CN207232016U - Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked - Google Patents

Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked Download PDF

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Publication number
CN207232016U
CN207232016U CN201721224975.8U CN201721224975U CN207232016U CN 207232016 U CN207232016 U CN 207232016U CN 201721224975 U CN201721224975 U CN 201721224975U CN 207232016 U CN207232016 U CN 207232016U
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China
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cigarette
triple valve
absorption cell
laser
flue gas
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CN201721224975.8U
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邓楠
邢昆明
张柯
计敏
张明建
王乐
李志刚
王金棒
王安
刘勇
李斌
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Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
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Hefei Institutes of Physical Science of CAS
Zhengzhou Tobacco Research Institute of CNTC
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Abstract

Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked is the utility model is related to, which includes integrated gases absorption cell and connected flue gas suction trapping system, nitrogen purge system, pumped vacuum systems and photodetector system.By the device can measure respectively cigarette it is unignited and light suction after under test gas concentration, remake difference, you can obtain the oxygen demand that cigarette burns and sucks a bite.Carry out multiple continuous sucking, you can reach that cigarette burns and sucks by mouth oxygen demand.The utility model is rational in infrastructure, easy to operate, and when test is pollution-free, and strong antijamming capability, non-contact, real-time is good.

Description

Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked
Technical field
The detection of combustion product gases is the utility model is related to, is specifically oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked.
Background technology
In aspiration procedure, a series of physical and chemical reaction occurs cigarette for pipe tobacco, forms substantial amounts of product, there is 5000 It is a variety of.Wherein harmful components have 149 kinds, including tar, and CO, nitrosamine, aldehyde and nitro hydrocarbon etc., they there is harm to make human body With.Smoking is harmful to your health, although the theory of tobacco control is constantly being promoted, but still has many people smoking.In order to reduce cigarette smoking During harmful substance yield, study during cigarette smoking influence harmful substance produce factor become to close weight Will.The harmful substance major part that cigarette smoking produces by the macromolecular compound imperfect combustion in tobacco and is cracked to form, cigarette Careless unique nitrosamine is by being that tobacco physical action produces, and such reaction and the heat that is produced in aspiration procedure are closely related, again Due to the oxygen positive correlation consumed in reaction quantity of heat production and aspiration procedure.And oxygen consumption is more, quantity of heat production is bigger, reaction Ground is more abundant, and the number of cigarette burning oxygen demand can reflect in cigarette combustion process the size of the completeness reacted.Therefore, grind Study carefully the oxygen demand during cigarette smoking have to the extent of reaction for studying cigarette and the yield for reducing harmful substance it is important Researching value.
Mass spectrography has the advantages that high sensitivity, detection speed are fast, but if do not carried out pre-treatment to cigarette smoke, quantitative Easily disturbed during analysis be subject to other materials ionization fragment in cigarette mainstream flue gas, be difficult to accurately realize quantitative detection.It is adjustable Humorous diode laser absorption spectrum(TDLAS)Technology can effectively exclude other due to the high-resolution characteristic using laser The absorption interference of material, has the advantages that strong antijamming capability, high sensitivity, fast response time and cost-effective, is that one kind exists The effective technology means of detection are realized under complicated gas condition.
The content of the invention
The purpose of this utility model is based on above-mentioned prior art situation, for research cigarette burns and sucks oxygen consumption quantifier elimination Oxygen consumption amount detecting device during a kind of cigarette provided is burnt and sucked, is oxygen demand when can be achieved to burn and suck cigarette using the device Measure.
The purpose of this utility model is achieved through the following technical solutions:
Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked, including integrated gases absorption cell and with the integrated form gas Flue gas suction trapping system, nitrogen purge system, pumped vacuum systems and the photodetector system that body absorption cell is connected.
The flue gas suction trapping system includes passing through the cigarette holder of pipeline connection, triple valve b, filter disc, cigarette successively Gas pump unit, servomotor, pass through two-way valve a and integrated gases absorption cell on the pipeline between filter disc and pump unit Gas inlet connection;
The nitrogen purge system includes nitrogen cylinder, pressure reducing valve, and passes through the cigarette in triple valve a and feeding flue gas gathering system Clamper, triple valve b connections;
The pumped vacuum systems includes vacuum pump, and passes through triple valve c, two-way valve b and the cigarette of integrated gases absorption cell Gas outlet;
The photodetector system includes laser, laser controller, temperature controller, data collector and calculating Machine, laser are connected by laser aligner with the light incidence end of integrated gases absorption cell, and data collector passes through photoelectricity Detector is connected with the beam projecting end of integrated gases absorption cell, the laser controller, temperature controller, data acquisition Device is connected with computer, and carries out respective handling by computer software control.
In the utility model device, the piping volume between the triple valve a and triple valve b is more than 100mL.
The process of oxygen demand is as follows during being burnt and sucked using above device detection cigarette:The nitrogen pair in nitrogen cylinder is used first System gas circuit is thoroughly purged, and then gas absorption cell is evacuated with vacuum pump, and pump unit carries out cigarette afterwards The suction of international standard pattern, after suction, the flue gas collected is inhaled into the gas absorption cell being evacuated;It is same with this When, temperature controller, laser controller to laser into trip temperature and electric current tuning, the scanned oxygen of laser beam after tuning Absorption line, enter absorption cell by laser aligner, absorbed by under test gas, by photodetector after multiple reflections Receive, gathered and stored by data collector, finally handled through computer, the absorption signal of under test gas is by calibration Obtain the concentration of under test gas.Detection cigarette is unignited respectively and lights the concentration of under test gas after suction, and two concentration are subtracted each other Can obtain the oxygen demand that cigarette burns and sucks a bite, carry out continuous sucking, you can obtain that cigarette burns and sucks by mouth oxygen demand.
Comprise the following steps that:
1. triple valve a, triple valve b, two-way valve a, two-way valve b, triple valve c at the same time it is electric interconnect, nitrogen cylinder afterwards In nitrogen 10s cleanings are carried out to whole conducting pipeline, make to be full of nitrogen in pipeline;
2. triple valve a cuts out system pipeline, it is set to connect air;Two-way valve a is closed;Two-way valve b is stayed open;
3. triple valve c switching states make it connect vacuum pump after 1s, vacuum pumping 9s, is pumped into gas absorption cell Vacuum state;
4. two-way valve b is closed;Triple valve c cuts out system pipeline after 1s, it is connected air, and triple valve b connections suction is single First pump unit aspirates 2s, completes the suction of 35ml;
5. switching three-way valve b, makes it connect triple valve a, the 35mL flue gases of suction enter subsequent pipeline, are saved in three Between port valve a and pump unit.Two-way valve a is opened after 3s, and the under test gas in pipeline is inhaled into the integrated form being evacuated Gas absorption cell, carries out the detection of oxygen content, detection time 32s, enters next circulation after waiting 2s.
The foundation of the detection method is dexterously to be pressed by the rule that oxygen content under the conditions of constant temperature and pressure constant humidity is constant Aspirated according to international standard suction mode, detect first cigarette it is unignited before suction a bite when oxygen concentration, then detect volume The remaining concentration of oxygen after every mouth when cigarette is burnt and sucked, the difference of two concentration are the oxygen demand during every mouthful of cigarette is burnt and sucked.
More specifically, the photodetector system is provided the saw of low frequency by laser controller and temperature controller respectively The sinewave modulation signal of tooth ripple modulated signal and high frequency, laser are modulated.Modulated laser beam is through integrated gases In absorption cell gas absorb and opto-electronic conversion after, through two frequency multiplication of data collector demodulation after be sent into computer upper computer software into Row processing, obtains the absorbed second harmonic strength signal of under test gas.The peak signal of second harmonic is demarcated through calibrating gas Afterwards, the concentration of under test gas is obtained.
The specification of pipeline in the flue gas suction trapping system between triple valve a and triple valve b needs to meet certain Requirement, the volume of pipeline is 50-500mL.Because cigarette is after the pump unit suction driven by servomotor, flue gas quilt Discharge into gas pipeline.Since flue gas cannot need to be full of nitrogen, be made the flue gas of suction in nitrogen atmosphere by air pollution, pipeline In.Flue gas cannot introduce foreign gas during being sucked into the integrated gases absorption cell of vacuum pumping at the same time.To sum up, pipeline The volume of middle nitrogen should be more than the volume and cigarette holder to integrated gases absorption cell front end of integrated gases absorption cell Between the sum of conduit volume.
The utility model has the advantage of:Detection device design advantages of simple, device stable and reliable operation, it is cost-effective, Easy to use, easy to maintain;Detection method is easy to operate, pollution-free, strong antijamming capability, it is non-contact, without destructiveness, response speed Degree is fast, and accuracy of detection is high, and sensitivity is higher, and real-time is good.
Brief description of the drawings
Fig. 1 is the utility model structure of the detecting device schematic diagram.
In figure:1. nitrogen cylinder, 2. pressure reducing valves, 3. cigarette holders, 4. triple valve a, 5. triple valve b, 6. two-way valve a, 7. Filter disc, 8. data collectors, 9. pump units, 10. computers, 11. servomotors, 12. lasers, 13. temperature controllers, 14. laser controller, 15. integrated gases absorption cells, 16. two-way valve b, 17. triple valve c, 18. vacuum pumps, 19. cigarette.
Fig. 2 is integrated gases absorption cell theory of constitution figure,
In figure:15-1. laser aligners, 15-2. gas absorption cell pond bodies, 15-3. photodetectors.
Fig. 3 is cigarette by mouth oxygen demand testing result figure.
Embodiment
The utility model embodiment is described further below in conjunction with the accompanying drawings.
As shown in Figure 1, 2:Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked, it is characterised in that:Including integrated form gas Body absorption cell and the flue gas suction trapping system, the nitrogen purge system that are connected with the integrated gases absorption cell, vacuumize System and photodetector system.
The flue gas suction trapping system is included by the cigarette holder [3] of pipeline connection, triple valve b [5], filter successively Piece [7], flue gas pump unit [9], servomotor [11] are logical by two on the pipeline between filter disc [7] and pump unit [9] Valve a [6] is connected with the gas inlet of integrated gases absorption cell [15];
The nitrogen purge system includes nitrogen cylinder [1], pressure reducing valve [2], and passes through triple valve a [4] and flue gas trapping system Cigarette holder [3], triple valve b [5] connections in system;
The pumped vacuum systems includes vacuum pump [18], and passes through triple valve c [17], two-way valve b [16] and integrated form gas The exhanst gas outlet connection of body absorption cell [15];
The photodetector system includes laser [12], laser controller [14], temperature controller [13], data acquisition Device [8] and computer [10], laser [12] pass through laser aligner [15-1] and the light of integrated gases absorption cell [15] Line incidence end connects, and data collector [8] is gone out by photodetector [15-3] and the light of integrated gases absorption cell [15] End to be penetrated to be connected, the laser controller [14], temperature controller [13], data collector [8] are connected with computer [10], And respective handling is carried out by computer software control.
In the utility model device, the piping volume between the triple valve a [4] and triple valve b [5] is more than 100mL, It can so prevent air from entering in integrated gases absorption cell [15], influence testing result.Because cigarette [19] is by by watching After taking pump unit [9] suction of motor [11] driving, flue gas is passed into gas pipeline.Due to flue gas cannot by air pollution, Therefore pipeline need to be full of nitrogen, make the flue gas of suction in nitrogen atmosphere.Flue gas is sucked into the integrated form gas of vacuum pumping at the same time Foreign gas cannot be introduced during body absorption cell.To sum up, the volume of nitrogen should be more than integrated gases absorption in pipeline The volume and cigarette holder [3] in pond [15] arrive the sum of conduit volume between integrated gases absorption cell [15] front end.
Integrated gases absorption cell [15] is by laser aligner [15-1], gas absorption cell pond body [15-2], photodetection Device [15-3] forms, as shown in Figure 2.
It is as follows using the above-mentioned process for stating oxygen demand during device detection cigarette is burnt and sucked:Described device detection cigarette is burnt and sucked During oxygen demand method, system gas circuit is thoroughly purged with the nitrogen in nitrogen cylinder [1] first, then uses vacuum pump [18] gas absorption cell is evacuated, pump unit [9] carries out cigarette the suction of international standard pattern afterwards, and suction terminates Afterwards, the flue gas collected is inhaled into the gas absorption cell [15] being evacuated;At the same time, laser controller [14] is to laser Device [12] is into trip temperature and electric current tuning, the absorption line of the scanned oxygen of laser beam after tuning, by optical fiber collimator Into absorption cell, absorbed, received after multiple reflections by photodetector [15-5], by data collector by under test gas [8] collection storage, is finally handled through computer [10], and the absorption signal of under test gas can obtain gas to be measured by calibration The concentration of body.Detection cigarette is unignited respectively and lights the concentration of under test gas after suction, and two concentration, which are subtracted each other, can be rolled up Cigarette burns and sucks the oxygen demand of a bite, carries out continuous sucking, you can obtain that cigarette burns and sucks by mouth oxygen demand.Carry out repeatedly continuous take out Inhale, you can reach that cigarette burns and sucks by mouth oxygen demand.
Comprise the following steps that:
(1)Triple valve a [4], triple valve b [5], two-way valve a [6], two-way valve b [16], triple valve c [17] at the same it is electric mutually It is connected, the nitrogen in nitrogen cylinder [1] carries out 10s cleanings to whole conducting pipeline afterwards, makes to be full of nitrogen in pipeline;
(2)Triple valve a [4] cuts out system pipeline, it is connected air;Two-way valve a [6] is closed;Two-way valve
B [16] is stayed open;
(3)Triple valve c [17] switching state makes it connect vacuum pump after 1s, and vacuum pumping 9s, makes gas absorption cell quilt Vacuum state;
(4)Two-way valve b [16] is closed;Triple valve c [17] cuts out system pipeline after 1s, it is connected air, triple valve b [5] pump unit [9] pump unit suction 2s is connected, completes the suction of 35ml;
(5) switching three-way valve b [5], make it connect triple valve a [4], and the 35mL flue gases of suction enter subsequent pipeline, protected There are between triple valve a [4] and pump unit [9].Two-way valve a [6] is opened after 3s, and the under test gas in pipeline, which is inhaled into, has taken out Into the integrated gases absorption cell [15] of vacuum, the detection of oxygen content is carried out, under entering after detection time 32s, wait 2s One circulation.

Claims (2)

  1. A kind of 1. oxygen consumption amount detecting device during cigarette is burnt and sucked, it is characterised in that:Including integrated gases absorption cell and with Flue gas suction trapping system, nitrogen purge system, pumped vacuum systems and the photoelectricity inspection that the integrated gases absorption cell is connected Examining system;
    The flue gas suction trapping system includes passing through the cigarette holder [3] of pipeline connection, triple valve b [5], filter disc successively [7], flue gas pump unit [9], servomotor [11], pass through two-way valve on the pipeline between filter disc [7] and pump unit [9] A [6] is connected with the gas inlet of integrated gases absorption cell [15];
    The nitrogen purge system includes nitrogen cylinder [1], pressure reducing valve [2], and by triple valve a [4] and feeding flue gas gathering system Cigarette holder [3], triple valve b [5] connection;
    The pumped vacuum systems includes vacuum pump [18], and is inhaled by triple valve c [17], two-way valve b [16] and integrated gases The exhanst gas outlet connection of receives pond [15];
    The photodetector system includes laser [12], laser controller [14], temperature controller [13], data collector [8] and computer [10], laser [12] pass through laser aligner [15-1] and the light of integrated gases absorption cell [15] Incidence end connects, and data collector [8] passes through photodetector [15-3] and the beam projecting of integrated gases absorption cell [15] End is connected, and the laser controller [14], temperature controller [13], data collector [8] are connected with computer [10], and Respective handling is carried out by computer software control.
  2. Oxygen consumption amount detecting device during 2. cigarette according to claim 1 is burnt and sucked, it is characterised in that:The triple valve a [4] piping volume between triple valve b [5] is more than 100ml.
CN201721224975.8U 2017-09-22 2017-09-22 Oxygen consumption amount detecting device during a kind of cigarette is burnt and sucked Active CN207232016U (en)

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Application Number Priority Date Filing Date Title
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Application Number Priority Date Filing Date Title
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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107505286A (en) * 2017-09-22 2017-12-22 中国烟草总公司郑州烟草研究院 Oxygen consumption amount detecting device and detection method during a kind of cigarette is burnt and sucked

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107505286A (en) * 2017-09-22 2017-12-22 中国烟草总公司郑州烟草研究院 Oxygen consumption amount detecting device and detection method during a kind of cigarette is burnt and sucked

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