CN207056570U - A kind of novel material stirring reaction device - Google Patents
A kind of novel material stirring reaction device Download PDFInfo
- Publication number
- CN207056570U CN207056570U CN201721026654.7U CN201721026654U CN207056570U CN 207056570 U CN207056570 U CN 207056570U CN 201721026654 U CN201721026654 U CN 201721026654U CN 207056570 U CN207056570 U CN 207056570U
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- reaction vessel
- lifting
- supporting plate
- end cap
- agitating
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Abstract
The utility model provide it is a kind of it is simple in construction, reaction effect is good and can effectively avoid producing the novel material stirring reaction device of dirt, its outer end cap for including being located at the reaction vessel top and being matched therewith, the agitating device being arranged in the reaction vessel inner chamber, the lowering or hoisting gear for lifting the agitating device lifting moving, the heater for being arranged at the reaction vessel circumferential periphery and the step switch for controlling the heater to act；This programme coordinates by using agitating device and lowering or hoisting gear is stirred effect to realize to the material in reaction vessel, in order to cause the material stirring in reaction vessel fully and dirt will not be produced in reaction vessel inwall, agitating device in this programme its in positive and negative rotation realize the stirring action to material, agitating shaft is in whipping process, lowering or hoisting gear drives agitating shaft to move up and down vertically, ensure that material is all uniformly stirred up and down in whole reaction vessel, so as to ensure that the entirety of whole material stirs.
Description
Technical field
Reactor technical field is the utility model is related to, refers in particular to a kind of novel material stirring reaction device.
Background technology
In chemical products production process, it typically can all use reactor equipment and be chemically reacted.Chemically reacted
A FAQs in journey is how to realize appropriate material contact in the reactor, to efficiently generate required production
Product.Reactant needs to mix, and the molecule of reactive component is contacted with other components including catalyst, to improve reaction effect
Rate.It is existing in order to ensure to contact with each other between each reactive component, its be typically all by extending each component connecing in reactor
What the tactile time was realized.Each component its during haptoreaction, it is typically all under hot environment state, therefore when long
Between under contact condition, reactor inwall formed with thin film or dirt, can influence the reaction rate of whole reactor, while
The reaction effect of subsequent product is influenced whether, especially in the production process of tonalid, in hydrochloric acid gas and organic
For gas jointly under impact, observation window visual effect is worse during material stirring, it is impossible to sees internal-response very well in the reaction
Phenomenon.
The tetralin musk deer fragrant perfume of tonalid category polycyclic musk, its note are closer to natural macrocyclic musk, preferably
Happy musk odor is more pure, lasting, and there is dense powder fragrance to cease, fragrant of fine quality good, gives people a kind of very comfortable happy sense
Feel.Due to tonalid under acid-base neutralization sunlight it is non-discolouring, most widely used in daily chemical essence, next can be used for cigarette
In hay-scented essence, tonalid has fabulous associativity with fabric, though scrubbed, fragrance still exists, and is usually used in washing essence
In, tonalid synthesis is convenient, and cheap, its product boiling point is relatively low, has the characteristics of lasting is lasting, while tonalid is met
Light does not add lustre to non-discolouring, therefore it has more superior working condition and higher economic valency than macrocyclic musk and nitro musk
Value.The synthesis of tonalid is typically broadly divided into two steps, first, by toluene or the derivative and alkene, alcohol initial ring of contraposition substitution
Change, generation intermediate hexamethyl tetrahydronaphthalene (HMT)；Second, HMT dealings with alcohol, using Fu's formula acylation reaction, preparation, which is told, receives musk deer
Fragrant (AHMT), typically also needs to add corresponding catalyst in whole preparation process.In course of reaction is produced, reaction is participated in
Reactant generally require sufficiently to be mixed, especially it is each participate in reaction reactant ratio do not controlled effectively
When processed, stir and just seem more important.In consideration of it, searching out, one kind is simple in construction, reaction effect is good and can effectively avoid
The reaction structure for producing dirt is just particularly important.
The content of the invention
In view of the shortcomings of the prior art, the utility model offer one kind is simple in construction, reaction effect is good and can effectively avoid
Produce the novel material stirring reaction device of dirt.
To achieve the above object, technical scheme provided by the utility model is：A kind of novel material stirring reaction device,
The stirring reaction device includes columnar reaction vessel, it is characterised in that：The stirring reaction device also includes being located at institute
The outer end cap stating reaction vessel top and be matched therewith, the agitating device being arranged in the reaction vessel inner chamber, for carrying
Rise the lowering or hoisting gear of the agitating device lifting moving, be arranged at the heater of the reaction vessel circumferential periphery and for controlling
The step switch of the heater action is made, the agitating device includes the stirring being vertically arranged in the reaction vessel inner chamber
Multiple stirring blades that axle, fixed intervals are arranged in the shaft bottom, the electricity for driving the agitating shaft positive and negative rotation
Machine and the hold-down support for installing the motor, the lowering or hoisting gear include supporting plate, are arranged on the supporting plate for a pair
Lifting support between outer end cap, the lifting shaft arranged vertically, the motor for driving the lifting shaft lifting moving and
For connecting the contiguous block of the lifting shaft and supporting plate, wherein the agitating shaft passes vertically through the supporting plate and formed therewith
Rotation connection, the support that the agitating shaft is provided with by its periphery are fixedly connected in the supporting plate, each lifting
Its bottom of pillar is fixedly linked with the supporting plate, and its other end is formed with the supporting plate to be connected along the activity of vertical lifting
Connect；This programme coordinates by using agitating device and lowering or hoisting gear is stirred effect to realize to the material in reaction vessel,
In order to cause material stirring in reaction vessel fully and dirt will not be produced in reaction vessel inwall, stirring in this programme
Mixing device, it realizes the stirring action to material in positive and negative rotation, and for agitating shaft in whipping process, lowering or hoisting gear drives stirring
Axle can move up and down vertically, ensure that material is all uniformly stirred up and down in whole reaction vessel, so as to ensure whole material
Entirety stirs.
Further, the stirring reaction device also includes the inner end cap being arranged between the outer end cap and stirring blade,
Wherein described inner end cap is fixedly connected on the agitating shaft, between the inner end cap outward flange and the reaction vessel madial wall
It is additionally provided with packing ring；By being provided with an inner end cap, it is ensured that material in whipping process more uniformly, more fill by stirring
Point.
Yet further, it is additionally provided with observation window on its one side of the reaction vessel；Can be with by being provided with observation window
Person easy to operation understands its internal response situation in real time in operation.
Relative to prior art, the utility model provides a kind of simple in construction, stirring reaction device for integrally stirring.
Brief description of the drawings
Fig. 1 is operation principle structural representation of the present utility model.
Embodiment
With reference to specific embodiment, the utility model is described in further detail：
Referring to shown in accompanying drawing 1, the utility model provides a kind of novel material stirring reaction device, the stirring reaction device bag
Include columnar reaction vessel 1, in addition to positioned at the top of reaction vessel 1 and be matched therewith outer end cap 2, be arranged at reaction and hold
Agitating device in the inner chamber of device 1, the lowering or hoisting gear for lifting agitating device lifting moving, it is arranged at outside the surrounding of reaction vessel 1
The heater 10 and the step switch 9 for controlling heater 10 to act enclosed, above-mentioned agitating device include being vertically arranged at instead
Answer multiple stirring blades 8 that the agitating shaft 4 in the inner chamber of container 1, fixed intervals be arranged on the bottom of agitating shaft 4, stirred for driving
The motor 3 of the positive and negative rotation of axle 4 and the hold-down support 5 for installing motor 3, above-mentioned lowering or hoisting gear include supporting plate 7, set for a pair
The lifting shaft 13 of put the lifting support 6 between supporting plate 7 and outer end cap 2, arranging vertically, for driving the lifting of lifting shaft 13 to move
Dynamic motor 12 and the contiguous block 14 for connecting lifting shaft 13 and supporting plate 7, wherein agitating shaft 4 pass vertically through supporting plate 7
And rotation connection is formed therewith, the support that agitating shaft 4 is provided with by its periphery is fixedly connected in supporting plate 7, each lifting
Its bottom of pillar 6 is fixedly linked with supporting plate 7, and its other end is formed with supporting plate 7 being flexibly connected along vertical lifting；We
Case coordinates by using agitating device and lowering or hoisting gear is stirred effect to realize to the material in reaction vessel 1, in order to
Enough so that material stirring in reaction vessel 1 fully and will not produce dirt in the inwall of reaction vessel 1, the stirring dress in this programme
It is put in positive and negative rotation to realize the stirring action to material, for agitating shaft 4 in whipping process, lowering or hoisting gear drives agitating shaft 4
It can vertically move up and down, ensure that material is all uniformly stirred up and down in whole reaction vessel 1, so as to ensure the whole of whole material
Body stirs.Further, above-mentioned stirring reaction device also includes the inner end cap being arranged between outer end cap 2 and stirring blade 8
11, wherein inner end cap 11 is fixedly connected on agitating shaft 4, between the above-mentioned outward flange of inner end cap 11 and the madial wall of reaction vessel 1 also
It is provided with packing ring 15；By being provided with an inner end cap 11, it is ensured that in whipping process more uniformly, stirring is more for material
Fully.In addition it is upper in this programme for the ease of the response situation inside operator's solution reaction kettle real-time in operation
State and be additionally provided with observation window 16 on reaction vessel 1 its one side.
Examples of implementation described above are only the preferred embodiment of the utility model, are not limited with this of the present utility model
Practical range, therefore the change that all shape, principles according to the utility model are made, all should cover in the scope of protection of the utility model
It is interior.
Claims (3)
1. a kind of novel material stirring reaction device, the stirring reaction device includes columnar reaction vessel, and its feature exists
In：The stirring reaction device also include positioned at the reaction vessel top and be matched therewith outer end cap, be arranged at it is described
Agitating device in reaction vessel inner chamber, the lowering or hoisting gear for lifting the agitating device lifting moving, be arranged at it is described anti-
The heater of container circumferential periphery and the step switch for controlling the heater action are answered, the agitating device includes perpendicular
The agitating shaft that is directly arranged in the reaction vessel inner chamber, fixed intervals are arranged on multiple stirrings in the shaft bottom
Knife, the motor for driving the agitating shaft positive and negative rotation and the hold-down support for installing the motor, the lifting dress
The lifting shaft put and be arranged on lifting support between the supporting plate and outer end cap including supporting plate, a pair, arranging vertically, it is used for
The motor of the lifting shaft lifting moving and the contiguous block for connecting the lifting shaft and supporting plate are driven, wherein described stir
Mix axle to pass vertically through the supporting plate and form rotation connection therewith, the support that the agitating shaft is provided with by its periphery is fixed
Be connected in the supporting plate, each its bottom of the lifting support is fixedly linked with the supporting plate, its other end with it is described
Supporting plate is formed can be along the flexible connection of vertical lifting.
A kind of 2. novel material stirring reaction device according to claim 1, it is characterised in that：The stirring reaction device
Also include the inner end cap being arranged between the outer end cap and stirring blade, wherein the inner end cap is fixedly connected on the agitating shaft
On, it is additionally provided with packing ring between the inner end cap outward flange and the reaction vessel madial wall.
A kind of 3. novel material stirring reaction device according to claim 1 or 2, it is characterised in that：The reaction vessel
Observation window is additionally provided with its one side.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721026654.7U CN207056570U (en) | 2017-08-16 | 2017-08-16 | A kind of novel material stirring reaction device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201721026654.7U CN207056570U (en) | 2017-08-16 | 2017-08-16 | A kind of novel material stirring reaction device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN207056570U true CN207056570U (en) | 2018-03-02 |
Family
ID=61515176
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201721026654.7U Active CN207056570U (en) | 2017-08-16 | 2017-08-16 | A kind of novel material stirring reaction device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN207056570U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109282627A (en) * | 2018-09-20 | 2019-01-29 | 彭婷 | A kind of dry system of processing of active carbon and its active carbon drying and processing method |
-
2017
- 2017-08-16 CN CN201721026654.7U patent/CN207056570U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109282627A (en) * | 2018-09-20 | 2019-01-29 | 彭婷 | A kind of dry system of processing of active carbon and its active carbon drying and processing method |
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