CN207204108U - Horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production - Google Patents
Horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production Download PDFInfo
- Publication number
- CN207204108U CN207204108U CN201720832201.7U CN201720832201U CN207204108U CN 207204108 U CN207204108 U CN 207204108U CN 201720832201 U CN201720832201 U CN 201720832201U CN 207204108 U CN207204108 U CN 207204108U
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- Prior art keywords
- horizontal
- kettle
- dmso
- dimethyl sulfoxide
- charging aperture
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a kind of dimethyl sulfoxide (DMSO) production horizontal convection reactor, including horizontal positioned horizontal kettle, charging aperture, discharging opening and the first motor for being symmetricly set on horizontal kettle both sides, second motor, the first rotary unit is provided with the rotary shaft side face, second rotary unit, and first rotary unit is connected with the second rotary unit by the intermediate connector being vertically set in the rotary shaft, the agitator arm of three blade compositions is arranged at intervals with the agitating shaft positioned at the intermediate connector both sides, the agitating shaft both ends are additionally provided with material scraping plate；The horizontal kettle is provided with support in both sides inwall centre position up and down, and four pieces of impeller are provided with along the longitudinal direction on two supports.The utility model has simple in construction, reasonable in design, easy to use, and dimethyl sulfoxide (DMSO) reaction solution is sufficiently mixed reaction, promotes the progress of chemical reaction, reaction effect is more preferable, and reaction efficiency is higher.
Description
Technical field
Chemical technology field is the utility model is related to, more particularly to a kind of dimethyl sulfoxide (DMSO) production is reacted with horizontal convection
Kettle.
Background technology
Dimethyl sulfoxide (DMSO) (DMSO) is a kind of organic compounds containing sulfur, and molecular formula is (CH3) 2SO, is colourless nothing under normal temperature
Smelly transparency liquid, it is a kind of hygroscopic flammable liquid.With highly polar, higher boiling, heat endurance is good, non-proton and water
Miscible characteristic, most of organic matters such as ethanol, propyl alcohol, benzene and chloroform can be dissolved in, are described as " alembroth ".Dimethyl sulfoxide (DMSO)
For colourless viscous liquid.There is hygroscopicity.Can be with water, ethanol, acetone, acetaldehyde, pyridine, ethyl acetate, dibatyl phithalate, two
Oxane and aromatic compound etc. arbitrarily dissolve each other, insoluble in the aliphatic compound beyond acetylene.
Dimethyl sulfoxide (DMSO) and acyl chloride material such as cyanuric chloride, benzoyl chloride, chloroacetic chloride, benzene sulfonyl chloride, thionyl chloride, sulfonyl
When chlorine, phosphorus trichloride etc. contact, the exothermal decomposition reactions of fierceness occur.Combined with nitric acid, generate (CH3) 2SONHO3.
Reactor the industries such as food, medicine, chemical industry application all very extensively, people are to its structure also not footpath between fields
It is raw, generally comprise the kettle with chuck, agitating device and the power set for driving agitating device to move.It is however, existing
Reactor can not reach preferably mixing effect, cannot also be effectively facilitated the progress of chemical reaction.
In view of disadvantages described above, the purpose of this utility model is to provide a kind of dimethyl sulfoxide production horizontal convection reactor,
It is set to have more practicality.
Utility model content
The defects of in order to overcome above-mentioned prior art, the purpose of this utility model are to provide a kind of dimethyl sulfoxide (DMSO) production and used
Horizontal convection reactor.
The utility model takes following technical scheme to realize：A kind of dimethyl sulfoxide (DMSO) production is reacted with horizontal convection
Kettle, including horizontal positioned horizontal kettle, charging aperture, discharging opening and be symmetricly set on horizontal kettle both sides the first motor,
Second motor, first motor, the rotary shaft of the second motor are extended to inside the horizontal retort body, on the rotary shaft side face
Be provided with the first rotary unit, the second rotary unit, and first rotary unit with the second rotary unit by being vertically arranged
Intermediate connector in the rotary shaft is connected, and three are arranged at intervals with positioned at the intermediate connector both sides in rotary shaft
The agitator arm of blade composition, rotating shaft terminal are additionally provided with material scraping plate；The charging aperture includes first charging aperture, the second charging
Mouthful, the first charging aperture, second charging aperture are separately positioned on the outer wall top of the horizontal kettle；Above and below the horizontal kettle
Both sides inwall centre position is provided with support, four pieces of impeller is provided with along the longitudinal direction on two supports, described in adjacent two pieces
Between impeller at an angle of 90.
Further, the discharging opening is arranged on the horizontal kettle side outer wall bottom.
Further, the lower surface of the material scraping plate is in contact with the horizontal inner wall of kettle.
Further, the horizontal kettle bottom both sides are symmetrically arranged with supporting leg.
The utility model has the beneficial effect that：The utility model has simple in construction, reasonable in design, easy to use, this practicality
The new shearing that can carry out strength to dimethyl sulfoxide (DMSO) reaction solution in stirring, reduce to greatest extent with the friction of storeroom and
Impulsive force, so that the existing horizontal motion of material, there is movement in vertical direction again, and in the inner chamber middle shape of horizontal kettle
The vortex larger into one, so as to which dimethyl sulfoxide (DMSO) reaction solution is sufficiently mixed into reaction, the progress of chemical reaction is promoted, is reacted
Effect is more preferable, and reaction efficiency is higher.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
Wherein：1st, the first motor；2nd, the second motor；3rd, the first rotary unit；4th, intermediate connector；5th, the second rotation is single
Member；6th, rotary shaft；7th, first charging aperture；8th, second charging aperture；9th, support；10th, impeller；11st, agitator arm；12nd, discharging opening；
13rd, horizontal kettle；14th, supporting leg；15th, material scraping plate.
Embodiment
The utility model is described further below in conjunction with the accompanying drawings：
As shown in figure 1, horizontal convection reactor, including horizontal positioned horizontal kettle are used in a kind of dimethyl sulfoxide (DMSO) production
13rd, charging aperture, discharging opening 12 and the first motor 1 of the horizontal both sides of kettle 13, the second motor 2 are symmetricly set on, described first
Motor 1, the rotary shaft 6 of the second motor 2 are extended to inside the horizontal kettle 13, and first is provided with the side face of rotary shaft 6
Rotary unit 3, the second rotary unit 5, the first rotary unit 3, the structure setting of the second rotary unit 5 can be sub- to dimethyl
Sulfone reaction solution carries out convection current and is thoroughly mixed, and accelerates reaction solution chemical reaction, and first rotary unit 3 and second rotates
Unit 5 is connected by the intermediate connector 4 being vertically set in the rotary shaft 6, and the centre is located in the rotary shaft
The both sides of connector 4 are arranged at intervals with the agitator arm 11 of three blade compositions, the structure setting of agitator arm 11, further speed up
Mixing speed and mixing quality.
As priority scheme of the present utility model, charging aperture of the present utility model includes first charging aperture 7, second charging aperture
8, the first charging aperture 7, second charging aperture 8 are separately positioned on the outer wall top of the horizontal kettle 13.
As priority scheme of the present utility model, horizontal kettle of the present utility model about 13 both sides inwall interposition install
Support 9 is equipped with, is provided with four pieces of impeller 10 on two supports 9 along the longitudinal direction, it is in 90 ° between adjacent two pieces of impeller 10
Angle.Four pieces of impeller 10 are provided with using in the inner chamber middle of horizontal kettle 13, in the promotion of the first motor 1, the second motor 2
Under rotated, the vortex formed in the inner chamber middle of horizontal kettle 13 is further stirred, has further speeded up dimethyl
The chemical reaction of sulfoxide reaction solution.
As priority scheme of the present utility model, discharging opening 12 of the present utility model is arranged on the horizontal kettle 13 1
Side outer wall bottom.
As priority scheme of the present utility model, the lower surface of material scraping plate 15 of the present utility model and the horizontal kettle 13
Inwall is in contact, the setting of material scraping plate 15, and the dimethyl sulfoxide (DMSO) material that be bonded in the horizontal inwall of kettle 13 can be scraped off,
Accelerate whole reaction process and reaction mass.
As priority scheme of the present utility model, the horizontal bottom both sides of kettle 13 of the present utility model are symmetrically arranged with supporting leg
14, supporting leg 14 supports whole device.
Although detailed description and explanation are given to concrete mode of the present utility model above, it should be noted that I
Above-mentioned various embodiments can be carried out with various equivalent changes and modification according to conception of the present utility model, produced by it
Function still covered without departing from specification spirit when, all should be within the scope of protection of the utility model.
Claims (4)
1. horizontal convection reactor, including horizontal positioned horizontal kettle, charging aperture, discharging opening are used in a kind of dimethyl sulfoxide (DMSO) production
And it is symmetricly set on the first motor of horizontal kettle both sides, the second motor, it is characterised in that：First motor, the second electricity
The rotary shaft of machine is extended to inside the horizontal retort body, and the first rotary unit, the second rotation are provided with the rotary shaft side face
Unit, and first rotary unit and the second rotary unit pass through the intermediate connector phase that is vertically set in the rotary shaft
Connect, be arranged at intervals with the agitator arm of three blades compositions, rotary shaft two in rotary shaft positioned at the intermediate connector both sides
End is additionally provided with material scraping plate；The charging aperture includes first charging aperture, second charging aperture, the first charging aperture, the second charging
Mouth is separately positioned on the outer wall top of the horizontal kettle；The horizontal kettle is provided with branch in both sides inwall centre position up and down
Frame, is provided with four pieces of impeller on two supports along the longitudinal direction, between adjacent two pieces of impeller at an angle of 90.
2. horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production according to claim 1, it is characterised in that：It is described go out
Material mouth is arranged on the horizontal kettle side outer wall bottom.
3. horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production according to claim 2, it is characterised in that：It is described to scrape
The lower surface of flitch is in contact with the horizontal inner wall of kettle.
4. horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production according to claim 1, it is characterised in that：It is described sleeping
Formula kettle bottom both sides are symmetrically arranged with supporting leg.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720832201.7U CN207204108U (en) | 2017-07-10 | 2017-07-10 | Horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720832201.7U CN207204108U (en) | 2017-07-10 | 2017-07-10 | Horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207204108U true CN207204108U (en) | 2018-04-10 |
Family
ID=61813014
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720832201.7U Expired - Fee Related CN207204108U (en) | 2017-07-10 | 2017-07-10 | Horizontal convection reactor is used in a kind of dimethyl sulfoxide (DMSO) production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207204108U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112604634A (en) * | 2020-12-28 | 2021-04-06 | 江苏阿科米科技有限公司 | Horizontal internal circulation stirring reactor |
-
2017
- 2017-07-10 CN CN201720832201.7U patent/CN207204108U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112604634A (en) * | 2020-12-28 | 2021-04-06 | 江苏阿科米科技有限公司 | Horizontal internal circulation stirring reactor |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180410 Termination date: 20200710 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |