CN211798956U

CN211798956U - Extraction tank for producing tetradecyl tributyl phosphine chloride

Info

Publication number: CN211798956U
Application number: CN202020260274.5U
Authority: CN
Inventors: 刘乾; 刘路远; 刘玉强; 刘玉真; 刘阳升
Original assignee: Shandong Weitian Fine Chemical Technology Co ltd
Current assignee: Shandong Weitian Fine Chemical Technology Co ltd
Priority date: 2020-03-05
Filing date: 2020-03-05
Publication date: 2020-10-30
Anticipated expiration: 2030-03-05

Abstract

The utility model relates to the technical field of extraction tanks, and discloses an extraction tank for producing tetradecyl tributyl phosphine chloride, which comprises an outer tank body and an inner tank body, wherein a blow-off pipe is arranged on the inner wall at the bottom of the inner tank body, the inner wall at the bottom of the inner tank body is arranged in a reversed hopper shape, a liquid outlet is arranged on the inclined plane at the bottom of the inner tank body, the other end of the liquid outlet is communicated with a circulating pump through a pipeline, the inner wall at the top of the inner tank body is provided with a circulating inlet, the circulating pump is communicated with the circulating inlet through the circulating pipe, the inner wall at the top of the inner tank body is provided with a charging pipe, and a stirring bin is fixedly arranged on the outer wall at the top of the outer tank body, the utility model has reasonable transmission structure, realizes the real-time stirring effect when extracting raw materials are extracted, and the stirring and, the production of enterprises is facilitated, and the production efficiency of the enterprises is improved.

Description

Extraction tank for producing tetradecyl tributyl phosphine chloride

Technical Field

The utility model relates to an extraction jar technical field especially relates to an extraction jar is used in production of tetradecyl tributyl phosphine chloride.

Background

The extraction is also called solvent extraction or liquid-liquid extraction (to be distinguished from solid-liquid extraction, namely leaching), also called extraction (generally used in petroleum refining industry), is a mass transfer separation process for realizing component separation by treating a two-component or multi-component solution which is immiscible with a liquid extracting agent, and the extraction has two modes by utilizing the principle of similar intermiscibility: liquid-liquid extraction, in which a selected solvent is used to separate a component from a liquid mixture, the solvent must be immiscible with the liquid mixture to be extracted, has selective dissolving power, must have good thermal and chemical stability, and has little toxicity and corrosiveness, such as separation of phenols from coal tar with benzene, separation of olefins from petroleum fractions with organic solvents, extraction of Br2 from water with CCl4, and the like; solid-liquid extraction, also known as leaching, uses solvents to separate the components of a solid mixture, such as "percolation" or "leaching", which is the process of extracting sugars from sugar beets with water, extracting soybean oil from soybeans with alcohol to increase oil yield, and extracting the active ingredients from Chinese herbs with water to produce a fluid extract.

The extraction tank is often used in production of tetradecyl tributyl phosphonium chloride, the existing tetradecyl tributyl phosphonium chloride is not easy to mix in the production process, if the existing tetradecyl tributyl phosphonium chloride is stirred and mixed in advance, the extraction work is not facilitated, the stirring effect of the existing extraction tank is poor, the stirring structure is often arranged in the extraction tank, the stirring and mixing or feeding work is difficult to control, and the production work of the tetradecyl tributyl phosphonium chloride of an enterprise is not facilitated.

SUMMERY OF THE UTILITY MODEL

The utility model provides an extraction jar is used in production of tetradecyl tributyl phosphonium chloride, the stirring of this extraction jar of aim at mixes the effect good, and easily controls, has satisfied the mixing operation of tetradecyl tributyl phosphonium chloride in extraction production.

In order to realize the technical purpose, the technical effect is achieved, the utility model discloses a realize through following technical scheme:

an extraction tank for producing tetradecyl tributyl phosphine chloride comprises an outer tank body and an inner tank body, wherein a heating plate is installed between the outer tank body and the inner tank body, a blow-off pipe is installed on the inner wall of the bottom of the inner tank body, the inner wall of the bottom of the inner tank body is arranged in a reversed bucket shape, a liquid outlet is arranged on the inclined plane of the bottom of the inner tank body outwards, a circulating pump is connected to the other end of the liquid outlet through a pipeline, a circulating inlet is arranged on the inner wall of the top of the inner tank body outwards, a circulating pipe is installed at the discharge outlet of the circulating pump, the circulating pump is connected with the circulating inlet through the circulating pipe, a feeding pipe is arranged on the inner wall of the top of the inner tank body outwards, a stirring bin is fixedly installed on the outer wall of the top of the outer tank body, a raw material inlet pipe is installed on the hole of the top of the, be provided with the transmission shaft among the gear reducer, fixed mounting has the ring board on the inner chamber lateral wall in stirring storehouse, the bottom of transmission shaft extends to in the ring board, install through gear engagement in the ring board and assist the axle, the bottom outer wall fixed mounting of transmission shaft has the main shaft, the main shaft passes through gear drive with the top of assisting the axle and connects, and the main shaft passes through the bottom inner wall in bearing swing joint stirring storehouse with the bottom of assisting the axle, equal fixed mounting has the puddler on the outer wall of main shaft and assistance axle.

Preferably, in the extraction tank for producing tetradecyl tributyl phosphonium chloride, three auxiliary shafts are annularly and equally arranged on the outer side of the main shaft.

Preferably, in the extraction tank for producing tetradecyl tributyl phosphonium chloride, the stirring rods are respectively and equally arranged on the outer walls of the main shaft and the auxiliary shaft from top to bottom in sequence.

Preferably, in the extraction tank for producing tetradecyl tributyl phosphonium chloride, the stirring rods on the main shaft and the auxiliary shaft are arranged in a vertically staggered manner.

Preferably, in the extraction tank for producing tetradecyl tributyl phosphonium chloride, valves are correspondingly arranged on the outer wall of the top of the feeding pipe and the outer wall of the drain pipe.

The utility model has the advantages that: the utility model discloses the transmission structure in stirring storehouse sets up rationally, the motor passes through gear reducer's the rotational speed that reduces, meshing through the gear can drive main shaft and every auxiliary shaft simultaneously and rotate, and then can drive every puddler in the stirring storehouse and rotate, the high-efficient stirring mixed work to tetradecyl tributyl phosphine chloride extraction raw materials has been accomplished, overall structure sets up rationally reliably, the real-time stirring effect when having realized extracting the raw materials, avoided installing additional stirring structure in the extraction jar and stirring in advance, subsequent extraction effect has been improved, the stirring is mixed simultaneously or reinforced work is easily controlled, higher extraction efficiency has, do benefit to the production of enterprise and improved the production efficiency of enterprise.

Drawings

In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the drawings used in the description of the embodiments will be briefly introduced below, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and it is obvious for those skilled in the art that other drawings can be obtained according to these drawings without creative efforts.

FIG. 1 is a schematic view of the overall internal structure of the present invention;

FIG. 2 is an enlarged view of a portion A of FIG. 1 according to the present invention;

fig. 3 is a schematic view of the transmission structure of the main shaft and the auxiliary shaft of the present invention.

In the drawings, the components represented by the respective reference numerals are listed below:

1. an outer tank body; 2. an inner tank body; 3. heating plates; 4. a blow-off pipe; 5. a feed tube; 6. a circulation inlet; 7. a circulation pipe; 8. a circulation pump; 9. a liquid outlet; 10. a stirring bin; 11. feeding the raw materials into a pipe; 12. a circular ring plate; 13. a motor; 14. a gear reducer; 15. a drive shaft; 16. a main shaft; 17. an auxiliary shaft; 18. a stirring rod.

Detailed Description

The technical solutions in the embodiments of the present invention will be described clearly and completely with reference to the accompanying drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only some embodiments of the present invention, not all embodiments. Based on the embodiments of the present invention, all other embodiments obtained by a person of ordinary skill in the art without creative efforts belong to the protection scope of the present invention.

Referring to fig. 1-3, the present embodiment is an extraction tank for producing tetradecyl tributyl phosphine chloride, including an outer tank 1 and an inner tank 2, a heating plate 3 is installed between the outer tank 1 and the inner tank 2, a sewage discharge pipe 4 is installed on the inner wall of the bottom of the inner tank 2, the inner wall of the bottom of the inner tank 2 is in a shape of a reversed funnel, a liquid outlet 9 is opened outwards on the bottom inclined plane of the inner tank 2, the other end of the liquid outlet 9 is communicated with a circulating pump 8 through a pipeline, and the model of the circulating pump 8 is IH 50-32-160A-304; rated power: 1.1 kW; the top inner wall of the inner tank body 2 is outwards opened and is equipped with circulation import 6, circulation pipe 7 is installed to the discharge port of circulation pump 8, and circulation pump 8 switches on circulation import 6 through circulation pipe 7, the inside wall of the top of the inner tank body 2 is outwards opened and is equipped with filling tube 5, all corresponding on the top outer wall of filling tube 5 and on the outer wall of blow off pipe 4 installs the valve, filling tube 5 and blow off pipe 4 easily control, fixed mounting has stirring storehouse 10 on the top outer wall of the outer tank body 1, filling tube 5 switches on stirring storehouse 10, the top trompil of stirring storehouse 10 is installed raw materials and is advanced tub 11, and install motor 13 on the top outer wall of stirring storehouse 10, motor 13 adopts E28-400-30-S model, rated power: 0.4 kW; rated voltage: 220V; rated rotation speed/super high rotation speed: 7RPM-1500 RPM; a gear reducer 14 is connected to an output shaft of the motor 13 in a transmission manner, a transmission shaft 15 is arranged in the gear reducer 14, a circular ring plate 12 is fixedly mounted on the side wall of an inner cavity of the stirring bin 10, the bottom end of the transmission shaft 15 extends into the circular ring plate 12, an auxiliary shaft 17 is mounted in the circular ring plate 12 through gear meshing, a main shaft 16 is fixedly mounted on the outer wall of the bottom end of the transmission shaft 15, the top ends of the main shaft 16 and the auxiliary shaft 17 are connected through gear transmission, the bottom ends of the main shaft 16 and the auxiliary shaft 17 are movably connected with the inner wall of the bottom of the stirring bin 10 through bearings, stirring rods 18 are fixedly mounted on the outer walls of the main shaft 16 and the auxiliary shaft 17, the number of the auxiliary shaft 17 is three, the stirring rods 18 are uniformly and annularly and uniformly mounted on the outer walls of the main shaft 16 and the auxiliary shaft 17 from top to bottom; the transmission structure of main shaft 16 and auxiliary shaft 17 sets up rationally, and motor 13 passes through gear reducer 14's the rotational speed that reduces, can drive main shaft 16 and every auxiliary shaft 17 through the meshing of gear simultaneously and rotate, and then can drive every puddler 18 in the stirring storehouse 10 and rotate, has accomplished the high-efficient stirring mixed work to tetradecyl tributyl phosphine chloride extraction raw materials, and overall structure sets up rationally reliably.

When the utility model is used, the motor 13 can be started by an external power supply and a switch, the raw materials for producing tetradecyl tributyl phosphine chloride can be transported into the inner cavity through the raw material inlet pipe 11 at the top of the stirring bin 10, the transmission structure of the stirring bin 10 is reasonable, the motor 13 reduces the rotating speed through the gear reducer 14, the main shaft 16 and each auxiliary shaft 17 can be driven to rotate through the meshing of the top gears of the main shaft 16 and the auxiliary shafts 17, and then each stirring rod 18 in the stirring bin 10 can be driven to rotate, the high-efficiency stirring and mixing work of the raw materials for extracting the tetradecyl tributyl phosphine chloride is completed, during extraction, a valve on the main shaft 5 can be opened for extraction work, the heating plate 3 between the outer tank body 1 and the inner tank body 2 can be electrified for heating work, the sewage liquid for extraction can be discharged from the liquid outlet 9 by the blow-off pipe 4, after the circulating pump 8 is started, the circulating extraction is carried out, and finally, the sewage is discharged from the sewage discharge pipe 4 and collected.

In the description herein, references to the description of "one embodiment," "an example," "a specific example," etc., mean that a particular feature, structure, material, or characteristic described in connection with the embodiment or example is included in at least one embodiment or example of the invention. In this specification, the schematic representations of the terms used above do not necessarily refer to the same embodiment or example. Furthermore, the particular features, structures, materials, or characteristics described may be combined in any suitable manner in any one or more embodiments or examples.

The preferred embodiments of the present invention disclosed above are intended only to help illustrate the present invention. The preferred embodiments are not exhaustive and do not limit the invention to the precise embodiments disclosed. Obviously, many modifications and variations are possible in light of the above teaching. The embodiments were chosen and described in order to best explain the principles of the invention and its practical applications, to thereby enable others skilled in the art to best understand the invention for and utilize the invention. The present invention is limited only by the claims and their full scope and equivalents.

Claims

1. The utility model provides a production of tetradecyl tributyl phosphine chloride is with extraction jar, includes outer jar of body (1) and inner tank body (2), its characterized in that: a heating plate (3) is installed between the outer tank body (1) and the inner tank body (2), a blow-off pipe (4) is installed on the bottom inner wall of the inner tank body (2), the bottom inner wall of the inner tank body (2) is arranged in a reversed hopper shape, a liquid outlet (9) is arranged on the bottom inclined plane of the inner tank body (2) outwards, a circulating pump (8) is connected to the other end of the liquid outlet (9) through a pipeline, a circulating inlet (6) is arranged on the top inner wall of the inner tank body (2) outwards, a circulating pipe (7) is installed at the discharge port of the circulating pump (8), the circulating pump (8) is connected with the circulating inlet (6) through the circulating pipe (7), a feeding pipe (5) is arranged on the top inner wall of the inner tank body (2) outwards, a stirring bin (10) is fixedly installed on the top outer wall of the outer tank body (1), the, a raw material inlet pipe (11) is arranged on a hole at the top of the stirring bin (10), a motor (13) is arranged on the outer wall of the top of the stirring bin (10), an output shaft of the motor (13) is connected with a gear reducer (14) in a transmission way, a transmission shaft (15) is arranged in the gear reducer (14), a circular ring plate (12) is fixedly arranged on the side wall of the inner cavity of the stirring bin (10), the bottom end of the transmission shaft (15) extends into a circular plate (12), an auxiliary shaft (17) is arranged in the circular plate (12) through gear engagement, a main shaft (16) is fixedly arranged on the outer wall of the bottom end of the transmission shaft (15), the top ends of the main shaft (16) and the auxiliary shaft (17) are in transmission connection through a gear, the bottom ends of the main shaft (16) and the auxiliary shaft (17) are movably connected with the inner wall of the bottom of the stirring bin (10) through a bearing, and stirring rods (18) are fixedly arranged on the outer walls of the main shaft (16) and the auxiliary shaft (17).

2. The extraction tank for producing tetradecyltributylphosphonium chloride according to claim 1, wherein the extraction tank comprises: the number of the auxiliary shafts (17) is three, and the auxiliary shafts are annularly and equally arranged on the outer side of the main shaft (16).

3. The extraction tank for producing tetradecyltributylphosphonium chloride according to claim 2, wherein the extraction tank comprises: the stirring rods (18) are respectively and evenly arranged on the outer walls of the main shaft (16) and the auxiliary shaft (17) from top to bottom in sequence.

4. The extraction tank for producing tetradecyltributylphosphonium chloride according to claim 3, wherein the extraction tank comprises: the stirring rods (18) on the main shaft (16) and the auxiliary shaft (17) are arranged in a vertically staggered manner.

5. The extraction tank for producing tetradecyltributylphosphonium chloride according to claim 1, wherein the extraction tank comprises: and valves are correspondingly arranged on the outer wall of the top of the feeding pipe (5) and the outer wall of the sewage discharge pipe (4).