CN207198116U - A kind of emulsifier energy force detection system - Google Patents
A kind of emulsifier energy force detection system Download PDFInfo
- Publication number
- CN207198116U CN207198116U CN201720946272.XU CN201720946272U CN207198116U CN 207198116 U CN207198116 U CN 207198116U CN 201720946272 U CN201720946272 U CN 201720946272U CN 207198116 U CN207198116 U CN 207198116U
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- aqueous phase
- oil phase
- unit
- incubator
- tubbing
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- 239000003995 emulsifying agent Substances 0.000 title claims abstract description 33
- 238000001514 detection method Methods 0.000 title claims abstract description 28
- 239000012071 phase Substances 0.000 claims abstract description 57
- 239000008346 aqueous phase Substances 0.000 claims abstract description 52
- 238000004945 emulsification Methods 0.000 claims abstract description 24
- 239000000839 emulsion Substances 0.000 claims abstract description 22
- 239000011159 matrix material Substances 0.000 claims abstract description 13
- 238000003756 stirring Methods 0.000 claims abstract description 12
- 230000001804 emulsifying effect Effects 0.000 claims abstract description 11
- 238000004458 analytical method Methods 0.000 claims abstract description 3
- 238000009413 insulation Methods 0.000 claims description 16
- 238000002156 mixing Methods 0.000 claims description 13
- 230000033228 biological regulation Effects 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 7
- 210000000481 breast Anatomy 0.000 claims description 4
- 239000004816 latex Substances 0.000 claims description 2
- 229920000126 latex Polymers 0.000 claims description 2
- 229910000831 Steel Inorganic materials 0.000 claims 2
- 239000010959 steel Substances 0.000 claims 2
- 239000002360 explosive Substances 0.000 abstract description 8
- 238000004519 manufacturing process Methods 0.000 abstract description 7
- 238000011156 evaluation Methods 0.000 abstract description 4
- 238000000034 method Methods 0.000 abstract description 4
- 238000005516 engineering process Methods 0.000 abstract description 3
- 238000003860 storage Methods 0.000 abstract description 3
- 238000007689 inspection Methods 0.000 abstract description 2
- 238000002360 preparation method Methods 0.000 abstract description 2
- 238000004321 preservation Methods 0.000 description 3
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- 229910001220 stainless steel Inorganic materials 0.000 description 2
- 239000010935 stainless steel Substances 0.000 description 2
- 238000005303 weighing Methods 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000004880 explosion Methods 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 239000011810 insulating material Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
Landscapes
- Colloid Chemistry (AREA)
Abstract
The utility model belongs to emulsifier in emulsion explosives method of inspection field, and in particular to a kind of emulsifier energy force detection system, including：Aqueous phase prepares unit, oil phase prepares unit, emulsification unit, emulsifying capacity detection unit, wherein described aqueous phase prepares unit and is used to prepare aqueous phase solution, the oil phase prepares unit and is used to prepare oil-phase solution, and the emulsification unit is used to make emulsion matrix by stirring；The emulsifying capacity detection unit is used to carry out viscosimetric analysis to emulsion matrix.The utility model has the advantages that：Aqueous phase, oil phase temperature control, emulsification stirring speed control can be carried out, emulsion matrix preparation can be carried out with simulated production Wiring technology.Can be with Fast Evaluation emulsifier ability by being detected to performance indications such as emulsion matrix viscosity, storage characteristics.The device is simple to operate, and speed is fast, each usage amount is few.
Description
Technical field
The utility model belongs to emulsifier in emulsion explosives method of inspection field, and in particular to a kind of emulsifier in emulsion explosives breast
Change validity check system.
Background technology
Aqueous ammonium nitrate solution droplet is dispersed in containing scattered gas by emulsion generally by the effect of emulsifying agent
In the oil phase of porous mass such as bubble or hollow glass micropearl, a kind of Water-In-Oil is formed（W/0）Type specific latexes system.Emulsifying agent exists
Proportion only 2% or so in emulsion, but the emulsifying effectiveness in emulsion, storage stability and explosion property etc.
Play an important role.
At present, emulsifying agent lacks relevant criterion and accurately and effectively detection method, the emulsifying agent matter of different manufacturers production
Amount is different, even if same producer, the emulsifying agent performance for producing different batches also has larger difference, causes Emulsion Explosive Production factory to exist
In the case that working condition is constant, stabilization, preferable emulsifying effectiveness are hardly resulted in.Current most Emulsion Explosive Production producers can not
Emulsifying agent is detected, emulsifying agent manufacturer can only be relied on to control, cause Quality of Emulsion Explosive stability control
It is very passive.
CN104101688A provides the emulsifying effectiveness evaluation method and device of a kind of emulsifier for emulsion explosive：Will be quantitative
Emulsion matrix be fitted into a bottom belt it is foraminate extruding tank in, with constant pressure from extruding pot bottom aperture in extrude, and
It is placed in an open-top receptacle, is taken out after placing certain time in quantitative water, dissociates ammonium nitrate content in water to evaluate
The emulsifying effectiveness of emulsifying agent.
The above method has certain feasibility, but simple to operate with greater need for one kind for Emulsion Explosive Production factory, directly,
The quick equipment for examining emulsifier effect, is controlled to ensure emulsion product matter entering factory's emulsifying agent by detection
Amount.
Utility model content
The purpose of this utility model is to provide a kind of emulsifier energy force detection system, easily and fast to detect emulsification
Agent emulsifying capacity.
The technical solution of the utility model is achieved in the following ways：
A kind of emulsifier energy force detection system, including：Aqueous phase prepares unit, and oil phase prepares unit, emulsification unit, breast
Change ability detection unit, it is used to prepare aqueous phase solution wherein the aqueous phase prepares unit, the oil phase prepares unit and is used to prepare
Oil-phase solution, the emulsification unit are used to make emulsion matrix by stirring；The emulsifying capacity detection unit is used for breast
Gel matrix carries out viscosimetric analysis.Aqueous phase, which prepares unit, includes aqueous phase with tubbing, aqueous phase incubator, the first constent temperature heater.It is described
Aqueous phase is positioned in the aqueous phase incubator equipped with thermal insulation medium with tubbing, and the aqueous phase incubator is quiet to be positioned over described first
On constent temperature heater, in described aqueous phase with having water conveying pipeline in tubbing, dispensing valve is installed on pipeline, to adjust water
Phase solution flow rate.Oil phase, which prepares unit, includes oil phase with tubbing, oil phase incubator, the second constent temperature heater.The oil phase is prepared
Bucket is positioned in the oil phase incubator equipped with thermal insulation medium, and the oil phase incubator is quiet to be put in second constent temperature heater
On.The emulsification unit includes support, agitating shaft, emulsification blade, mixing control instrument, and institute is fixed in the top of the agitating shaft
To state on support, the emulsification blade is fixed on the bottom on the agitating shaft, and mixing control instrument is connected with stirring motor, and then
Control the rotating speed of agitating shaft.
As to above-mentioned restriction, described aqueous phase incubator is stainless steel welded square, is left above square
One circular osculum is incubated for putting aqueous phase with tubbing, and its diameter is bigger 0.85-1.25cm with tubbing diameter than aqueous phase.
As the restriction to above-mentioned technical proposal, the aqueous phase incubator carries thermometer, to monitor thermal insulation medium in real time
Temperature；The aqueous phase incubator puts thermal insulation medium, Ru Shui, oil etc., is incubated by constent temperature heater heating and thermal insulation media implementation
Function.
As the restriction to above-mentioned technical proposal, described oil phase incubator is stainless steel welded square, square
Top is left a circular osculum and is incubated for putting oil phase with tubbing, and its diameter is bigger 0.25- with tubbing diameter than oil phase
0.75cm。
As the restriction to above-mentioned technical proposal, the oil phase incubator also carries thermometer, is situated between with real-time monitoring insulation
Matter temperature；Oil phase incubator puts thermal insulation medium, Ru Shui, oil etc., and work(is incubated by constent temperature heater heating and thermal insulation media implementation
Energy.
As the restriction to above-mentioned technical proposal, it is intraoral that the oil phase with tubbing is put into oil phase incubator roundlet, by embracing
The mode of card is fixed on oil phase incubator.
As the restriction to above-mentioned technical proposal, there is handle the oil phase incubator both sides, and handle is high temperature resistant, heat insulating material
Matter.
As the restriction to above-mentioned technical proposal, the mixing control instrument includes speed of agitator table, rotational speed regulation knob, leads to
Cross rotational speed regulation button control emulsification blade mixing speed.
As to above-mentioned restriction, the emulsifying capacity detection unit is specially rotary viscosimeter.
The utility model has the advantages that：Aqueous phase, oil phase temperature control can be carried out using emulsifier energy force detection system
System, emulsification stirring speed control, emulsion matrix preparation can be carried out with simulated production Wiring technology.By to emulsion matrix viscosity, storage
The detection of the performance indications such as sustainability can be with Fast Evaluation emulsifier ability.The device is simple to operate, and speed is fast, each usage amount
It is few.
Brief description of the drawings
Fig. 1 shows a kind of structural representation of emulsifier energy force detection system.
Description of symbols is as follows shown in schematic diagram：
1：First thermometer；2：Aqueous phase matches somebody with somebody tubbing；3：Aqueous phase incubator；4：First thermal insulation medium；5：First heated at constant temperature
Device；6：Baiting valves；7：Oil phase matches somebody with somebody tubbing；8：Second temperature meter；9：Handle；10：Holding card；11：Oil phase incubator；12：Second
Thermal insulation medium；13a：Agitating shaft；13b：Emulsify blade；14：Second constent temperature heater；15：Stir support；16：Speed of agitator table；
17：Rotational speed regulation knob.
Embodiment
Below in conjunction with the accompanying drawings, the embodiment of the present apparatus is further elaborated.
As shown in figure 1, aqueous phase, which prepares unit, includes aqueous phase with tubbing 2, aqueous phase incubator 3, the first constent temperature heater 5, water
Matching tubbing 2 is positioned in the aqueous phase incubator 3 equipped with the first thermal insulation medium 4, and aqueous phase incubator 3 is quiet to be positioned over first perseverance
On warm heater 5, the first constent temperature heater 5 is placed in above desk.Matching somebody with somebody in aqueous phase has water conveying pipeline in tubbing 2, on pipeline
Dispensing valve 6 is installed.Oil phase, which prepares unit, includes oil phase with tubbing 7, oil phase incubator 11, the second constent temperature heater 14, oil
Matching tubbing 7 is positioned in the oil phase incubator 11 equipped with the second thermal insulation medium 12, and oil phase incubator 11 is quiet to be put in described second
On constent temperature heater 14, the second constent temperature heater 14 is placed in above another desk.Emulsification unit includes stirring support 15, agitating shaft
13a, emulsification blade 13b, mixing control instrument, agitating shaft 13a the top are fixed on the stirring support 15, emulsify blade
13b is fixed on agitating shaft bottom, and mixing control instrument is connected with stirring motor, and then controls the rotating speed of agitating shaft.Mixing control
Instrument includes speed of agitator table 16, rotational speed regulation knob 17, and emulsification blade mixing speed is controlled by rotational speed regulation button 17.
Aqueous phase is placed in the aqueous phase incubator 3 equipped with the first thermal insulation medium 4 with tubbing 2 during experiment, by aqueous phase with tubbing 2
Dispensing valve 6 is closed, and aqueous phase raw material are placed in aqueous phase after weighing interior by the Heat preservation of the first constent temperature heater 5 with tubbing 2
It is aqueous phase solution after dissolving.Oil phase is placed in the oil phase incubator 11 equipped with the second thermal insulation medium 12 with tubbing 7, by embracing
Card 10 is fixed, and oil phase raw material are placed in oil phase after weighing interior by the Heat preservation of the second constent temperature heater 14 with tubbing 2
Oil-phase solution is then configured to after fusing.Temperature is monitored in real time by thermometer during Heat preservation.
After aqueous phase, oil-phase solution temperature reach technological requirement temperature, emulsification blade 13b is immersed in oil-phase solution, passed through
Rotational speed regulation knob 17 adjusts mixing speed, when showing that numerical value reaches technological requirement value on revolution counter 16 to be mixed, by baiting valve
Door 6 is opened, and aqueous phase solution is entered in oil-phase solution by delivery pipe, and the latex of Water-In-Oil is formed in the presence of emulsification is stirred
Matrix.In emulsion process, aqueous phase solution flow velocity can be controlled by adjusting dispensing valve 3, can with the addition of aqueous phase solution
To improve emulsification stirring speed by rotational speed regulation button, while oil phase incubator can be moved up and down by handle 9, so as to
Stirred up and down, emulsification is fully carried out.
After the completion of process to be emulsified, holding card 10 is released, takes out emulsion matrix, viscosity survey is carried out using rotation viscometer
It is fixed, while carry out thermocycling etc..Can be fast after detection data are compared with production line data and control group experiment
Speed evaluation emulsifier ability.
Above-mentioned illustrated to of the present utility model, is not intended to limit the scope of protection of the utility model.
Claims (9)
1. a kind of emulsifier energy force detection system, including aqueous phase prepares unit, oil phase prepares unit, emulsification unit and emulsification
Ability detection unit, it is used to prepare aqueous phase solution wherein the aqueous phase prepares unit, the oil phase prepares unit and is used to match somebody with somebody liquefaction
Phase solution, the emulsification unit are used to make emulsion matrix by stirring；The emulsifying capacity detection unit is used for latex
Matrix carries out viscosimetric analysis；The aqueous phase, which prepares unit, includes aqueous phase with tubbing, aqueous phase incubator, the first constent temperature heater, institute
State aqueous phase to be positioned in the aqueous phase incubator equipped with thermal insulation medium with tubbing, the aqueous phase incubator is quiet to be positioned over described
On one constent temperature heater, in the aqueous phase with having water conveying pipeline in tubbing, dispensing valve is installed on pipeline；The oil phase
Unit is prepared to be positioned over equipped with insulation with tubbing with tubbing, oil phase incubator, the second constent temperature heater, the oil phase including oil phase
In the oil phase incubator of medium, the oil phase incubator is quiet to be put on second constent temperature heater；The emulsification unit
Including support, agitating shaft, emulsification blade, mixing control instrument, the top of the agitating shaft is fixed on the support, the breast
Change the bottom that blade is fixed on the agitating shaft, mixing control instrument is connected with stirring motor, and then controls turning for agitating shaft
Speed.
2. emulsifier energy force detection system according to claim 1, it is characterised in that：The aqueous phase incubator is not
Become rusty the square that steel welds, and a circular osculum is left above square and is incubated for putting aqueous phase with tubbing, its diameter ratio
Aqueous phase matches somebody with somebody the big 0.85-1.25cm of tubbing diameter.
3. emulsifier energy force detection system according to claim 1, it is characterised in that：The oil phase incubator is not
Become rusty the square that steel welds, and a circular osculum is left above square and is incubated for putting oil phase with tubbing, its diameter ratio
Oil phase matches somebody with somebody the big 0.25-0.75cm of tubbing diameter.
4. emulsifier energy force detection system according to claim 1, it is characterised in that：The aqueous phase incubator carries
Thermometer.
5. emulsifier energy force detection system according to claim 1, it is characterised in that：The oil phase passes through with tubbing
The mode of holding card is fixed in the oil phase incubator.
6. emulsifier energy force detection system according to claim 1, it is characterised in that：The oil phase incubator both sides
Provided with handle.
7. emulsifier energy force detection system according to claim 1, it is characterised in that：The oil phase incubator also band
There is thermometer.
8. emulsifier energy force detection system according to claim 1, it is characterised in that：The mixing control instrument includes
Speed of agitator table, rotational speed regulation knob, blade mixing speed is emulsified by rotational speed regulation button control.
9. emulsifier energy force detection system according to claim 1, it is characterised in that：The emulsifying capacity detection is single
Member is specially rotary viscosimeter.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720946272.XU CN207198116U (en) | 2017-08-01 | 2017-08-01 | A kind of emulsifier energy force detection system |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720946272.XU CN207198116U (en) | 2017-08-01 | 2017-08-01 | A kind of emulsifier energy force detection system |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207198116U true CN207198116U (en) | 2018-04-06 |
Family
ID=61799520
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720946272.XU Expired - Fee Related CN207198116U (en) | 2017-08-01 | 2017-08-01 | A kind of emulsifier energy force detection system |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207198116U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109323960A (en) * | 2017-08-01 | 2019-02-12 | 巴彦淖尔盛安化工有限责任公司 | A kind of emulsifier energy force detection system |
-
2017
- 2017-08-01 CN CN201720946272.XU patent/CN207198116U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109323960A (en) * | 2017-08-01 | 2019-02-12 | 巴彦淖尔盛安化工有限责任公司 | A kind of emulsifier energy force detection system |
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|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180406 |
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| CF01 | Termination of patent right due to non-payment of annual fee |