CN207085395U - Separable Accelerate solvent extraction device - Google Patents
Separable Accelerate solvent extraction device Download PDFInfo
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- CN207085395U CN207085395U CN201720779698.0U CN201720779698U CN207085395U CN 207085395 U CN207085395 U CN 207085395U CN 201720779698 U CN201720779698 U CN 201720779698U CN 207085395 U CN207085395 U CN 207085395U
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- solvent
- solvent extraction
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Abstract
The utility model discloses separable Accelerate solvent extraction device, wherein solvent extraction plant is connected or separated by some connecting interfaces located at control main frame side with the solvent extraction plant located at its side including control main frame, is convenient for carrying and use.And Accelerate solvent extraction device of the present utility model is in use, the various solvents for needing to extract are heated to predetermined temperature first by the solvent preheating device at the top of control main frame and solvent preheating container, and it is incubated in real time, is ready to add corresponding solvent extraction bottle.Then, the reverse pressue device reverse punching press upwards located at solvent extraction bottom of bottle portion is used into solvent heating a period of time of solvent extraction bottle or in heating, and then improve the pressure in solvent extraction bottle, and then realize the extraction of solvent and be concentrated in solvent extraction bottle while carry out, the efficiency of extraction is improved, realizes full-automatic Rapid Extraction solvent.
Description
Technical field
Rapid extraction technology field is the utility model is related to, more particularly to separable Accelerate solvent extraction device.
Background technology
Accelerate solvent extraction technology is one kind developed in recent years in high temperature（Room temperature~200 DEG C）, high pressure（Atmospheric pressure
~20MPa）Under the conditions of the sample-pretreating method of rapid extraction solid or semi-solid sample, with conventional surname extraction, ultrasound
The methods of extraction, microwave-assisted extraction technique, is compared, and is substantially shorter extraction time, improves extraction efficiency, reduces extractant dosage,
The extraction expense of single sample is significantly reduced, has the advantages that saving solvent, quick, health environment-friendly, automaticity are high.
Solvent extraction is immiscible at two kinds using material（Or slightly soluble）Solvent in solubility or distribution coefficient not
Together, the method for making solute substance be transferred to out of a kind of solvent in another solvent.It is widely used in chemistry, metallurgical, food
Deng industry, extraction is to be used for purifying one of means with purifying compound in Organic Chemistry Laboratory, can be from solid by extraction
Or required material is extracted in liquid mixture.In the prior art, there are a variety of extraction process, respectively by using different
Extraction equipment is extracted.But the monitoring and control of existing extraction equipment usually relies on the control system that equipment carries in itself
System, operating personnel must wait for be operated and understands course of reaction on one side in equipment, therefore noise caused by equipment even has
Evil gas etc. can produce infringement to operating personnel, and operating personnel must dress safeguard, so as to be brought not to operation and control
Just.
Utility model content
In order to overcome the above-mentioned deficiencies of the prior art, the utility model provides a kind of extraction efficiency height, installs and take
With convenient Accelerate solvent extraction device and extracting system.
Technical scheme is used by the utility model：Separable Accelerate solvent extraction device, including control main frame and
The tip position of solvent extraction plant located at its side, wherein control main frame is provided with solvent preheating device, and bottom is provided with control
Panel, control main frame is interior to be provided with heater and refrigerator；Heater and refrigerator are connect by some connections of control main frame side
Mouth connection solvent heater and condensing unit；Solvent extraction plant, including the solvent connected as one by column heat dress
Put, solvent extraction bottle Support bracket, condensing unit and containing base plate；Solvent extraction bottle Support bracket is stuck in solvent heater
Tip position, and solvent extraction bottle Support bracket is additionally provided with some solvent extraction bottles along its outward flange, solvent extraction bottle
Bottom is provided with reverse pressue device；Each described solvent extraction bottle includes hard shell and flexible bladder type inner bag, closure, firmly
Matter shell is fixedly connected with solvent extraction bottle Support bracket, and flexible bladder type liner at the bottom contacts supercharging with reverse pressue device；Institute
State reverse pressue device and correspond to each solvent extraction bottle opening position and be provided with a pressurization drift, each pressurization drift is right by its
The flexible bladder type inner bag answered is upward, and then increases the pressure in flexible bladder type inner bag；Reversely pressue device passes through one simultaneously
Individual swing mechanism and swing power source drive it to be rocked to the side of column；Solvent preheating device is preheated by least one solvent
Container supplies preheated solvent into each solvent extraction bottle.
Further, each solvent preheating container is also connected with a temperature sensor and solvent preheating device, chain of command
Plate, control panel show the Temperature numerical of each solvent preheating container.
Further, each solvent preheating container is respectively by a feed pipe and a controlled valve to solvent extraction
Bottle supplies preheated solvent.
Further, each feed pipe supplies preheated solvent to solvent extraction bottle through a support deck, and
And the support deck is fixed on the tip position of control main frame.
Further, the condensing unit is fixed on column by condensing support, condensation support connection condensation tube, condensation
The opening position that cylinder corresponds to each solvent extraction bottle is provided with a condensation sleeve pipe, while is provided with condenser coil in condensation tube, described
Condenser coil connection refrigerator obtains low-temperature receiver.
Further, the center of the containing base plate is provided with some accommodating grooves, and corresponding one of each accommodating groove is molten
Agent extraction flask.
Further, column and the one side fitting design of control main frame contact.
Further, reverse pressue device is one kind in cylinder or oil cylinder.
Compared with prior art, the beneficial effects of the utility model are：Accelerate solvent extraction device of the present utility model, control
Main frame processed is connected or divided by some connecting interfaces located at control main frame side with the solvent extraction plant located at its side
From being convenient for carrying and use.
And Accelerate solvent extraction device of the present utility model is in use, first by the top of control main frame
Solvent preheating device and solvent preheating container need the solvents that extract to be heated to predetermined temperature by various, and be incubated in real time,
It is ready to add corresponding solvent extraction bottle.
Then, use into solvent heating a period of time of solvent extraction bottle or in heating and be located at solvent extraction bottom of bottle
The reverse punching press upwards of the reverse pressue device in portion, so improve solvent extraction bottle in pressure, and then realize solvent extraction and
It is concentrated in solvent extraction bottle while carries out, improves the efficiency of extraction.Reverse pressue device passes through a swing mechanism and pendulum
Dynamic power source drives it to be rocked to the side of column, after pressurization is completed every time, control of the reverse pressue device in control main frame
By swing mechanism and swing power source down and swing to the side of column, facilitate solute in solvent extraction bottle and residual solution from
It is dynamic to enter condensing unit, storage device is subsequently entered, realizes full-automatic Rapid Extraction solvent.
Heated and pressurizeed in the solvent of solvent extraction bottle, can accelerated to dissolve mainly due to high temperature, spread, dropped
The viscosity of low solvent, improve surface tension of sample etc. so that the speed and efficiency of extraction are greatly speeded up, and are made in this container
Filled with solvent and be added to certain high pressure, make the elevation of boiling point of solvent, the solvent in such container is constantly at high temperature
Liquid, sample can be extracted at high temperature, and solvent extraction bottle of the present utility model not only has enough high temperature, simultaneously
Enough pressure is also assures that, improves its rate of extraction.
Based on the extracting system of Accelerate solvent extraction device of the present utility model, including the pre- hot charging of solvent being sequentially connected
Put, solvent preheating device, automatically supply solvent device, automatically supply solvent device, condensation abstraction device so that extractant exists
By automatic transmission and seamless completion between preheating, HTHP concentration extraction and condensation abstraction, fast solvent extraction is improved
The automaticity that takes, extraction efficiency.
Brief description of the drawings
Fig. 1 is the structure chart of one embodiment of separable Accelerate solvent extraction device；
Fig. 2 is the structure chart of the control main frame of Fig. 1 embodiment；
Fig. 3 is the structure chart of the solvent extraction plant of Fig. 1 embodiment；
Fig. 4 is the structure chart of the solvent extraction bottle of Fig. 1 embodiment；
Fig. 5 be Fig. 1 A to structure chart；
Fig. 6 be Fig. 1 B to structure chart；
Wherein：1- control main frames, 2- solvent extraction plants, 3- solvent preheating devices, 4- control panels, 5- solvents heating dress
Put, 6- solvent extraction bottle Support brackets, 7- condensing units, 71- condensation supports, 72- condensation tubes, 73- condenser coils, 74- condensations
Sleeve pipe；8- columns, 9- solvent extraction bottles, the reverse pressue devices of 10-, 101- pressurization drifts；11- supports deck, 12- storages bottom
Seat, 121- accommodating grooves；13- swing mechanisms, 14- swing power sources, 15- solvent preheating containers, 16- heaters, 17- refrigerators,
18- feed pipes, 19- controlled valves.
Embodiment
In order to deepen to understanding of the present utility model, with reference to the accompanying drawings and examples to the utility model furtherly
Bright, the embodiment is only used for explaining the utility model, and the scope of protection of the utility model is not formed and limited.
As shown in figure 1, separable Accelerate solvent extraction device, it is characterised in that：Including control main frame 1 and located at one
The solvent extraction plant 2 of side, wherein as shown in Fig. 2 the tip position of control main frame 1 is provided with solvent preheating device 3, bottom is provided with
Control panel 4, control main frame 1 is interior to be provided with heater 16 and refrigerator 17；Heater and refrigerator pass through the side of control main frame 1
Some connecting interface connection solvent heaters 5 and condensing unit 7；As shown in figure 3, solvent extraction plant 2 includes passing through column 8
Solvent heater 5, solvent extraction bottle Support bracket 6, condensing unit 7 and the containing base plate 12 connected as one, is done directly
HTHP extraction, condensation abstraction and the storage of solvent, improve its extraction efficiency；Solvent extraction bottle Support bracket 6 blocks
In the tip position of solvent heater 5, and solvent extraction bottle Support bracket 6 is additionally provided with some solvent extractions along its outward flange
Bottle 9 is taken, the bottom of solvent extraction bottle 9 is provided with reverse pressue device 10, realizes solvent while high-temperature extraction or high temperature
High-temperature pressurizing concentration is carried out after extraction, there is high extraction efficiency, shortens and transports and intermediate treatment link.
Fig. 4 is referred to, each described solvent extraction bottle 9 includes hard shell 91 and flexible bladder type inner bag 92, closure 93,
Hard shell 91 is fixedly connected with solvent extraction bottle Support bracket 6, and the bottom of flexible bladder type inner bag 92 connects with reverse pressue device 10
Touch supercharging；Described each corresponding opening position of solvent extraction bottle 9 of reversely pressue device 10 is provided with a pressurization drift 101, each
Individual pressurization drift 101 is upward by its corresponding flexible bladder type inner bag 92, and then increases the pressure in flexible bladder type inner bag 92；
Reversely pressue device 10 drives it to be rocked to the side of column by a swing mechanism 13 and swing power source 14 simultaneously；Solvent
Preheating device 3 supplies preheated solvent, pre- thermal effect into each solvent extraction bottle 9 by least one solvent preheating container 15
Fruit is good, and can preheat multi-solvents simultaneously.Say in more detail, the flexible bladder type of solvent extraction bottle 9 of the present utility model
Inner bag 92 is made up of high temperature resistant and pressure-resistant polytetrafluoroethylmaterial material or silica gel, and service life is longer, and durable effect is preferable.
As depicted in figs. 1 and 2, each solvent preheating container 15 is also connected with a temperature sensor 151 and solvent preheating
Device 3, control panel 4, control panel 4 show the Temperature numerical of each solvent preheating container 15, convenient control in real time.It is each
Individual solvent preheating container 15 is supplied preheated by a feed pipe 18 and a controlled valve 19 to solvent extraction bottle 9 respectively
Solvent preheating container 15 can be automatically added to its corresponding solvent extraction bottle and be extracted by solvent, the setting of these structures,
Improve the efficiency of multi-solvents while extraction.And each feed pipe 18 supports deck 11 to solvent extraction bottle through one
9 preheated solvents of supply, and the support deck 11 is fixed on the tip position of control main frame 1, rational deployment support card
Holder structure, it is easy to use.
As shown in figures 1 and 3, the condensing unit 7 is fixed on column 8 by condensing support 71, and condensation support 71 connects
Condensation tube 72 is connect, the opening position of each the corresponding solvent extraction bottle 9 of condensation tube 72 is provided with a condensation sleeve pipe 74, while condensation tube
Condenser coil 73 is provided with 72, the condenser coil 73 connects refrigerator 17 and obtains low-temperature receiver.The centre bit of the containing base plate 12
Some accommodating grooves 121 are installed, the corresponding solvent extraction bottle 9 of each accommodating groove 121.What column 8 and control main frame 1 contacted
Simultaneously fitting design.In addition, reversely pressue device 10 is one kind in cylinder or oil cylinder, preferable using effect is respectively provided with.
The extracting system of above-mentioned Accelerate solvent extraction device, including the following device being sequentially connected：
Solvent preheating device, for the solvent of each solvent preheating container to be preheated to 40-55 °C of temperature, reach pre-
After constant temperature degree, real-time heat preservation for standby use, when the solvent temperature that the temperature sensor in solvent preheating device detects is less than predetermined
During 3 ° -5 ° of temperature, start the preheating of solvent preheating device；Automatic supply solvent device, will be pre- in each solvent preheating container
Hot solvent automatic transport is to solvent extraction bottle；Heating concentration extraction equipment；Solvent extraction bottle is heated to suitable extraction temperature automatically
Degree, then using the flexible bladder type inner bag of each solvent extraction bottle of the pressurization drift of reverse pressue device, realize solvent
High-temperature extraction and high pressure concentration；Condensation abstraction device, the isolate after HTHP concentration extraction is subjected to cooling receipts
Receive.
In the above-described embodiments, extracting system also includes storage device, and storage device is located at the bottom of condensation abstraction device
Position, the extracting substance obtained for individually reclaiming each solvent extraction bottle, improve the easy-to-use performance of the device.So that should
System is more convenient when using, without other instruments.Extraction system based on Accelerate solvent extraction device of the present utility model
System, including be sequentially connected solvent preheating device, solvent preheating device, automatically supply solvent device, automatically supply solvent device,
Condensation abstraction device so that extractant by between preheating, HTHP concentration extraction and condensation abstraction it is automatic transmit with
And seamless completion, improve automaticity, the extraction efficiency of Accelerate solvent extraction.
In general, separable Accelerate solvent extraction device either of the present utility model, or the extraction based on it
System is taken, can realize a variety of or same more parts of solvent simultaneously, extract by preheating, HTHP concentration extraction and condensation
Automatically transmission and seamless completion between taking, automaticity, the extraction efficiency of Accelerate solvent extraction is improved, is had preferable
Use market.
What embodiment of the present utility model was announced is preferred embodiment, but is not limited thereto, the common skill of this area
Art personnel, easily according to above-described embodiment, understand spirit of the present utility model, and make different amplification and change, but as long as
Spirit of the present utility model is not departed from, all in the scope of protection of the utility model.
Claims (8)
1. separable Accelerate solvent extraction device, it is characterised in that：Including control main frame（1）With the solvent extraction located at its side
Take device（2）, wherein control main frame（1）Tip position be provided with solvent preheating device（3）, bottom is provided with control panel（4）, control
Main frame processed（1）It is interior to be provided with heater（16）And refrigerator（17）；Heater and refrigerator pass through control main frame（1）Side it is some
Connecting interface connects solvent heater（5）And condensing unit（7）；
Solvent extraction plant（2）, including pass through column（8）The solvent heater connected as one（5）, solvent extraction bottle support
Bracket（6）, condensing unit（7）And containing base plate（12）；
Solvent extraction bottle Support bracket（6）It is stuck in solvent heater（5）Tip position, and solvent extraction bottle Support bracket
（6）Some solvent extraction bottles are additionally provided with along its outward flange（9）, solvent extraction bottle（9）Bottom be provided with reverse pressue device
（10）；
Each described solvent extraction bottle（9）Including hard shell（91）With flexible bladder type inner bag（92）, closure（93）, hard
Shell（91）With solvent extraction bottle Support bracket（6）It is fixedly connected, flexible bladder type inner bag（92）Bottom and reverse pressue device
（10）Contact supercharging；
The reverse pressue device（10）Each corresponding solvent extraction bottle (9) opening position is provided with a pressurization drift（101）, often
One pressurization drift（101）By its corresponding flexible bladder type inner bag（92）It is upward, and then increase flexible bladder type inner bag（92）
Interior pressure；Reverse pressue device simultaneously（10）Pass through a swing mechanism（13）With swing power source（14）Drive it to be rocked to
The side of column；
Solvent preheating device（3）Pass through at least one solvent preheating container（15）To each solvent extraction bottle（9）Interior supply preheating
Good solvent.
2. separable Accelerate solvent extraction device according to claim 1, it is characterised in that：The pre- thermal capacitance of each solvent
Device（15）It is also connected with a temperature sensor（151）With solvent preheating device（3）, control panel（4）, control panel（4）Display
Each solvent preheating container（15）Temperature numerical.
3. separable Accelerate solvent extraction device according to claim 2, it is characterised in that：The pre- thermal capacitance of each solvent
Device（15）Pass through a feed pipe respectively（18）With a controlled valve（19）To solvent extraction bottle（9）Supply preheated molten
Agent.
4. separable Accelerate solvent extraction device according to claim 3, it is characterised in that：Each feed pipe（18）
Through a support deck（11）To solvent extraction bottle（9）Supply preheated solvent, and the support deck（11）It is fixed on
Control main frame（1）Tip position.
5. separable Accelerate solvent extraction device according to claim 1, it is characterised in that：The condensing unit（7）
By condensing support（71）It is fixed on column（8）On, condense support（71）Connect condensation tube（72）, condensation tube（72）It is corresponding each
Individual solvent extraction bottle（9）Opening position be provided with a condensation sleeve pipe（74）, while condensation tube（72）It is interior to be provided with condenser coil（73）,
The condenser coil（73）Connect refrigerator（17）Obtain low-temperature receiver.
6. separable Accelerate solvent extraction device according to claim 1, it is characterised in that：The containing base plate（12）
Center be provided with some accommodating grooves（121）, each accommodating groove（121）A corresponding solvent extraction bottle（9）.
7. the separable Accelerate solvent extraction device according to claim 1-6 any one, it is characterised in that：Column
（8）And control main frame（1）The one side fitting design of contact.
8. separable Accelerate solvent extraction device according to claim 7, it is characterised in that：Reverse pressue device（10）
For one kind in cylinder or oil cylinder.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720779698.0U CN207085395U (en) | 2017-06-30 | 2017-06-30 | Separable Accelerate solvent extraction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720779698.0U CN207085395U (en) | 2017-06-30 | 2017-06-30 | Separable Accelerate solvent extraction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207085395U true CN207085395U (en) | 2018-03-13 |
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ID=61554851
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720779698.0U Expired - Fee Related CN207085395U (en) | 2017-06-30 | 2017-06-30 | Separable Accelerate solvent extraction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207085395U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107308680A (en) * | 2017-06-30 | 2017-11-03 | 迪天环境技术南京股份有限公司 | Separable Accelerate solvent extraction device and extracting system |
-
2017
- 2017-06-30 CN CN201720779698.0U patent/CN207085395U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107308680A (en) * | 2017-06-30 | 2017-11-03 | 迪天环境技术南京股份有限公司 | Separable Accelerate solvent extraction device and extracting system |
| CN107308680B (en) * | 2017-06-30 | 2022-08-23 | 迪天环境技术南京股份有限公司 | Separable rapid solvent extraction device and extraction system |
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| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180313 Termination date: 20200630 |
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| CF01 | Termination of patent right due to non-payment of annual fee |