaternary pump 1200 described in the utility model and vacuum degassing machine composition one
Design, by 2 tandem pistons to float and accurate SERVO CONTROL, obtains the solvent stream of no pulse, stabilization, this design is logical
Crossing stroke changeable volume makes solvent delivery not have pulse, and has obtained effective mixing, main application：Suitable for environment and food
Routinely applied in analysis field, and the method exploitation of pharmaceutical industry, four kinds of solvents carry out unit or gradient mixing, so as to accelerate
The speed of method exploitation, prepare mobile phase and rinse liquid chromatographic system, reduces to greatest extent and safeguards, reduces running cost,
By using most of durable materials for requiring harsh applications can be born, as stainless steel, titanium, gold, ruby, sapphire,
Ceramics etc., it is ensured that the long life, realizing active sealing pad cleaning option is recommended under the conditions of high salt mobile phase, to prevent from corroding,
The wide range of flow that peak flow rate (PFR) reaches, works suitable for different liquid chromatograies, including half preparative separation, and controller is held by hand
Or different Agilent data systems, such as Agilent chem workstation, it is programmed and controls, built-in leakage and pressure detecting,
Graphically pressure change, and early stage safeguard feedback, there is provided more to help.
Carrying out in use, the water inlet 206 in the delivery pipe 3 and devil liquor recovery filter mechanism 2 that will convey waste liquid connects
Together, waste liquid is entered in next step by the filtering of filter screen plate 207, and lower heavy punch 211 and upper weight are had on vibration motor 210
208 by the work of vibration motor 210 make upper weight 208 and lower heavy punch 211 be quick, high-frequency percussion vibration body 209 so as to
Sound wave is produced to make the harmful substance in waste liquid separate and then excrete out harmful substance by water outlet 203, can be recycled
Also the mask work that waste liquid can be carried out at the same time greatly alleviates required workload.
Its structure and principle are all that this technology personnel can be learnt by technical manual or be known by normal experiment method,
The utility model solves the problems, such as it is that prior art construction is simple, and the waste liquid recovery apparatus for being traditionally used for liquid chromatogram is most of
The accumulation for not having timely processing to cause harmful substance for recycling waste water is served only for, since being not equipped with recycling and can handle at the same time
The device of waste liquid, therefore it is cumbersome using program to cause workload to increase, the utility model is combined with each other by above-mentioned component, this
Utility model realizes a kind of waste liquid recovery apparatus for liquid chromatogram by being provided with devil liquor recovery filter mechanism, is using
Shi Rongyi is transported in devil liquor recovery filter mechanism unwanted waste liquid by high speed vibration to realize pollution separation and then say
Harmful substance is isolated in device, therefore not only beneficial to environmental protection but also eliminates multinomial cumbersome process, described in detail below:
The engine base 201 is welded in the lower section of lower heavy punch 211, the spring 202 by screw connection above engine base 201,
The water outlet 203 is welded in 202 upper left of spring, and the beam ring 204 is welded in the lower section of dust cover 205, described dust-proof
By screw connection above beam ring 204, the water inlet 206, which runs through, is connected to the left side of detector 1, described lower heavy for capping 205
Hammer 211 is bolted to the lower section of vibration motor 210, and the filter screen plate 207 is nested in the top of weight 208, described heavy
Hammer 208 is by the way that through being connected to above vibration motor 210, the vibration motor 210 is located among the left side of vibration body 209, described
Vibration body 209 is welded in inside 202 both sides of spring.
The advantages of basic principle and main feature and the utility model of the utility model has been shown and described above, for
For those skilled in the art, it is clear that the utility model is not limited to the details of above-mentioned one exemplary embodiment, and without departing substantially from this
In the case of the spirit or essential attributes of utility model, the utility model can be realized in other specific forms.Therefore, no matter
From the point of view of which point, the present embodiments are to be considered as illustrative and not restrictive, and the scope of the utility model is by institute
Attached claim rather than described above limit, it is intended that will fall in the implication and scope of the equivalency of claim
All changes are embraced therein.Any reference numeral in claim should not be considered as to the involved right of limitation
It is required that.
Moreover, it will be appreciated that although the present specification is described in terms of embodiments, not each embodiment is only wrapped
Containing an independent technical solution, this narrating mode of specification is only that those skilled in the art should for clarity
Using specification as an entirety, the technical solutions in the various embodiments may also be suitably combined, forms those skilled in the art
It is appreciated that other embodiment.
Claims (5)
1. a kind of waste liquid recovery apparatus for liquid chromatogram, its structure include detector (1), devil liquor recovery filter mechanism (2),
Delivery pipe (3), autosampler (4), quaternary pump (5), vacuum degassing machine (6), solvent bottle (7), solvent bottle case (8), automatic note
Emitter (9), column oven (10), supporting rod (11), support pad (12), it is characterised in that：
The detector (1) is bolted to below column oven (10), and the column oven (10) is located at autosampler (4)
Lower section, the automatic injector (9) are passed through by being mechanically connected to autosampler inner right side, the autosampler (4)
It is electrically connected to below quaternary pump (5), the quaternary pump (5), which is run through, to be connected to below vacuum degassing machine (6), the vacuum degassing machine
(6) below solvent bottle (7), the solvent bottle case (8) is welded in above quaternary pump (5), the liquid recycling filter mechanism (2)
Through being connected on the left of delivery pipe (3), the support pad (12) is nested in below supporting rod (11), and the supporting rod (11) passes through spiral shell
Line is connected to below detector (1)；
The devil liquor recovery filter mechanism (2) is by engine base (201), spring (202), water outlet (203), beam ring (204), dust seal
Cover (205), water inlet (206), filter screen plate (207), upper weight (208), vibration body (209), vibration motor (210), lower heavy punch
(211) form, the engine base (201) is welded in below lower heavy punch (211), and the spring (202) is by screw connection in engine base
(201) top, the water outlet (203) are welded in spring (202) upper left, and the beam ring (204) is welded in dust cover
(205) lower section, the dust cover (205) is by screw connection above beam ring (204), and the water inlet (206) is through company
It is connected on the left of detector (1), the lower heavy punch (211) is bolted to below vibration motor (210), the filter screen plate
(207) it is nested in above weight (208), the upper weight (208) is by through being connected to above vibration motor (210), institute
State vibration motor (210) to be located among vibration body (209) left side, the vibration body (209) is welded in spring (202) both sides
Portion.
A kind of 2. waste liquid recovery apparatus for liquid chromatogram according to claim 1, it is characterised in that：The delivery pipe
(3) run through and be connected on the left of detector (1).
A kind of 3. waste liquid recovery apparatus for liquid chromatogram according to claim 1, it is characterised in that：The solvent bottle
(7) it is positioned over solvent bottle case (8) upper interior.
A kind of 4. waste liquid recovery apparatus for liquid chromatogram according to claim 1, it is characterised in that：The column oven
(10) same vertical plane is in autosampler (4) to be mutually perpendicular to.
A kind of 5. waste liquid recovery apparatus for liquid chromatogram according to claim 1, it is characterised in that：The solvent bottle
Case (8) is parallel to each other with solvent bottle (7) in same level.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721389086.7U CN207318425U (en) | 2017-10-26 | 2017-10-26 | A kind of waste liquid recovery apparatus for liquid chromatogram |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721389086.7U CN207318425U (en) | 2017-10-26 | 2017-10-26 | A kind of waste liquid recovery apparatus for liquid chromatogram |
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| Publication Number | Publication Date |
|---|---|
| CN207318425U true CN207318425U (en) | 2018-05-04 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201721389086.7U Active CN207318425U (en) | 2017-10-26 | 2017-10-26 | A kind of waste liquid recovery apparatus for liquid chromatogram |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112147263A (en) * | 2020-09-16 | 2020-12-29 | 内蒙古电力(集团)有限责任公司内蒙古电力科学研究院分公司 | Full-automatic degasser |
-
2017
- 2017-10-26 CN CN201721389086.7U patent/CN207318425U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112147263A (en) * | 2020-09-16 | 2020-12-29 | 内蒙古电力(集团)有限责任公司内蒙古电力科学研究院分公司 | Full-automatic degasser |
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