CN207286755U - One kind production 3,3- acid dimethyl extractors - Google Patents
One kind production 3,3- acid dimethyl extractors Download PDFInfo
- Publication number
- CN207286755U CN207286755U CN201721222702.XU CN201721222702U CN207286755U CN 207286755 U CN207286755 U CN 207286755U CN 201721222702 U CN201721222702 U CN 201721222702U CN 207286755 U CN207286755 U CN 207286755U
- Authority
- CN
- China
- Prior art keywords
- tank body
- agitating shaft
- stirring
- ring
- acid dimethyl
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Landscapes
- Extraction Or Liquid Replacement (AREA)
- Mixers Of The Rotary Stirring Type (AREA)
Abstract
The utility model discloses one kind production 3, 3 acid dimethyl extractors, including tank body and stent, tank body is arranged on stent, feed liquor bucket and feed pipe are respectively equipped with the top of tank body, the bottom of tank body is equipped with drain pipe, the top of tank body is equipped with driving motor, agitating shaft is connected with tank body, drive motor connection agitating shaft, agitator disk and scraping plate mechanism are respectively equipped with agitating shaft, it is surround on agitator disk and stirring gap is distributed with, scraping plate mechanism includes axle sleeve, stir plate and arc scraper plate, stir plate connecting bushing and arc scraper plate, stir plate is evenly distributed on the circumference of axle sleeve, axle sleeve is fixed on agitating shaft, hemisphere protrusion is evenly distributed with the outer wall of arc scraper plate, hemisphere protrusion is in contact with inner tank wall.The utility model is simple in structure, stirs evenly, thoroughly, and extraction efficiency is high, and effect of extracting is good, highly practical.
Description
Technical field
The utility model belongs to pharmaceutical chemistry technical field, more particularly to a kind of 3,3- of production acid dimethyl extractions
Tank.
Background technology
3,3- acid dimethyls are a kind of important medicine, pesticide, organic synthesis intermediate, are mainly used as medicine, pesticide
Intermediate, lubricant etc..For 3,3- acid dimethyls to be yellowish to colourless transparent liquid, fusing point is -8~6 DEG C, boiling point for 185~
190℃。
Pot type extractor is suitable for the extraction during production 3,3- acid dimethyls, its is simple in structure, cheap, easy
In manufacture and maintenance, discontinuous extraction is particularly suitable for.But it there is also it is obvious the shortcomings that：I.e. extraction efficiency is low, this is main
It is due to that general extractor simply uses simple mechanical agitation so that mutual exclusive two phase liquid can not be abundant in tank
Contact, mass transfer surface is limited, thus to reach solute and take a long time in the partition equilibrium of two-phase.
Utility model content
The utility model aim is to solve above-mentioned technical problem existing in the prior art, there is provided one kind production 3,3- bis-
Methylbutanoic acid extractor, it is simple in structure, stir evenly, thoroughly, extraction efficiency is high, and effect of extracting is good, highly practical.
In order to solve the above-mentioned technical problem, the utility model adopts the following technical solution：
One kind production 3,3- acid dimethyl extractors, including tank body and stent, tank body are arranged on stent, the top of tank body
Portion is respectively equipped with feed liquor bucket and feed pipe, and the bottom of tank body is equipped with drain pipe, it is characterised in that：The top of tank body is equipped with driving electricity
Machine, is connected with agitating shaft in tank body, driving motor connection agitating shaft, and agitator disk and scrapper conveyor are respectively equipped with agitating shaft
Structure, around stirring gap is distributed with agitator disk, scraping plate mechanism includes axle sleeve, stir plate and arc scraper plate, stir plate connecting shaft
Set and arc scraper plate, stir plate are evenly distributed on the circumference of axle sleeve, and axle sleeve is fixed on agitating shaft, on the outer wall of arc scraper plate
Hemisphere protrusion is evenly distributed with, hemisphere protrusion is in contact with inner tank wall；The extractor is simple in structure, stirs evenly, thoroughly, extraction
Take efficient, effect of extracting is good, highly practical.
Further, agitator disk includes central ring, stirring sheet and stirring ring, stirring sheet connection stirring ring and central ring, adjacent
Stirring gap is formed between stirring sheet, central ring is fixed on agitating shaft, and driving motor drives central ring to rotate, and stirring sheet and is stirred
Mix ring and then to rotate synchronously, the setting for stirring gap increases the contact area of agitator disk and liquid, passes through stirring sheet and stirring
Ring stirs liquid at the same time, and mixing power is strong, stirs evenly, and in whipping process, the liquid in stirring gap mutually clashes secondary
Number is more, more acutely so that 3,3- acid dimethyls and extract contact are more abundant, so as to improve effect of extracting.
Further, be equipped with interlocking bar between stirring sheet and stir plate, interlocking bar not only increase stirring sheet and stir plate it
Between bonding strength, together with also so that agitator disk pins down with scraping plate mechanism, strengthen synchronous rotation and act on, so as to improve stirring
Effect.
Further, choke block is equipped with feed pipe, is evenly distributed with throttle orifice on choke block, 3,3- dimethyl butyrates will be contained
The mixed liquor of acid is sent into from feed pipe, and mixed liquor can only be from throttle orifice by the way that instantaneous delivery reduces, so as to reduce mixed liquor pair
The percussion of inner tank wall, protects tank body, and the impurity mixed in mixed liquor can not be stopped in choke block by throttle orifice
On, easy cleaning.
Further, tank body is equipped with observation visor, facilitates people to observe extraction process and extraction in tank body exactly and stands
The delamination of liquid afterwards, significantly reduces error caused by discharging, reduces product loss.
Further, stent includes fixed weld-ring and leg, leg are evenly distributed on the circumference of fixed weld-ring, fixed weld-ring
Fixedly sleeved tank body, stent improve stability when tank body is kept flat by leg, and supporting role is strong, ensure that tank body will not fall
Turn over.
The utility model is by adopting the above-described technical solution, have the advantages that：
Agitator disk and scraping plate mechanism are respectively equipped with the utility model on agitating shaft, driving motor drives agitating shaft to rotate,
Agitating shaft rotates drives agitator disk and scraping plate mechanism to rotate synchronously at the same time, and stir plate and arc scraper plate are rotated with axle sleeve, to liquid
Stirred, around stirring gap is distributed with agitator disk, the setting for stirring gap increases the contact surface of agitator disk and liquid
Product, stirs liquid, Double stirring, mixing power is strong, stirs evenly so that 3,3- dimethyl butyrates at the same time by stirring sheet and stirring ring
Acid and extract contact are more abundant, improve extraction efficiency；In whipping process, the liquid in stirring gap mutually clashes secondary
Number is more, and more acutely, so as to improve effect of extracting, hemisphere protrusion is constantly contacted with inner tank wall, will be adhered to inner tank wall
On liquid scrape, prevent it to be bonded in inner tank wall, so as to improve the rate of recovery of 3,3- acid dimethyls after extraction, and subtract
Scraping effect of the small arc scraper plate to inner tank wall, reduces the degree of wear, extends the service life of tank body.The utility model knot
Structure is simple, stirs evenly, thoroughly, and extraction efficiency is high, and effect of extracting is good, highly practical.
Brief description of the drawings
The utility model is described in further detail below in conjunction with the accompanying drawings：
Fig. 1 is the internal structure schematic diagram of tank body in the utility model；
Fig. 2 is the structure diagram that driving motor is connected with agitator disk, scraping plate mechanism in the utility model；
Fig. 3 is the structure diagram of the utility model middle scraper mechanism；
Fig. 4 is the structure diagram of agitator disk in the utility model；
Fig. 5 is the structure diagram that tank body is connected with stent in the utility model.
In figure：1- tank bodies；2- stents；3- fixes weld-ring；4- legs；5- feed liquor buckets；6- feed pipes；7- choke blocks；8- is saved
Discharge orifice；9- drain pipes；10- drives motor；11- agitating shafts；12- agitator disks；13- scraping plate mechanisms；14- axle sleeves；15- stir plates；
16- arc scraper plates；17- hemisphere is raised；18- central rings；19- stirring sheets；20- stirs ring；21- stirs gap；22- interlocking bar；
23- observes visor.
Embodiment
As shown in Figures 1 to 5, it is a kind of production 3,3- acid dimethyl extractors of the utility model, including 1 He of tank body
Stent 2, stent 2 includes fixed weld-ring 3 and leg 4, leg 4 are evenly distributed on the circumference of fixed weld-ring 3, and fixed weld-ring 3 is solid
Surely tank body 1 is socketed, stent 2 improves stability when tank body 1 is kept flat by leg 4, and supporting role is strong, ensures that tank body 1 will not
Tipping.The top of tank body 1 is respectively equipped with feed liquor bucket 5 and feed pipe 6, and extract is sent into from feed liquor bucket 5, and section is equipped with feed pipe 6
Flowing plate 7, is evenly distributed with throttle orifice 8 on choke block 7, and the mixed liquor that will contain 3,3- acid dimethyls is sent into from feed pipe 6, mixes
Closing liquid can only be from throttle orifice 8 by the way that instantaneous delivery reduces, so as to reduce percussion of the mixed liquor to 1 inner wall of tank body, protects
Tank body 1, the impurity mixed in mixed liquor can not be stopped on choke block 7, easy cleaning by throttle orifice 8.Tank body 1
Bottom is equipped with drain pipe 9, and the solution after layering is discharged successively from drain pipe 9.The top of tank body 1 is equipped with driving motor 10, tank body 1
Agitating shaft 11 is inside connected with, driving motor 10 connects agitating shaft 11, agitator disk 12 and scraper plate are respectively equipped with agitating shaft 11
Mechanism 13, driving motor 10 drive agitating shaft 11 to rotate, and agitating shaft 11 rotates drives agitator disk 12 and scraping plate mechanism 13 same at the same time
Step rotates, and scraping plate mechanism 13 includes axle sleeve 14, stir plate 15 and arc scraper plate 16,15 connecting bushing 14 of stir plate and arc scraper plate
16, stir plate 15 is evenly distributed on the circumference of axle sleeve 14, and axle sleeve 14 is fixed on agitating shaft 11, on the outer wall of arc scraper plate 16
Hemisphere protrusion 17 is evenly distributed with, hemisphere protrusion 17 is in contact with 1 inner wall of tank body, in whipping process, stir plate 15 and arc
Scraper plate 16 is rotated with axle sleeve 14, and liquid is stirred, and hemisphere protrusion 17 is constantly contacted with 1 inner wall of tank body, will be adhered to tank body 1
Liquid on inner wall scrapes, and prevents it to be bonded on 1 inner wall of tank body, so as to improve the recycling of 3,3- acid dimethyls after extraction
Rate, and scraping effect of the arc scraper plate 16 to 1 inner wall of tank body is reduced, the degree of wear is reduced, extends the service life of tank body 1.
Agitator disk 12 includes central ring 18, stirring sheet 19 and stirring ring 20, the connection of stirring sheet 19 stirring ring 20 and central ring
18, stirring gap 21 is formed between adjacent stirring sheet 19, central ring 18 is fixed on agitating shaft 11, and driving motor 10 drives center
Circle 18 rotates, and stirring sheet 19 and stirring ring 20 and then rotate synchronously, and the setting in stirring gap 21 increases agitator disk 12 and liquid
Contact area, by stirring sheet 19 and stirring ring 20 at the same time stir liquid, mixing power is strong, stirs evenly, in whipping process,
Liquid in stirring gap 21 mutually clashes often, more acutely so that 3,3- acid dimethyls and extract contact
More fully, so as to improve effect of extracting.Interlocking bar 22 is equipped between stirring sheet 19 and stir plate 15, interlocking bar 22 not only increases
Bonding strength between stirring sheet 19 and stir plate 15, together with also so that agitator disk 12 pins down with scraping plate mechanism 13, strengthens together
Rotary action is walked, so as to improve mixing effect.Tank body 1 is equipped with observation visor 23, facilitates people to observe exactly in tank body 1
The delamination of liquid after extraction process and extraction are stood, significantly reduces error caused by discharging, reduces product damage
Lose.
Agitator disk 12 and scraping plate mechanism 13 are respectively equipped with the utility model on agitating shaft 11, driving motor 10 drives stirring
Axis 11 rotates, and agitating shaft 11 rotates drives agitator disk 12 and scraping plate mechanism 13 to rotate synchronously at the same time, stir plate 15 and arc scraper plate
16 rotate with axle sleeve 14, and liquid is stirred, and around stirring gap 21 is distributed with agitator disk 12, stir the setting in gap 21
The contact area of agitator disk 12 and liquid is increased, liquid is stirred by stirring sheet 19 and stirring ring 20 at the same time, Double stirring, is stirred
It is strong to mix power, stirs evenly so that 3,3- acid dimethyls and extract contact are more abundant, improve extraction efficiency；In whipping process
In, the liquid in stirring gap 21 mutually clashes often, and more acutely, so as to improve effect of extracting, hemisphere is raised
17 constantly contact with 1 inner wall of tank body, and the liquid being adhered on 1 inner wall of tank body is scraped, and prevent it to be bonded on 1 inner wall of tank body,
So as to improve the rate of recovery of 3,3- acid dimethyls after extraction, and scraping effect of the arc scraper plate 16 to 1 inner wall of tank body is reduced,
The degree of wear is reduced, extends the service life of tank body 1.The utility model is simple in structure, stirs evenly, thoroughly, and extraction efficiency is high,
Effect of extracting is good, highly practical.
The above are only specific embodiments of the present invention, but the technical characteristics of the utility model is not limited thereto.Appoint
How based on the utility model, to solve essentially identical technical problem, essentially identical technique effect is realized, it is made
Simple change, equivalent substitution or modification etc., are all covered by among the scope of protection of the utility model.
Claims (6)
1. one kind production 3,3- acid dimethyl extractors, including tank body and stent, the tank body are arranged on the stent, institute
State and feed liquor bucket and feed pipe be respectively equipped with the top of tank body, the bottom of the tank body is equipped with drain pipe, it is characterised in that：The tank
The top of body is equipped with driving motor, and agitating shaft is connected with the tank body, and the driving motor connects the agitating shaft, institute
State and agitator disk and scraping plate mechanism are respectively equipped with agitating shaft, surround on the agitator disk and stirring gap, the scrapper conveyor is distributed with
Structure includes axle sleeve, stir plate and arc scraper plate, and the stir plate connects the axle sleeve and the arc scraper plate, and the stir plate is equal
Even to be distributed on the circumference of the axle sleeve, the axle sleeve is fixed on the agitating shaft, on the outer wall of the arc scraper plate uniformly
Hemisphere protrusion is distributed with, the hemisphere is raised to be in contact with the inner tank wall.
A kind of 2. production 3,3- acid dimethyl extractors according to claim 1, it is characterised in that：The agitator disk
Including central ring, stirring sheet and stirring ring, the stirring sheet connection stirring ring and the central ring, the adjacent stirring sheet
Between form the stirring gap, the central ring is fixed on the agitating shaft.
A kind of 3. production 3,3- acid dimethyl extractors according to claim 2, it is characterised in that：The stirring sheet
Interlocking bar is equipped between the stir plate.
A kind of 4. production 3,3- acid dimethyl extractors according to claim 1, it is characterised in that：The feed pipe
It is interior to be equipped with choke block, it is evenly distributed with throttle orifice on the choke block.
A kind of 5. production 3,3- acid dimethyl extractors according to claim 1, it is characterised in that：On the tank body
Equipped with observation visor.
A kind of 6. production 3,3- acid dimethyl extractors according to claim 1, it is characterised in that：The stent bag
Fixed weld-ring and leg are included, the leg is evenly distributed on the circumference of the fixed weld-ring, and the fixed weld-ring is fixedly sleeved
The tank body.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721222702.XU CN207286755U (en) | 2017-09-22 | 2017-09-22 | One kind production 3,3- acid dimethyl extractors |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721222702.XU CN207286755U (en) | 2017-09-22 | 2017-09-22 | One kind production 3,3- acid dimethyl extractors |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207286755U true CN207286755U (en) | 2018-05-01 |
Family
ID=62442218
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721222702.XU Expired - Fee Related CN207286755U (en) | 2017-09-22 | 2017-09-22 | One kind production 3,3- acid dimethyl extractors |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207286755U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112619552A (en) * | 2020-12-01 | 2021-04-09 | 姜瑞玉 | Fertilizer granulator |
| CN112958026A (en) * | 2021-02-19 | 2021-06-15 | 河南星汉生物科技有限公司 | Continuous acidolysis reaction device for lactic acid production |
-
2017
- 2017-09-22 CN CN201721222702.XU patent/CN207286755U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112619552A (en) * | 2020-12-01 | 2021-04-09 | 姜瑞玉 | Fertilizer granulator |
| CN112958026A (en) * | 2021-02-19 | 2021-06-15 | 河南星汉生物科技有限公司 | Continuous acidolysis reaction device for lactic acid production |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN207286755U (en) | One kind production 3,3- acid dimethyl extractors | |
| CN207546372U (en) | The raw material Two-way Cycle agitation mixer of composite heat transfer | |
| CN208584666U (en) | A kind of road construction cement mortar mixing arrangement | |
| CN205887039U (en) | A ball mill belt cleaning device for mud production device | |
| CN101972624A (en) | Combined stirred tank reactor | |
| CN106378870A (en) | Clearing device of stirring machine | |
| CN208193728U (en) | A kind of Chinese medicine extracting tank with waste residue filtering device | |
| CN201832652U (en) | Combined stirring reaction kettle | |
| CN108608577A (en) | A kind of uniformly mixed concrete central mix plant | |
| CN108057367A (en) | Stir the adjustable agitating device of radius | |
| CN207256549U (en) | A kind of thoroughly concrete batch plant that discharges | |
| CN208066244U (en) | Toothpaste Manufacturing medicine extract machine | |
| CN207430188U (en) | A kind of Chinese medicine ointment making apparatus | |
| CN211798956U (en) | Extraction tank for producing tetradecyl tributyl phosphine chloride | |
| CN114214115A (en) | Tea oil production equipment and processing technology | |
| CN213012832U (en) | Fermentation cylinder with scrape flitch | |
| CN209631136U (en) | A kind of at the uniform velocity chemical-dosing mixer | |
| CN209173819U (en) | A kind of battery manufacture pulp blender | |
| CN203469892U (en) | Planetary vacuum mixer | |
| CN209333607U (en) | A kind of cylindricality double worm mixer of anti-clogging easy to clean | |
| CN203369355U (en) | Mushroom digester | |
| CN208080476U (en) | Chocolate mass agitation mixer | |
| CN207210230U (en) | The double-deck stirring frock of sludge treatment mud-water separation | |
| CN208049917U (en) | A kind of glass lined stirring kettle that mixing effect is good | |
| CN106378025B (en) | A kind of graphene slurry stirring device and its stirring means |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180501 Termination date: 20210922 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |