CN207130317U - The electric dissolving device of electric solution and the earth of positive pole during separating high-temp alloy electricity is molten - Google Patents

The electric dissolving device of electric solution and the earth of positive pole during separating high-temp alloy electricity is molten Download PDF

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Publication number
CN207130317U
CN207130317U CN201721071449.2U CN201721071449U CN207130317U CN 207130317 U CN207130317 U CN 207130317U CN 201721071449 U CN201721071449 U CN 201721071449U CN 207130317 U CN207130317 U CN 207130317U
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electric
earth
positive pole
molten
kettle
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CN201721071449.2U
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邓丽
周亦胄
孙元
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Institute of Metal Research of CAS
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Institute of Metal Research of CAS
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Abstract

The utility model discloses a kind of electric dissolving device of separating high-temp alloy electricity electric solution and the earth of positive pole during molten, belong to high-temperature alloy waste material recovery technology field.The electric dissolving device is designed as:Electric fluid bowl bottom uses conical design, electric fluid bowl is connected with collecting kettle by pipeline, circuit design drop is 2 3m, pipeline diameter is 100 150mm, collect kettle and be configured with agitating device, mixing speed is 20 50r/min, and collecting kettle lower end has dispensing valve, and connecting vacuum apparatus by valve realizes the earth of positive pole and the final filtration of filtrate.Electric solution containing the earth of positive pole is after this device, and separation of solid and liquid reaches more than 99%, and filtering rate improves 100 200 times.The utility model has the advantage of that can realize efficiently to separate electric solution Anodic mud, the efficiency in production process is improved, reduces the labor intensity of worker, saves the energy, there is preferably application and economic value.

Description

The electric dissolving device of electric solution and the earth of positive pole during separating high-temp alloy electricity is molten
Technical field
It the utility model is related to high-temperature alloy waste material recovery technology field, and in particular to a kind of molten mistake of separating high-temp alloy electricity The electric dissolving device of electric solution and the earth of positive pole in journey.
Background technology
The regenerative process of high-temperature alloy waste material has already been through the laboratory research stage, realizes small-sized simulation production line The trial production stage.This technology has filled up domestic technique blank, alleviates the demand of China's strategy scarcity metals resource, reduces high temperature The cost of alloy.
The molten process of electricity is key technology in high temperature alloy regenerative process in batch production process, and its speed handled determines The ability of high temperature alloy regeneration treatment, operated in small test research process using small electrical fluid bowl, it is easy to operate, simple It is single, but in batch production process, because electricity it is molten caused by the earth of positive pole than great, be easily sunken to electric fluid bowl bottom, it is tired there is cleaning Difficult, the problems such as labor strength is big.In order to realize ease for operation, the high efficiency of the molten process of electricity in large-scale production, research and development one kind The electric dissolving device of electric solution and the earth of positive pole during energy high efficiency separation electricity is molten is to improving production efficiency, reducing worker's intensity extremely Close important.
Utility model content
The purpose of this utility model be to provide a kind of separating high-temp alloy electricity it is molten during electric solution and the earth of positive pole electricity Dissolving device, the device can efficiently separate electric solution Anodic mud, improve the efficiency in production process, have preferably application And economic value.
To achieve the above object, technical scheme is as follows used by the utility model:
The electric dissolving device of electric solution and the earth of positive pole during a kind of separating high-temp alloy electricity is molten, it is molten that the electric dissolving device includes electricity Groove, collect kettle and filter bucket, be connected between electric fluid bowl and collection kettle by pipeline;Wherein:The electric fluid bowl is used for the molten height of electricity Temperature alloy waste material, the bottom of electric fluid bowl are connected by connecting line with collecting kettle;Electric solution and the molten generation of electricity in electric fluid bowl The earth of positive pole by connecting line enter it is described collection kettle in;Agitating device is provided with the collection kettle, the bottom for collecting kettle is set There is dispensing valve, enter under agitation through dispensing valve into the mixed material collected in kettle and filter bucket, filtering in bucket Carry out the separation of electrode solution and the earth of positive pole.
The bottom of the electric fluid bowl is cone structure, and the caused earth of positive pole is deposited on the taper knot of electric fluid bowl during electricity is molten In structure.
The cone angle of the cone structure is 45 degree, and a diameter of 100-150mm of bottom open end, the bottom of cone structure is provided with Dispensing valve, the dispensing valve connection anti-acid pump housing, the anti-acid pump housing are attached by the pumping hole on the pump housing with connecting line.
In the electric dissolving device, the electric fluid bowl is located at the top for collecting kettle, for connecting electric fluid bowl and collecting the connection of kettle The design drop of pipeline is 2-3m, and connecting line intended diameter is 100-150mm.The connecting line is the PVC of acidproof alkaline Material.
The mixing speed of agitating device is 20-50r/min in the collection kettle.
Vacuum apparatus is provided with the suction filtration bucket, the mixed material entered in bucket is carried out by vacuum apparatus Filtering, and then realize the separation of the earth of positive pole and electrode solution.
The vacuum apparatus includes filter board and drain hole, and drain hole is connected in sample cell.
The beneficial effects of the utility model are as follows:
The utility model for cleaning high temperature alloy electricity it is molten during the caused earth of positive pole device, it is electric molten containing the earth of positive pole Liquid is after the device, and separation of solid and liquid reaches more than 99%, and filtering rate improves 100-200 times, and the utility model can be real Electric solution Anodic mud is now efficiently separated, improves the efficiency in production process, reduces the labor intensity of worker, is had preferable Using and economic value.
Brief description of the drawings
Fig. 1 is apparatus structure schematic diagram of the present utility model.
Wherein:1- electricity fluid bowls;11- cone structures;2- connecting lines;3- collects kettle;31- agitating devices;4- filters bucket.
Embodiment
It is for a more detailed description to the utility model below in conjunction with drawings and examples.These embodiments are only to this reality With the description of new preferred forms, there are not any restrictions to the scope of the utility model.
The utility model is the electric dissolving device of separating high-temp alloy electricity electric solution and the earth of positive pole during molten, and its structure is as schemed Shown in 1.The electric dissolving device includes electric fluid bowl 1, collects kettle 3 and filters bucket 4, and the bottom of the electric fluid bowl 1 is cone structure 11, electricity The caused earth of positive pole is deposited in the cone structure 11 of electric fluid bowl during molten.The bottom of electric fluid bowl is provided with dispensing valve, blowing Valve is connected by connecting line 2 with collecting kettle.Electric solution and the caused earth of positive pole during electric fluid bowl Inner electrolysis is through even Road 2 is taken over to enter in collection kettle 3;Agitating device 31 is provided with the collection kettle, the bottom for collecting kettle is provided with dispensing valve, enters Collect the mixed material in kettle and enter suction filtration bucket 4 through dispensing valve under 20-50r/min stirring condition, filtering in bucket 4 The separation of row electrode solution and the earth of positive pole.
The cone angle of the cone structure of the bottom of electric fluid bowl 1 is 45 degree, a diameter of 100-150mm of bottom open end, taper The bottom of structure is provided with dispensing valve, the dispensing valve connection anti-acid pump housing, and the anti-acid pump housing passes through the pumping hole on the pump housing and company Adapter road is attached.
The electric fluid bowl 1 of the electric dissolving device is located at the top for collecting kettle 3, for connecting electric fluid bowl and collecting the connecting line of kettle Design drop be 2-3m, connecting line intended diameter is 100-150mm.The connecting line is the PVC material of acidproof alkaline.
Vacuum apparatus is provided with the suction filtration bucket 4, vacuum apparatus includes filter board and drain hole, drain hole It is connected in sample cell.By vacuum apparatus to enter bucket in mixed material filter, and then realize the earth of positive pole with The separation of electrode solution, and further reclaim.
Embodiment 1
The high-temperature alloy waste material of molten 5 tons of electricity in electric fluid bowl, electricity molten time are 500 hours, and the molten amount of electricity is 1 ton, it is contemplated that production Green anode mud amount is 0.5 ton, and the earth of positive pole is sunken in cone structure during electricity is molten, and the dispensing valve of cone structure bottom is beaten Open, the earth of positive pole of conical lower portion is washed away using the solution in groove, the earth of positive pole is entered by connecting line collects kettle, and circuit design falls Difference is 3m, a diameter of 100mm of circuit design, collects kettle and is configured with agitating device, after solidliquid mixture enters collection kettle, stirring Speed is 50r/min, and solidliquid mixture enters the vacuum apparatus filtered in bucket by collecting the dispensing valve of kettle lower end, real The existing earth of positive pole and the final filtration of filtrate.For electric solution containing the earth of positive pole after this device, separation of solid and liquid reaches more than 97%, Filtering rate improves 120 times.
Embodiment 2
The high-temperature alloy waste material of molten 10 tons of electricity in electric fluid bowl, electricity molten time are 1000 hours, and the molten amount of electricity is 5 tons, it is contemplated that It is 2 tons to produce earth of positive pole amount, and the earth of positive pole is sunken in shape structure during electricity is molten, and the dispensing valve of cone structure bottom is beaten Open, the earth of positive pole of conical lower portion is washed away using the solution in groove, the earth of positive pole is entered by connecting line collects kettle, and connecting line is set Meter drop is 3m, a diameter of 120mm of circuit design, collects kettle and is configured with agitating device, after solidliquid mixture enters collection kettle, Mixing speed is 50r/min, and solidliquid mixture enters the vacuum apparatus filtered in bucket by collecting kettle lower end dispensing valve, Realize the earth of positive pole and the final filtration of filtrate.Electric solution containing the earth of positive pole after this device, separation of solid and liquid reach 97% with On, filtering rate improves 160 times.
According to the utility model has the advantage of that can realize efficiently to separate electric solution Anodic mud, production process is improved In efficiency, reduce the labor intensity of worker, it is not necessary to handle again, it is both economically and environmentally beneficial, reduce production cost, have very Good application value.

Claims (7)

  1. A kind of 1. electric dissolving device of electric solution and the earth of positive pole during separating high-temp alloy electricity is molten, it is characterised in that:The molten dress of the electricity Put including electric fluid bowl, collect kettle and suction filtration bucket, be connected between electric fluid bowl and collection kettle by pipeline;Wherein:The electric fluid bowl For the molten high-temperature alloy waste material of electricity, the bottom of electric fluid bowl is connected by connecting line with collecting kettle;Electric solution in electric fluid bowl Entered with the molten caused earth of positive pole of electricity by connecting line in the collection kettle;Agitating device is provided with the collection kettle, is collected The bottom of kettle is provided with dispensing valve, enters under agitation through dispensing valve into the mixed material collected in kettle and filters bucket, The separation of electric solution and the earth of positive pole is carried out in suction filtration bucket.
  2. The electric dissolving device of electric solution and the earth of positive pole during 2. separating high-temp alloy electricity according to claim 1 is molten, it is special Sign is:The bottom of the electric fluid bowl is cone structure, and the caused earth of positive pole is deposited on the taper knot of electric fluid bowl during electricity is molten In structure.
  3. The electric dissolving device of electric solution and the earth of positive pole during 3. separating high-temp alloy electricity according to claim 2 is molten, it is special Sign is:The cone angle of the cone structure is 45 degree, and a diameter of 100-150mm of bottom open end, the bottom of cone structure is provided with Dispensing valve, the dispensing valve connection anti-acid pump housing, the anti-acid pump housing are attached by the pumping hole on the pump housing with connecting line.
  4. The electric dissolving device of electric solution and the earth of positive pole during 4. separating high-temp alloy electricity according to claim 1 is molten, it is special Sign is:In the electric dissolving device, the electric fluid bowl is located at the top for collecting kettle, for connecting electric fluid bowl and collecting the connecting tube of kettle The design drop on road is 2-3m, and connecting line intended diameter is 100-150mm;The connecting line is the PVC materials of acidproof alkaline Matter.
  5. The electric dissolving device of electric solution and the earth of positive pole during 5. separating high-temp alloy electricity according to claim 1 is molten, it is special Sign is:The mixing speed of agitating device is 20-50r/min in the collection kettle.
  6. The electric dissolving device of electric solution and the earth of positive pole during 6. separating high-temp alloy electricity according to claim 1 is molten, it is special Sign is:Vacuum apparatus is provided with the suction filtration bucket, the mixed material entered in bucket is carried out by vacuum apparatus Filtering, and then realize the separation of the earth of positive pole and electrode solution.
  7. The electric dissolving device of electric solution and the earth of positive pole during 7. separating high-temp alloy electricity according to claim 6 is molten, it is special Sign is:The vacuum apparatus includes filter board and drain hole, and drain hole is connected in sample cell.
CN201721071449.2U 2017-08-23 2017-08-23 The electric dissolving device of electric solution and the earth of positive pole during separating high-temp alloy electricity is molten Active CN207130317U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108359804A (en) * 2018-03-30 2018-08-03 西安瑞鑫科金属材料有限责任公司 A method of it being enriched with tungsten tantalum hafnium from high-temperature alloy waste material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108359804A (en) * 2018-03-30 2018-08-03 西安瑞鑫科金属材料有限责任公司 A method of it being enriched with tungsten tantalum hafnium from high-temperature alloy waste material

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