CN207243905U - A kind of automatic reactor of lipase - Google Patents
A kind of automatic reactor of lipase Download PDFInfo
- Publication number
- CN207243905U CN207243905U CN201721234198.5U CN201721234198U CN207243905U CN 207243905 U CN207243905 U CN 207243905U CN 201721234198 U CN201721234198 U CN 201721234198U CN 207243905 U CN207243905 U CN 207243905U
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- CN
- China
- Prior art keywords
- microwave
- housing
- wall
- reaction kettle
- temperature sensor
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
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Abstract
The utility model discloses a kind of automatic reactor of lipase, including reaction kettle housing, feed inlet, liquid outlet, heating layer and agitating device, temperature sensor, microwave device, PLC controller and strainer, temperature sensor is on the inner wall of housing, contacted with reaction liquid, microwave device includes microwave and wall, magnetron and microwave source occurs, and microwave occurs wall and is arranged on the inner wall of housing side, passes through the microwave source outside magnetron coupled reaction kettle；Temperature sensor is connected with microwave device with PLC controller；Position inside reaction kettle close to bottom is equipped with strainer, above blender.The utility model automatically controls time and the temperature of each reactions steps by PLC controller combination temperature sensor, liquid level sensor, and accelerates the speed of esterification by microwave device, greatly improves production efficiency, reduces labor intensity.
Description
Technical field
It the utility model is related to fine chemistry industry production field, more particularly to a kind of automatic reactor of lipase.
Background technology
In fine chemistry industry production field, reaction kettle is the common production equipment that sterol refines, and it is more that sterol refines needs addition
Kind material is reacted, and in the prior art, the addition time of each material still manually monitors mostly, the time of reaction and temperature
It is also required to artificially adjust, it is less efficient.And multiple tracks reaction process also needs to a variety of reaction vessels, such as saponification, filtering,
Special container is needed, is taken up an area greatly, it is of high cost.
The content of the invention
The purpose of this utility model is to provide a kind of automatic reactor of lipase, and biology is completed in same reaction kettle
The processes such as automatic fermentation, crystallization, filtering, and reaction speed is accelerated by microwave, the degree of automation is high, and production efficiency is high.
The technical problem that the utility model is solved can be realized using following technical scheme：
A kind of automatic reactor of lipase, including reaction kettle housing, feed inlet, liquid outlet, heating layer and agitating device,
The top of reaction kettle housing is equipped with feed inlet, and lower section is equipped with liquid outlet, is heating layer on the outside of housing, equipped with insulating layer, stirring
Device includes motor and transmission device, agitating shaft and blender, and motor and transmission device are arranged on the exterior center top of housing,
One end of the mixing shaft connects the output shaft of motor and transmission device, and the other end connects blender through intracavitary in housing to reaction kettle,
It is characterized in that：Temperature sensor, microwave device, PLC controller and strainer are further included, the temperature sensor is mounted in housing
Inner wall on, contacted with reaction liquid, the microwave device includes microwave and wall, magnetron and microwave source, the microwave hair occurs
Raw wall is arranged on the inner wall of housing side, passes through the microwave source outside magnetron coupled reaction kettle；The temperature sensor with it is micro-
Wave apparatus is connected with PLC controller；Position inside the reaction kettle close to bottom is equipped with strainer, and the strainer is installed on and stirs
Mix above device.
Preferably, sliding block is provided with the strainer side, inner walls are equipped with guide rail, and the sliding block is sliding on guide rail
Dynamic, the lower end of the guide rail is equipped with limited block.
Preferably, liquid level gauge is further included, the liquid level gauge is installed on inner walls upper end.
Preferably, conductive fluid entrance is equipped with above the heating layer, lower section is exported equipped with conductive fluid.
Preferably, the mouth of pipe of all pipelines is equipped with electrical ball valve, and on and off is beaten by PLC controller control electrical ball valve
Close.
The utility model automatically controls each reactions steps by PLC controller combination temperature sensor, liquid level sensor
Time and temperature, and by the speed of microwave device quickening esterification, greatly improve production efficiency, reduce labor intensity.
Brief description of the drawings
Fig. 1 is the structure diagram of the utility model.
In figure, 1- reaction kettles housing, 2- feed inlets, 3- liquid outlets, 4- heating layers, 5- agitating devices, 6- sensing devices, 7-
Microwave device, 8- strainers, 41- insulating layers, 42- conductive fluids entrance, the outlet of 43- conductive fluids, 51- motors and transmission device, 52- are stirred
Mix axis, 53- blenders, 61- temperature sensors, 62- liquid level gauges, 71- microwaves and wall, 72- magnetrons, 73- microwave sources occurs.
Embodiment
The utility model is described in further detail with reference to embodiment, but the embodiment of the utility model is not
It is limited to this.
As Fig. 1 be the utility model preferred solution, including reaction kettle housing 1, feed inlet 2, liquid outlet 3, heating layer 4,
Agitating device 5, sensing device 6, microwave device 7 and strainer 8.
The shape of reaction kettle is identical with common reaction kettle, can be improved on the basis of original reactor.The top of reaction kettle housing 1
Equipped with feed inlet 2, lower section is equipped with liquid outlet 3.
The outside of housing 1 is heating layer 4, and equipped with insulating layer 41, in the present embodiment, mode of heating is heat-conducting oil heating,
Can be other mode of heatings such as hot water, infrared, microwave, the built-in conduction oil liquid of interlayer between insulating layer 41 and housing 1, on
Side is equipped with the lower section of conductive fluid entrance 42 and is equipped with conductive fluid outlet 43.
Agitating device 5 includes motor and transmission device 51, agitating shaft 52 and blender 53, and motor and transmission device 51 are set
Above the exterior center of housing 1, the output shaft of 52 one end of agitating shaft connection motor and transmission device 51, the other end passes through housing
1 in reaction kettle intracavitary connect blender 53.Blender 53 can be multiple layers of vanes, and the end of agitating shaft 52 is close to intracavity bottom
But do not contact.
Sensing device 6 includes temperature sensor 61 and liquid level gauge 62, and temperature sensor 61 is mounted on the inner wall of housing 1, with
Reaction liquid contacts, for controlling reaction temperature.Liquid level gauge 62 is installed on 1 inner wall upper end of housing, is reached in liquid level and requires numerical value
When send signal.Temperature sensor 61 and liquid level gauge 62 are connected with PLC controller.
Microwave device 7 includes microwave and wall 71, magnetron 72 and microwave source 73 occurs, and microwave occurs wall 71 and is arranged on housing 1
On the inner wall of side, pass through the microwave source 73 outside 72 coupled reaction kettle of magnetron.
Position inside reaction kettle close to bottom is equipped with strainer 8, and the strainer 8 is installed on above blender, and sterol will be through
Cross repeatedly rinsing, dissolution filter, between can be completed in reaction kettle.Sliding block 81 is provided with 8 side of strainer, on 1 inner wall of housing
Equipped with guide rail 82, the sliding block 81 can slide on guide rail 82, and the lower end of guide rail 82 is equipped with limited block 83, and sterol filtering is completed
Afterwards, it is necessary to when taking out, agitating shaft 52 drives blender 53 to rise, while pulls strainer 8 to rise, so that it may which the sterol after filtering is wet
Slag takes out.
In the present embodiment, the mouth of pipe of all pipelines is equipped with electrical ball valve, by the opening of PLC controller control electrical ball valve
And closing.
By taking Hydrolysis kinetics sterol in deodorization distillate as an example, the course of work of the utility model is as follows：
1) deodorization distillate is put into reaction kettle along feed inlet 2, volume ratio is added from another feed inlet 2 is
100:1~1.5（Kg/L or g/ml）, mass concentration is 20~30% aqueous slkali, after the completion of material is launched, motor and transmission dress
Put 51 drive blenders 53 to rotate, stop after liquid in kettle is sufficiently mixed；The electrical ball valve of feed inlet 2 is closed, heating layer 4
Conductive fluid entrance 42 is opened, and is heated to fluid temperature in kettle and is reached 60~70 DEG C of stopping heating, when saponification 2~4 is small, is controlled by PLC
Device control time processed；
2) when saponification time reaches preset time, the electrical ball valve of feed inlet 2 is opened, and input mass ratio is 100:0.5~2
Lipase, it is 100 that mass volume ratio is added in another feed inlet 2:8~20（Kg/L or g/ml）Methanol, reduce heating layer 4
Conductive fluid temperature so that the temperature of reaction kettle is maintained at 20~30 DEG C of low temperature, carries out esterification.Microwave dress is opened at the same time
Put 7, microwave occurs wall 71 and produces microwave assisted esterification, by it is original need 8 it is small when esterification speed-raising to 3 it is small when it is interior,
Esterification is more complete at the same time；The time of PLC controller control reaction, temperature sensor 61 detect the temperature of reaction solution, will
Temperature signal is sent to PLC controller, the opening of PLC controller controller control conductive fluid entrance 42 and conductive fluid outlet 43 and
Close, with heating-up temperature processed；
3) the conductive fluid temperature of heating layer 4 is reduced, allows esterifying liquid slow cooling to 0 ~ 5 DEG C, freezing and crystallizing, growing the grain 7~
After 11 hours, liquid outlet 3 is opened, liquid is discharged and is filtered, it is thick sterol to obtain filter cake；
4) feed inlet 2 is opened after having filtered, is 1 toward the interior mass volume ratio that adds of kettle:2~6（Kg/L or g/ml）Solvent,
The temperature recovery of heating layer 4 to room temperature, motor and transmission device 51 drives blender 53 to rotate, after filter cake stirring rinsing in kettle
Liquid outlet 3 is opened, liquid is discharged and is filtered, PLC controller controls the step, repeats 2 ~ 5 rinsings；
5) mass volume ratio is added after the completion of rinsing as 1:2~6（Kg/L or g/ml）Solvent dissolving filter cake, heating layer
For 4 temperature recovery to 65~90 DEG C, motor and transmission device 51 drive blender 53 to rotate, and filter cake in kettle is stirred to completely molten
Solution；
6) the conductive fluid temperature of heating layer 4 is reduced, allows esterifying liquid slow cooling to 0 ~ 5 DEG C, freezing and crystallizing, growing the grain 7~
After 11 hours, liquid outlet 3 is opened, liquid is discharged and is filtered, it is refined sterol wet slag to obtain filter cake；
7) reaction kettle upper cover is opened, agitating shaft 52 is carried upwards, blender 53 pulls the sliding block 81 of strainer 8, along guide rail 82
Slide, to top after can by strainer 8 sterol wet slag take out.
The utility model is mainly beaten by the step that automatically engages of PLC controller control material, each mouth of pipe electrical ball valve
Switch closes, and the flowing of conductive fluid in the temperature signal control heating layer 4 collected according to temperature sensor 61, the temperature of conductive fluid can
By external heat rod and cooling rod control, while PLC controller controls the either on or off of microwave device, is esterified using microwave assisted
Reaction so that react more complete, the yield higher of sterol.
The above, is only the utility model preferred embodiment, not the technical scope of the utility model is appointed
What is limited, therefore every any trickle amendment made according to technical spirit of the invention to above example, equivalent variations are with repairing
Decorations, still fall within the scope of protection of the utility model.
Claims (5)
1. a kind of automatic reactor of lipase, including reaction kettle housing, feed inlet, liquid outlet, heating layer and agitating device, instead
The top of still shell body is answered to be equipped with feed inlet, lower section is equipped with liquid outlet, is heating layer on the outside of housing, equipped with insulating layer, stirring dress
Put and be arranged on above the exterior center of housing, stir including motor and transmission device, agitating shaft and blender, motor and transmission device
The output shaft of axis one end connection motor and transmission device is mixed, the other end connects blender through intracavitary in housing to reaction kettle, its
It is characterized in that：Temperature sensor, microwave device, PLC controller and strainer are further included, the temperature sensor is mounted in housing
On inner wall, contacted with reaction liquid, the microwave device includes microwave and wall, magnetron and microwave source occurs, and the microwave occurs
Wall is arranged on the inner wall of housing side, passes through the microwave source outside magnetron coupled reaction kettle；The temperature sensor and microwave
Device is connected with PLC controller；Position inside the reaction kettle close to bottom is equipped with strainer, and the strainer is installed on stirring
Above device.
A kind of 2. automatic reactor of lipase according to claim 1, it is characterised in that：Set on the strainer side
There is sliding block, inner walls are equipped with guide rail, and the sliding block slides on guide rail, and the lower end of the guide rail is equipped with limited block.
A kind of 3. automatic reactor of lipase according to claim 1, it is characterised in that：Liquid level gauge is further included, it is described
Liquid level gauge is installed on inner walls upper end.
A kind of 4. automatic reactor of lipase according to claim 1, it is characterised in that：It is equipped with above the heating layer
Conductive fluid entrance, lower section are exported equipped with conductive fluid.
A kind of 5. automatic reactor of lipase according to one of claim 1-4, it is characterised in that：The pipe of all pipelines
Mouth is equipped with electrical ball valve, by the opening and closing of PLC controller control electrical ball valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721234198.5U CN207243905U (en) | 2017-09-25 | 2017-09-25 | A kind of automatic reactor of lipase |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721234198.5U CN207243905U (en) | 2017-09-25 | 2017-09-25 | A kind of automatic reactor of lipase |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207243905U true CN207243905U (en) | 2018-04-17 |
Family
ID=61886857
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721234198.5U Expired - Fee Related CN207243905U (en) | 2017-09-25 | 2017-09-25 | A kind of automatic reactor of lipase |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207243905U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113248120A (en) * | 2020-02-11 | 2021-08-13 | 深圳市绎立锐光科技开发有限公司 | Production equipment for preparing glass by sol-gel method and related preparation method |
-
2017
- 2017-09-25 CN CN201721234198.5U patent/CN207243905U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113248120A (en) * | 2020-02-11 | 2021-08-13 | 深圳市绎立锐光科技开发有限公司 | Production equipment for preparing glass by sol-gel method and related preparation method |
| CN113248120B (en) * | 2020-02-11 | 2023-12-22 | 深圳市绎立锐光科技开发有限公司 | Production equipment for preparing glass by sol-gel method and related preparation method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180417 |