CN207007567U - A kind of electrolyte sampler - Google Patents

A kind of electrolyte sampler Download PDF

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Publication number
CN207007567U
CN207007567U CN201720585039.3U CN201720585039U CN207007567U CN 207007567 U CN207007567 U CN 207007567U CN 201720585039 U CN201720585039 U CN 201720585039U CN 207007567 U CN207007567 U CN 207007567U
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China
Prior art keywords
electrolyte
valve
syringe
probe tube
ready
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CN201720585039.3U
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Chinese (zh)
Inventor
张天祥
侯建波
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Anhui Li Xing New Energy Co Ltd
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Anhui Li Xing New Energy Co Ltd
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Priority to CN201720585039.3U priority Critical patent/CN207007567U/en
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Abstract

A kind of electrolyte sampler of the utility model, including electrolyte bucket, probe tube, ready-packaged joint and syringe, electrolyte bottom of the barrel is stretched into described probe tube one end, the probe tube other end connects ready-packaged joint, the ready-packaged joint is sequentially connected the first valve by delivery pipe, second valve and raffinate cup, drawing liquid pipeline is connected in delivery pipe between first valve and the second valve, the drawing liquid pipeline connects sample connection, on the drawing liquid pipeline the 3rd valve is provided with sample connection, the sample connection connects syringe, the syringe is provided with closure.The utility model is simple in construction, easy to operate, the possibility of electrolyte and air contact is greatly reduced in sampling process, it ensure that and take liquid quality, sample is more representative, simultaneously electrolyte in transfer pipeline can be forbidden to be back to electrolyte bucket by Valve controlling, avoid causing the electrolyte contamination in electrolyte bucket.

Description

A kind of electrolyte sampler
Technical field
Electrolyte equipment manufacturing technology field is the utility model is related to, more specifically a kind of electrolyte sampler.
Background technology
The water of trace, free acid content directly result in the decomposition of electrolyte in electrolyte for lithium ion battery, further make Corrode into battery pole piece, have a strong impact on the performance of battery performance, therefore, it is necessary to be electrolysed to lithium battery in lithium ion battery production Moisture and free acid content in liquid are strictly controlled, and this is just needed during electrolyte is produced, and electrolyte is sampled Moisture test is carried out, current sampling method is first to imported into bottle mode with cover from the bucket for being loaded with electrolyte to carry out Sampling, this sampling mode is not only troublesome in poeration, and extremely causes the moisture in electrolyte absorption air, and test result is caused Deviation.
Utility model content
The utility model is in view of the shortcomings of the prior art, there is provided when one kind is easy to operate, sample rate is fast, electrolyte samples The good sampler of airtight performance.
The utility model realizes solve above-mentioned technical problem by following technological means:
A kind of electrolyte sampler, including electrolyte bucket, probe tube, ready-packaged joint and syringe, the probe tube one Electrolyte bottom of the barrel is stretched at end, probe tube other end connection ready-packaged joint, and the ready-packaged joint is sequentially connected the by delivery pipe One valve, the second valve and raffinate cup, drawing liquid pipeline is connected in the delivery pipe between first valve and the second valve, it is described Drawing liquid pipeline connects sample connection, is provided with the 3rd valve on the drawing liquid pipeline at sample connection, and the sample connection connects Syringe is connect, the syringe is provided with closure.
Preferably, the probe tube and delivery pipe are that transparent polyethylene material is made.
Preferably, the electrolyte bucket upper end side is provided with air inlet pipe, and air inlet pipe is provided with control valve.
The utility model has the advantage of:The utility model sampler, by setting the first valve, the second valve and the It three valves, can be switched by the control of each valve, coordinate injection-tube to complete empty in probe tube and delivery pipe before electrolyte extracts Gas is discharged, and reduces the possibility with air contact in electrolyte extraction process, and the electrolyte purity sampled in syringe is higher, The probability that electrolyte absorbs outside moisture is smaller, and electrolyte sample is more representative, ensure that electrolyte moisture detects Accuracy.
Further, probe tube and delivery pipe are that transparent polyethylene material is made, it can be seen that electrolyte in sampling process Mobility status, be advantageous to control opening and closing and the syringe pump drainage of each valve, the air inlet pipe of electrolyte bucket upper end side is set, electricity When solution liquid bucket electrolyte inside is extracted generation negative pressure, protective gas can be filled with time and carries out ftercompction, is advantageous to the suitable of electrolyte Profit sampling.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Embodiment
It is new below in conjunction with this practicality to make the purpose, technical scheme and advantage of the utility model embodiment clearer Accompanying drawing in type embodiment, the technical scheme in the embodiment of the utility model is clearly and completely described, it is clear that is retouched The embodiment stated is the utility model part of the embodiment, rather than whole embodiments.Based on the implementation in the utility model Example, the every other embodiment that those of ordinary skill in the art are obtained under the premise of creative work is not made, is belonged to The scope of the utility model protection.
As shown in figure 1, a kind of electrolyte sampler, including electrolyte bucket 1, probe tube 2, ready-packaged joint 3 and syringe 5, the bottom of electrolyte bucket 1, the other end of probe tube 2 connection ready-packaged joint 3 are stretched into described one end of probe tube 2, and the ready-packaged joint 3 leads to Cross delivery pipe 9 and be sequentially connected the first valve 6, the second valve 7 and raffinate cup 12, between the valve 7 of the first valve 6 and second Drawing liquid pipeline 11 is connected in delivery pipe, the drawing liquid pipeline 11 connects sample connection 4, connect on the drawing liquid pipeline 11 close to sampling The 3rd valve 8 is provided with first 4, the sample connection 4 connects syringe 5, and the syringe is provided with closure 10, the electrolysis The upper end side of liquid bucket 1 is provided with air inlet pipe 14.
The probe tube 2 and delivery pipe 9 are that transparent polyethylene material is made.
The air inlet pipe 14 is provided with control valve 13.
When the utility model is specifically used, the syringe needle of syringe is stretched into sample connection, opens the first valve and the 3rd Valve, close the second valve, pull syringe, the air in delivery pipe between the first valve and ready-packaged joint and in probe tube Device extraction is injected, electrolyte is also begun to ramp up with pipeline, when liquid to be electrolysed reaches the first valve, closes the first valve, after Continuous pull syringe, air in the connecting line between the first valve, the second valve and the 3rd valve is continued to be evacuated to syringe, After taking out air, the 3rd valve is closed, syringe needle is removed in exhaustjet device after air from ready-packaged joint, connected again It is connected on sample connection, is again turned on the first valve and the 3rd valve and twitches syringe sampling, after sampling terminates, by closure Syringe needle is covered, closes the first valve and the 3rd valve, and removes syringe, opens the second valve by delivery pipe and drawing liquid Electrolyte in pipeline is drained into raffinate cup, effectively prevents that air-discharging not exclusively causes electrolyte to be contaminated in pipeline, returns again A large amount of electrolyte are caused damage when flowing in electrolyte bucket.In electrolyte extraction process, while control valve in air inlet pipe is opened, Air inlet pipe connects nitrogen pot, can carry out pressurising to electrolyte bucket, be advantageous to the smooth sampling of electrolyte.
The utility model sampler, simple in construction, easy to operate, electrolyte can be effectively by the sky in device before extracting Gas is discharged, and ensure that the purity of sampling electrolyte, and sample is more representative, ensure that the accuracy of electrolyte water content detection, The electrolyte remained after sampling in delivery pipe and drawing liquid pipeline is discharged to the collection of raffinate cup, effectively prevent air-discharging in pipeline Not exclusively cause electrolyte to be contaminated, a large amount of electrolyte are caused damage when being back to again in electrolyte bucket.Further, sample Pipe and delivery pipe are that transparent polyethylene material is made, it can be seen that the mobility status of electrolyte, is advantageous to control in sampling process Opening and closing and the syringe pump drainage of each valve are made, the air inlet pipe of electrolyte bucket upper end side is set, and electrolyte bucket electrolyte inside is taken out When going out to produce negative pressure, protective gas can be filled with time and carries out ftercompction, is advantageous to the smooth sampling of electrolyte.
It should be noted that herein, if being used merely in the presence of first and second or the like relational terms by one Individual entity or operation make a distinction with another entity or operation, and not necessarily require or imply these entities or operate it Between any this actual relation or order be present.Moreover, term " comprising ", "comprising" or its any other variant are intended to Cover including for nonexcludability, so that process, method, article or equipment including a series of elements not only include those Key element, but also the other element including being not expressly set out, or also include for this process, method, article or set Standby intrinsic key element.In the absence of more restrictions, the key element limited by sentence "including a ...", it is not excluded that Other identical element in the process including the key element, method, article or equipment also be present.
Above example is only to illustrate the technical solution of the utility model, rather than its limitations;Although with reference to foregoing reality Example is applied the utility model is described in detail, it will be understood by those within the art that:It still can be to preceding State the technical scheme described in each embodiment to modify, or equivalent substitution is carried out to which part technical characteristic;And these Modification is replaced, and the essence of appropriate technical solution is departed from the spirit and model of various embodiments of the utility model technical scheme Enclose.

Claims (3)

1. a kind of electrolyte sampler, it is characterised in that described including electrolyte bucket, probe tube, ready-packaged joint and syringe Electrolyte bottom of the barrel is stretched into probe tube one end, probe tube other end connection ready-packaged joint, the ready-packaged joint by delivery pipe according to It is secondary to connect the first valve, the second valve and raffinate cup, it is connected to drawing liquid in the delivery pipe between first valve and the second valve Pipeline, the drawing liquid pipeline connects sample connection, the 3rd valve is provided with sample connection on the drawing liquid pipeline, described to take Sample joint connects syringe, and the syringe is provided with closure.
2. a kind of electrolyte sampler according to claim 1, it is characterised in that the probe tube and delivery pipe are Transparent polyethylene material is made.
3. a kind of electrolyte sampler according to claim 1, it is characterised in that the electrolyte bucket upper end side is set There is air inlet pipe, air inlet pipe is provided with control valve.
CN201720585039.3U 2017-05-24 2017-05-24 A kind of electrolyte sampler Active CN207007567U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720585039.3U CN207007567U (en) 2017-05-24 2017-05-24 A kind of electrolyte sampler

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720585039.3U CN207007567U (en) 2017-05-24 2017-05-24 A kind of electrolyte sampler

Publications (1)

Publication Number Publication Date
CN207007567U true CN207007567U (en) 2018-02-13

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109060427A (en) * 2018-10-12 2018-12-21 广东华劲金属型材有限公司 A kind of sampler for molten aluminum detection
CN109187109A (en) * 2018-10-12 2019-01-11 安徽兴锂新能源有限公司 A kind of solvent dehydration/purificasystem system and its application method with novel sampling device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109060427A (en) * 2018-10-12 2018-12-21 广东华劲金属型材有限公司 A kind of sampler for molten aluminum detection
CN109187109A (en) * 2018-10-12 2019-01-11 安徽兴锂新能源有限公司 A kind of solvent dehydration/purificasystem system and its application method with novel sampling device

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