CN207266850U - A kind of polyphosphoric acids reaction kettle monitored in real time - Google Patents
A kind of polyphosphoric acids reaction kettle monitored in real time Download PDFInfo
- Publication number
- CN207266850U CN207266850U CN201720983441.7U CN201720983441U CN207266850U CN 207266850 U CN207266850 U CN 207266850U CN 201720983441 U CN201720983441 U CN 201720983441U CN 207266850 U CN207266850 U CN 207266850U
- Authority
- CN
- China
- Prior art keywords
- autoclave body
- reaction kettle
- real time
- monitored
- polyphosphoric acids
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 229920000137 polyphosphoric acid Polymers 0.000 title claims abstract description 22
- 239000010453 quartz Substances 0.000 claims abstract description 24
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims abstract description 24
- 238000003756 stirring Methods 0.000 claims abstract description 10
- 239000007787 solid Substances 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 description 7
- 238000001816 cooling Methods 0.000 description 4
- 238000013461 design Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000000203 mixture Substances 0.000 description 2
- 238000012544 monitoring process Methods 0.000 description 2
- 239000000376 reactant Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 238000013459 approach Methods 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 230000006837 decompression Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 210000004907 gland Anatomy 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000011897 real-time detection Methods 0.000 description 1
- 238000012546 transfer Methods 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Landscapes
- Physical Or Chemical Processes And Apparatus (AREA)
- Treatment Of Sludge (AREA)
Abstract
The utility model discloses a kind of polyphosphoric acids reaction kettle monitored in real time, including autoclave body and upper cover, the outer surface of the autoclave body is equipped with fixed frame, the inner surface of the autoclave body is equipped with agitating shaft, the side of the autoclave body is equipped with quartz cover, the inner surface of the quartz cover is equipped with endoscope, the side of the endoscope is equipped with controller, the side of the controller is equipped with display, the opposite side of the autoclave body is equipped with exhaust pipe, the side of the exhaust pipe is equipped with control valve, and the top of the upper cover is equipped with stirring motor, and the side of the charge door is equipped with pressure gauge.A kind of polyphosphoric acids reaction kettle monitored in real time described in the utility model, equipped with quartz cover, endoscope and exhaust pipe, reaction solution and observer can be isolated, and the response situation in energy remote observation reaction kettle, the gas that discharge produces in time, the suitable of pressure is maintained, different operating situation is applicable in, brings more preferable prospect of the application.
Description
Technical field
Reaction kettle field is the utility model is related to, more particularly to a kind of polyphosphoric acids reaction kettle monitored in real time.
Background technology
The broad understanding of reaction kettle has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter
Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.Reaction kettle is by autoclave body, kettle cover, chuck, stirring
Device, transmission device, gland seal device, supporting etc. form.Whipped form generally has anchor formula, paddle, turbine type, push type or frame
Deng agitating device can use multiple impellers leaf when ratio of height to diameter is larger, also can arbitrarily be matched according to the requirement of user.And in kettle
Chuck is set outside wall, or heat-transfer surface is set in device, can also be exchanged heat by outer circulation.Mode of heating has electrical heating, hot water
Heating, conduction oil circulating-heating, Far-infrared Heating, outer (interior) coil pipe heating etc., the type of cooling is chuck cooling and kettle inner coil pipe
Cooling, form of stirrer paddle etc..Fulcrum bearing has supporting type or hanging support etc..Rotating speed preferably uses gear more than more than 160 turns
Gear reducer, the number of openings, specification or other requirements can require design according to user, make.
Existing polyphosphoric acids reaction kettle when in use there are it is certain the drawbacks of, it is impossible in real time detection reaction carry out degree
And in reaction kettle mixture situation, for have gas produce reaction cannot timely row pressure, to polyphosphoric acids reaction kettle
Using certain influence is brought, for this reason, a kind of it is proposed that polyphosphoric acids reaction kettle monitored in real time.
Utility model content
The main purpose of the utility model is that providing a kind of polyphosphoric acids reaction kettle monitored in real time, can effectively solve
Certainly in background technology the problem of.
To achieve the above object, the technical solution that the utility model is taken is：
A kind of polyphosphoric acids reaction kettle monitored in real time, including autoclave body and upper cover, the outer surface of the autoclave body are equipped with admittedly
Determine frame, the bottom of the autoclave body is equipped with slag-drip opening, and the inner surface of the autoclave body is equipped with agitating shaft, and the outer surface of agitating shaft is equipped with
Agitator arm, the side of the autoclave body are equipped with quartz cover, and the inner surface of the quartz cover is equipped with endoscope, and the one of the endoscope
Side is equipped with controller, and the side of the controller is equipped with display, and the opposite side of the autoclave body is equipped with exhaust pipe, the exhaust pipe
Side be equipped with control valve, the outer surface of the upper cover is equipped with charge door and temperature-measuring port, and the lower section of temperature-measuring port is equipped with thermometer,
The top of the upper cover is equipped with stirring motor, and the side of the charge door is equipped with pressure gauge, and the outside of the upper cover, which is equipped with, to be fixed
Flange, the autoclave body are fixedly connected with upper cover.
Preferably, the agitator arm is fixedly connected by agitating shaft with stirring motor.
Preferably, the quartz cover is fixedly connected by autoclave body with fixed frame.
Preferably, the upper cover is fixedly connected with mounting flange.
Preferably, the endoscope is fixedly connected by controller with display.
Preferably, the control valve is fixedly connected by exhaust pipe with autoclave body.
Compared with prior art, the utility model has the advantages that：The polyphosphoric acids that can be monitored in real time reacts
Kettle, using quartz cover is equipped with the side of autoclave body, the inner surface of quartz cover is equipped with endoscope, and the side of the endoscope is equipped with control
Device processed, the side of controller are equipped with display, and when the time that reaction carries out is longer and the carry out of reaction is steady, operator exists
Reaction kettle looks on the waste surveyed and cause manpower, and quartz cover has the advantages that translucency is good, and the performance of the acid-fast alkali-proof of quartz
Excellent, quartz cover can be used as good isolated part, prevent mixed liquor from damaging endoscope, and endoscope can detect instead in real time
The response situation in kettle is answered, signal or image are sent to by display by controller, display can be connected with computer
Get up, it is possible to achieve it can not equally observe the carry out degree of reaction at any time at the scene of experiment, save manpower, can in pressure gauge
To detect the pressure of reaction kettle, for the reaction for thering is gas to produce, if cannot timely row pressure, the pressure in autoclave body can be increasingly
Greatly, it may reach and react parallel and suppress being normally carried out for reaction, by opening control valve gas can be realized from exhaust pipe
Discharge, maintain reaction kettle in pressure stablize, whole device is simple, easy to operate, real time monitoring and decompression effect relative to
Traditional approach is more preferable.
Brief description of the drawings
Fig. 1 is a kind of overall structure diagram of the polyphosphoric acids reaction kettle monitored in real time of the utility model.
Fig. 2 is a kind of partial view of the polyphosphoric acids reaction kettle monitored in real time of the utility model.
In figure：1st, autoclave body；2nd, fixed frame；3rd, slag-drip opening；4th, agitating shaft；5th, agitator arm；6th, quartz cover；7th, endoscope；
8th, controller；9th, display；10th, exhaust pipe；11st, control valve；12nd, temperature-measuring port；13rd, thermometer；14th, stirring motor；15th, on
Lid；16th, charge door；17th, mounting flange；18th, pressure gauge.
Embodiment
To make the technical means, creative features, achievable purpose and effectiveness that the utility model is realized easy to understand, below
With reference to embodiment, the utility model is expanded on further.
As shown in Figs. 1-2, a kind of polyphosphoric acids reaction kettle monitored in real time, including autoclave body 1 and upper cover 15, the autoclave body
1 outer surface is equipped with fixed frame 2, and the bottom of the autoclave body 1 is equipped with slag-drip opening 3, and the inner surface of the autoclave body 1 is equipped with agitating shaft 4,
And the outer surface of agitating shaft 4 is equipped with agitator arm 5, the side of the autoclave body 1 is equipped with quartz cover 6, the inner surface of the quartz cover 6
Equipped with endoscope 7, the side of the endoscope 7 is equipped with controller 8, and the side of the controller 8 is equipped with display 9, the kettle
The opposite side of body 1 is equipped with exhaust pipe 10, and the side of the exhaust pipe 10 is equipped with control valve 11, and the outer surface of the upper cover 15 is equipped with
Charge door 16 and temperature-measuring port 12, and the lower section of temperature-measuring port 12 is equipped with thermometer 13, the top of the upper cover 15 is equipped with stirring motor
14, the side of the charge door 16 is equipped with pressure gauge 18, and the outside of the upper cover 15 is equipped with mounting flange 17,1 He of autoclave body
Upper cover 15 is fixedly connected.
Wherein, the agitator arm 5 is fixedly connected by agitating shaft 5 with stirring motor 14.
Wherein, the quartz cover 6 is fixedly connected by autoclave body 1 with fixed frame 2.
Wherein, the upper cover 15 is fixedly connected with mounting flange 17.
Wherein, the endoscope 7 is fixedly connected by controller 8 with display 9.
Wherein, the control valve 11 is fixedly connected by exhaust pipe 10 with autoclave body 1.It should be noted that the utility model
For a kind of polyphosphoric acids reaction kettle monitored in real time, when in use, reactant is placed in autoclave body 1, upper cover 15 is closed and opens
Opening stirring motor 14 makes agitator arm 5 start to work, and being stirred liquid is uniformly mixed reactant, is equipped with the side of autoclave body 1
Quartz cover 6, the inner surface of quartz cover 6 are equipped with endoscope 7, and the side of the endoscope 7 is equipped with controller 8, the side of controller 8
Equipped with display 9, when the time that reaction carries out is longer and the carry out of reaction is steady, operator looks on survey in reaction kettle and causes
The waste of manpower, quartz cover 6 have the advantages that translucency is good, and the excellent performance of the acid-fast alkali-proof of quartz, quartz cover 6 can be with
Used as good isolated part, prevent mixed liquor from damaging endoscope 7, endoscope 7 can detect the reaction in reaction kettle in real time
Situation, is sent to display 9 by signal or image by controller 8, can connect display 9 and computer, can be with
The carry out degree of reaction can not equally be observed at any time at the scene of experiment by realizing, saved manpower, be equipped with the side of upper cover 15
Pressure gauge 18, the opposite side of autoclave body 1 are equipped with exhaust pipe 10, and the side of exhaust pipe 10 is equipped with control valve 11, and pressure gauge 18 can be examined
Survey the pressure of reaction kettle, for the reaction for thering is gas to produce, if cannot timely row pressure, the pressure in autoclave body 1 can be increasing, can
It can reach and react parallel and suppress being normally carried out for reaction, by opening control valve 11 gas can be realized from 10 row of exhaust pipe
Go out, maintain the pressure in reaction kettle to stablize, it is more practical.A kind of polyphosphoric acids for monitoring in real time described in the utility model is anti-
Kettle is answered, equipped with quartz cover 6, endoscope 7 and exhaust pipe 10, reaction solution and observer can be isolated, and energy remote observation is anti-
The response situation in kettle is answered, the gas that discharge produces in time, maintains the suitable of pressure, is applicable in different operating situation, brings more preferable
Prospect of the application.
The advantages of basic principle and main feature and the utility model of the utility model has been shown and described above.One's own profession
The technical staff of industry is it should be appreciated that the present utility model is not limited to the above embodiments, described in above embodiments and description
Simply illustrate the utility model principle, on the premise of not departing from the spirit and scope of the utility model, the utility model is also
Various changes and modifications are had, these various changes and improvements fall within the scope of the claimed invention.The utility model
Claimed scope is defined by the appending claims and its equivalent thereof.
Claims (6)
1. a kind of polyphosphoric acids reaction kettle monitored in real time, including autoclave body (1) and upper cover (15), it is characterised in that：The kettle
The outer surface of body (1) is equipped with fixed frame (2), and the bottom of the autoclave body (1) is equipped with slag-drip opening (3), the inner surface of the autoclave body (1)
Equipped with agitating shaft (4), and the outer surface of agitating shaft (4) is equipped with agitator arm (5), and the side of the autoclave body (1) is equipped with quartz cover
(6), the inner surface of the quartz cover (6) is equipped with endoscope (7), and the side of the endoscope (7) is equipped with controller (8), described
The side of controller (8) is equipped with display (9), and the opposite side of the autoclave body (1) is equipped with exhaust pipe (10), the exhaust pipe (10)
Side be equipped with control valve (11), the outer surface of the upper cover (15) is equipped with charge door (16) and temperature-measuring port (12), and temperature-measuring port
(12) lower section is equipped with thermometer (13), and the top of the upper cover (15) is equipped with stirring motor (14), the charge door (16)
Side is equipped with pressure gauge (18), and the outside of the upper cover (15) is equipped with mounting flange (17), and the autoclave body (1) and upper cover (15) are solid
Fixed connection.
A kind of 2. polyphosphoric acids reaction kettle monitored in real time according to claim 1, it is characterised in that：The paddle
Wheel (5) is fixedly connected by agitating shaft (4) with stirring motor (14).
A kind of 3. polyphosphoric acids reaction kettle monitored in real time according to claim 1, it is characterised in that：The quartz cover
(6) it is fixedly connected by autoclave body (1) with fixed frame (2).
A kind of 4. polyphosphoric acids reaction kettle monitored in real time according to claim 1, it is characterised in that：The upper cover
(15) it is fixedly connected with mounting flange (17).
A kind of 5. polyphosphoric acids reaction kettle monitored in real time according to claim 1, it is characterised in that：The endoscope
(7) it is fixedly connected by controller (8) with display (9).
A kind of 6. polyphosphoric acids reaction kettle monitored in real time according to claim 1, it is characterised in that：The control valve
(11) it is fixedly connected by exhaust pipe (10) with autoclave body (1).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720983441.7U CN207266850U (en) | 2017-08-08 | 2017-08-08 | A kind of polyphosphoric acids reaction kettle monitored in real time |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720983441.7U CN207266850U (en) | 2017-08-08 | 2017-08-08 | A kind of polyphosphoric acids reaction kettle monitored in real time |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207266850U true CN207266850U (en) | 2018-04-24 |
Family
ID=61960255
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720983441.7U Expired - Fee Related CN207266850U (en) | 2017-08-08 | 2017-08-08 | A kind of polyphosphoric acids reaction kettle monitored in real time |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207266850U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116726857A (en) * | 2023-08-14 | 2023-09-12 | 烟台百川汇通科技有限公司 | Reaction kettle for preparing anthraquinone hydrogenation catalyst |
-
2017
- 2017-08-08 CN CN201720983441.7U patent/CN207266850U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN116726857A (en) * | 2023-08-14 | 2023-09-12 | 烟台百川汇通科技有限公司 | Reaction kettle for preparing anthraquinone hydrogenation catalyst |
| CN116726857B (en) * | 2023-08-14 | 2023-10-10 | 烟台百川汇通科技有限公司 | Reaction kettle for manufacturing anthraquinone hydrogenation catalyst |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180424 |