CN207187759U - A kind of solubility and viscosity measurements reactor - Google Patents
A kind of solubility and viscosity measurements reactor Download PDFInfo
- Publication number
- CN207187759U CN207187759U CN201721221541.2U CN201721221541U CN207187759U CN 207187759 U CN207187759 U CN 207187759U CN 201721221541 U CN201721221541 U CN 201721221541U CN 207187759 U CN207187759 U CN 207187759U
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- kettle
- inner cylinder
- reactor
- agitator
- sapphire
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Abstract
The utility model discloses a kind of solubility and viscosity measurements reactor, include kettle and the viewing window being arranged on the front side outer wall of kettle, the agitator connected with kettle is provided with the top of kettle, the pressure gauge connected with kettle, intake valve, rupture disk and air bleeding valve are respectively arranged with around agitator, the inside of kettle sets gradually Packed quartzy inner cylinder and sapphire inner cylinder from outside to inside, heating region is provided between quartzy inner cylinder and sapphire inner cylinder, the bottom of quartzy inner cylinder and sapphire inner cylinder is equipped with autoclave bottom.Overall structure is simple, and floor space is small, and manufacturing cost is low, can be heated by being passed through deep fat in heating region during use, and heating is quick, safe；By being embedded with viscosimeter in the intermediate region at autoclave bottom, the viscosity and solubility of material can be detected simultaneously, better meet the use demand of people.
Description
Technical field
Chemical industry measurement equipment technical field is the utility model is related to, is reacted more particularly, to a kind of solubility and viscosity measurements
Kettle.
Background technology
The broad understanding of reactor has the container physically or chemically reacted, is matched somebody with somebody by the structure design to container with parameter
Put, realize the mixture function of the heating of technological requirement, evaporation, cooling and low high speed.Reactor be widely used in oil, chemical industry,
Rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrifying, hydrogenating, hydrocarbonylation, polymerization, the pressure of the technical process such as condensation
Force container, such as reactor, reaction pot, decomposition pot, polymeric kettle etc..Reactor is filled by kettle, kettle cover, chuck, agitator, transmission
Put, gland seal device, the composition such as supporting.Agitating device can use multiple impellers leaf when ratio of height to diameter is larger, also can be according to user's
It is required that any apolegamy.Chuck is set outside kettle wall, or heat-transfer surface is set in device, can also be exchanged heat by outer circulation.Fulcrum bearing
There are supporting type or hanging support etc..Rotating speed preferably used more than more than 160 turns gear reduction unit the number of openingss, specification or it is other will
Design can be required according to user, make by asking.Existing reactor is mostly complicated, and floor space is big, and manufacturing cost is high, safety
Property it is poor, and the solubility and viscosity of material can not be detected simultaneously, it is impossible to preferably meet use demand.
Utility model content
Problem to be solved in the utility model be to provide it is a kind of it is simple in construction, floor space is small, manufacturing cost is low, security
It is high and can be simultaneously to the reactor of solubility, viscosity measurements.
In order to solve the above technical problems, the technical solution adopted in the utility model is：A kind of solubility and viscosity measurements are anti-
Answer kettle, include kettle and the viewing window being arranged on the front side outer wall of the kettle, be provided with the top of the kettle with
The agitator of kettle connection, be respectively arranged with around the agitator pressure gauge connected with the kettle, intake valve,
Rupture disk and air bleeding valve, the inside of the kettle set gradually Packed quartzy inner cylinder and sapphire inner cylinder, institute from outside to inside
State the bottom that heating region, the quartzy inner cylinder and the sapphire inner cylinder are provided between quartzy inner cylinder and the sapphire inner cylinder
Portion is equipped with autoclave bottom, and the intermediate region at the autoclave bottom is embedded with viscosimeter.
Preferably, above-mentioned a kind of solubility and viscosity measurements reactor, wherein the company of the agitator and the kettle
The place of connecing is provided with sealing device, and the sealing device is fixed by gripping mechanism.
Preferably, above-mentioned a kind of solubility and viscosity measurements reactor, wherein being provided with temperature in the sapphire inner cylinder
Degree probe, the power connection of the temp probe pass from the agitator.
Preferably, above-mentioned a kind of solubility and viscosity measurements reactor, wherein side of the viscosimeter to be threadedly coupled
Formula is detachably connected with the autoclave bottom.
Preferably, above-mentioned a kind of solubility and viscosity measurements reactor, wherein the lower end of the agitator is provided with and stirred
Axle is mixed, the agitating shaft is arranged on the inside of the sapphire inner cylinder.
The utility model has the advantage that is with beneficial effect：The agitator connected with kettle is provided with the top of kettle,
It is respectively arranged with the pressure gauge connected with kettle, intake valve, rupture disk and air bleeding valve around agitator, the inside of kettle is from outer
Packed quartzy inner cylinder and sapphire inner cylinder are inwardly set gradually, heating zone is provided between quartzy inner cylinder and sapphire inner cylinder
Domain, the bottom of quartzy inner cylinder and sapphire inner cylinder are equipped with autoclave bottom.Overall structure is simple, and floor space is small, manufacture
Cost is low, can be heated by being passed through deep fat in heating region during use, and heating is quick, safe；By in high pressure
The intermediate region of bottom is embedded with viscosimeter, the viscosity and solubility of material can be detected simultaneously, better meet people
Use demand.
Brief description of the drawings
Fig. 1 is overall structure diagram of the present utility model；
Fig. 2 is front view of the present utility model；
Fig. 3 is top view of the present utility model；
Fig. 4 is left view of the present utility model；
Fig. 5 is along the cross section structure schematic diagram at E-E in Fig. 4；
Fig. 6 is the partial enlarged drawing at A in Fig. 5.
In figure：1st, kettle；2nd, viewing window；3rd, agitator；4th, pressure gauge；5th, intake valve；6th, rupture disk；7th, air bleeding valve；8、
Temp probe；9th, sealing device；10th, gripping mechanism；11st, sapphire inner cylinder；12nd, quartzy inner cylinder；13rd, heating region；14th, stir
Axle；15th, viscosimeter；16th, autoclave bottom.
Embodiment
In order that the purpose of this utility model, technical scheme and advantage are more clearly understood, below in conjunction with accompanying drawing and implementation
Example, below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out it is clear,
It is fully described by, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole implementation
Example.Based on the embodiment in the utility model, those of ordinary skill in the art are obtained under the premise of creative work is not made
The every other embodiment obtained, belong to the scope of the utility model protection.
As shown in Figure 1, Figure 2 and Figure 3, a kind of solubility and viscosity measurements reactor, include kettle 1 and be arranged on kettle
Viewing window 2 on the front side outer wall of body 1, viewing window 2 are made up of acrylic panel, can pass through viewing window 2 during work and observe kettle 1
Internal response situation, the top of kettle 1 are provided with the agitator 3 connected with kettle 1, and the junction of agitator 3 and kettle 1 is set
Sealing device 9 is equipped with, sealing device 9 is fixed by gripping mechanism 10, and the lower end of agitator 3 is provided with agitating shaft 14, work
Agitating shaft 14 can be stirred to material when making, be easy to hybrid reaction more fully, be respectively arranged with around agitator 3 and kettle
Pressure gauge 4, intake valve 5, rupture disk 6 and the air bleeding valve 7 that body 1 connects, pressure gauge 4 can monitor the pressure inside kettle 1, intake valve
5 and air bleeding valve 7 can control air inlet and outlet in kettle 1 respectively, and rupture disk 6 can then prevent the too high pressure of kettle 1 and
Explode, security is higher.
As shown in Figure 4, Figure 5 and Figure 6, the inside of kettle 1 sets gradually Packed quartzy inner cylinder 12 and indigo plant from outside to inside
Jewel inner cylinder 11, heating region 13 is provided between quartzy inner cylinder 12 and sapphire inner cylinder 11, wherein material is in sapphire inner cylinder
Being reacted in 11, agitating shaft 14 is arranged on the inside of sapphire inner cylinder 11, and temp probe 8 is provided with sapphire inner cylinder 11,
The power connection of temp probe 8 passes from agitator 3, and temp probe 8 can be with temperature in at-once monitor sapphire inner cylinder 11
Size, the bottom of quartzy inner cylinder 12 and sapphire inner cylinder 11 are equipped with autoclave bottom 16, the intermediate region at autoclave bottom 16
Viscosimeter 15 is embedded with, viscosimeter 15 is detachably connected with autoclave bottom 16 threadably.
It can be heated during use by being passed through deep fat in heating region 13, heating is quick, safe；By in height
The intermediate region of pressure bottom 16 is embedded with viscosimeter 15, and the viscosity and solubility of material can be detected simultaneously, preferably full
The use demand of sufficient people.
In description of the present utility model, it is to be understood that the indicating position such as term " on ", " under ", "left", "right" or
Position relationship is based on orientation shown in the drawings or position relationship, is for only for ease of description the utility model and simplifies description,
Rather than the device or element of instruction or hint meaning must have specific orientation and specific azimuth configuration and operation,
It is thus impossible to it is interpreted as to limitation of the present utility model.In addition, " first ", " second " are merely due to describe purpose, and be not understood that
To indicate or implying relative importance or the implicit quantity for indicating indicated technical characteristic.Therefore, define " first ",
One or more this feature can be expressed or be implicitly included to the feature of " second ".In description of the present utility model, unless
It is otherwise noted, " multiple " are meant that two or more.
, it is necessary to illustrate in description of the present utility model, unless otherwise clearly defined and limited, term " installation "
" connected " " connection " etc. should be interpreted broadly, for example, it may be being fixedly connected or being detachably connected, or integratedly be connected
Connect；Can be mechanical connection or electrical connection；Can be joined directly together, can also be indirectly connected with by intermediary, can
To be the connection of two element internals.For the ordinary skill in the art, above-mentioned term can be understood with concrete condition
Concrete meaning in the utility model.
One embodiment of the present utility model is described in detail above, but the content is only of the present utility model
Preferred embodiment, it is impossible to be considered as being used to limit practical range of the present utility model.It is all to be made according to present utility model application scope
Equivalent change with improve etc., all should still belong within patent covering scope of the present utility model.
Claims (5)
1. a kind of solubility and viscosity measurements reactor, include kettle（1）And it is arranged on the kettle（1）Front side outer wall
On viewing window（2）, it is characterised in that：The kettle（1）Top be provided with and the kettle（1）The agitator of connection（3）,
The agitator（3）Around be respectively arranged with and the kettle（1）The pressure gauge of connection（4）, intake valve（5）, rupture disk（6）
And air bleeding valve（7）, the kettle（1）Inside set gradually Packed quartzy inner cylinder from outside to inside（12）With sapphire inner cylinder
（11）, the quartzy inner cylinder（12）With the sapphire inner cylinder（11）Between be provided with heating region（13）, the quartzy inner cylinder
（12）With the sapphire inner cylinder（11）Bottom be equipped with autoclave bottom（16）, the autoclave bottom（16）Middle area
Domain is embedded with viscosimeter（15）.
2. a kind of solubility according to claim 1 and viscosity measurements reactor, it is characterised in that：The agitator（3）
With the kettle（1）Junction be provided with sealing device（9）, the sealing device（9）Pass through gripping mechanism（10）Consolidate
It is fixed.
3. a kind of solubility according to claim 1 and viscosity measurements reactor, it is characterised in that：The sapphire inner cylinder
（11）Inside it is provided with temp probe（8）, the temp probe（8）Power connection from the agitator（3）In pass.
4. a kind of solubility according to claim 1 and viscosity measurements reactor, it is characterised in that：The viscosimeter（15）
Threadably with the autoclave bottom（16）It is detachably connected.
5. a kind of solubility according to claim 1 and viscosity measurements reactor, it is characterised in that：The agitator（3）
Lower end be provided with agitating shaft（14）, the agitating shaft（14）It is arranged on the sapphire inner cylinder（11）Inside.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721221541.2U CN207187759U (en) | 2017-09-22 | 2017-09-22 | A kind of solubility and viscosity measurements reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721221541.2U CN207187759U (en) | 2017-09-22 | 2017-09-22 | A kind of solubility and viscosity measurements reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207187759U true CN207187759U (en) | 2018-04-06 |
Family
ID=61786798
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721221541.2U Active CN207187759U (en) | 2017-09-22 | 2017-09-22 | A kind of solubility and viscosity measurements reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207187759U (en) |
-
2017
- 2017-09-22 CN CN201721221541.2U patent/CN207187759U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP03 | Change of name, title or address |
Address after: 528300 2 Daliang Road, five Sha Road, Shunde District, Foshan, Guangdong. Patentee after: Guangdong Fu Yan Sheng Technology Co., Ltd. Address before: 528308 2 Daliang Road, five Sha Road, Shunde District, Foshan, Guangdong. Patentee before: Foshan Shunde Fuyansheng Lubricant Co., Ltd. |
|
| CP03 | Change of name, title or address |