CN206960445U - The detection means of iron content in a kind of carbonyl nickel liquid - Google Patents
The detection means of iron content in a kind of carbonyl nickel liquid Download PDFInfo
- Publication number
- CN206960445U CN206960445U CN201720863377.9U CN201720863377U CN206960445U CN 206960445 U CN206960445 U CN 206960445U CN 201720863377 U CN201720863377 U CN 201720863377U CN 206960445 U CN206960445 U CN 206960445U
- Authority
- CN
- China
- Prior art keywords
- reagent bottle
- detection means
- end socket
- air inlet
- pipe
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- 238000001514 detection method Methods 0.000 title claims abstract description 22
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 title claims abstract description 19
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 title claims abstract description 17
- 239000007788 liquid Substances 0.000 title claims abstract description 16
- 229910052742 iron Inorganic materials 0.000 title claims abstract description 9
- 239000003153 chemical reaction reagent Substances 0.000 claims abstract description 56
- 238000007789 sealing Methods 0.000 claims abstract description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 8
- 229910052757 nitrogen Inorganic materials 0.000 claims description 4
- 230000000295 complement effect Effects 0.000 claims description 3
- 239000002699 waste material Substances 0.000 claims description 3
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 9
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 125000002915 carbonyl group Chemical group [*:2]C([*:1])=O 0.000 abstract description 4
- 230000007547 defect Effects 0.000 abstract description 4
- 229910052759 nickel Inorganic materials 0.000 abstract description 4
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000006073 displacement reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000012544 monitoring process Methods 0.000 description 1
- 238000005496 tempering Methods 0.000 description 1
Abstract
The utility model discloses a kind of detection means of iron content in carbonyl nickel liquid, the device includes reagent bottle, reagent bottle end socket, vacuum extractor, air inlet pipe, feed tube and escape pipe, reagent bottle end socket is covered on the reagent bottle, and sealing ring is provided between reagent bottle bottleneck and reagent bottle end socket；Vacuum extractor, air inlet pipe, feed tube and escape pipe are connected by reagent bottle end socket with reagent bottle respectively；Valve is equipped with air inlet pipe, feed tube and escape pipe.Detection means of the present utility model, the content of ferro element in the process system of carbonyl process production nickel can be monitored in real time, technological parameter is adjusted in time, reduces the defect rate of product, the structure of device is simple, practical.
Description
Technical field
The utility model belongs to testing equipment field, and in particular to the detection means of iron content in a kind of carbonyl nickel liquid.
Background technology
During carbonyl process production nickel, impurity content is few in product, but iron is not easily removed, therefore, in production process
In monitoring to ferro element be particularly important.In existing production process, due to the hypertoxicity of carbonyl iron, carbonyl nickel, ferro element
Detection process is limited, and is caused after ferro element is exceeded in product, then technological parameter is adjusted.Technological parameter is adjusted in whole process
It is whole not in time, cause product defect rate high.
The content of the invention
The purpose of the utility model is to be directed to above-mentioned technical deficiency, there is provided one kind can detect carbonyl process production nickel technique in real time
The device of iron content in system, it is easy in time be adjusted technological parameter, reduces the defect rate of product.
To achieve the above object, the utility model uses following technical proposals：
The detection means of iron content in a kind of carbonyl nickel liquid, it is characterised in that the device includes reagent bottle, reagent bottle seals
Head, vacuum extractor, air inlet pipe, feed tube and escape pipe, the reagent bottle end socket is covered on the reagent bottle, and reagent bottle bottle
Sealing ring is provided between mouth and reagent bottle end socket；The vacuum extractor, air inlet pipe, feed tube and escape pipe are by described
Reagent bottle end socket is connected with reagent bottle；Valve is equipped with described air inlet pipe, feed tube and escape pipe.
According to above-mentioned detection means, it is characterised in that in described air inlet pipe, by media flow direction in pipe, according to
It is secondary to be provided with intake valve, non-return valve and intake valve；Two liquid feed valves are provided with described feed tube；On described escape pipe,
By media flow direction in pipe, air outlet valve, non-return valve and air outlet valve are sequentially provided with.
According to above-mentioned detection means, it is characterised in that the reagent bottle top is provided with external screw thread, the reagent bottle end socket
Provided with the internal thread to match with the external screw thread, described reagent bottle and reagent bottle end socket are connected through a screw thread.
According to above-mentioned detection means, it is characterised in that the air inlet pipe is connected with nitrogen pipeline, and the feed tube is with needing
The system connection of detection, the escape pipe are connected with waste line.
According to above-mentioned detection means, it is characterised in that the body of the reagent bottle is provided with double complementary scale.
The beneficial effects of the utility model：
The detection means of ferro element in carbonyl nickel liquid of the present utility model, the technique that carbonyl process production nickel can be monitored in real time
The content of ferro element, is adjusted to technological parameter in time in system, reduces the defect rate of product, and the structure of device is simple, real
It is strong with property.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model.
Embodiment
Fig. 1 is structural representation of the present utility model.As shown in figure 1, iron content in carbonyl nickel liquid of the present utility model
Detection means include reagent bottle 11, the inside of reagent bottle 11 is equipped with quantitative reagent 12.Detection means also include reagent bottle end socket 21,
Reagent bottle sealing ring 22, reagent bottle end socket 21 are covered on reagent bottle 11, and sealing ring 22 is arranged on the bottleneck of reagent bottle 11 and reagent bottle
Between end socket 21.Detection means also includes vacuum extractor 61, air inlet pipe 51, feed tube 31 and escape pipe 41, vacuum plant 61,
Air inlet pipe 51, feed tube 31 and escape pipe 41 are connected by reagent bottle end socket 21 with reagent bottle 11 respectively, feed tube 31 it is another
End is connected with the system that need to be detected, and waste line connects in the other end of escape pipe 41 and field, the other end of air inlet pipe 51 and field
Interior nitrogen pipeline connection.
Valve is equipped with air inlet pipe 51, feed tube 31 and escape pipe 41, particularly, by media flow direction in pipe, is entered
Tracheae 51 is provided with intake valve 52, non-return valve 53 and intake valve 54, and feed tube 31 is provided with two liquid feed valves 32,33, escape pipe
Air outlet valve 42, non-return valve 43 and air outlet valve 44 are sequentially provided with 41.
Reagent bottle 11 of the present utility model is handled by tempering.Particularly, reagent bottle 11 and reagent bottle end socket 21 pass through spiral shell
Line connects, i.e. the top of reagent bottle 11 is provided with external screw thread, and reagent bottle end socket 21 is provided with the internal thread to match with external screw thread.Reagent
11 bodies of bottle are provided with double complementary scale, make metering more accurate.
The utility model when in use, closes all valves, by reagent bottle 11 and reagent bottle equipped with a certain amount of reagent 12
End socket 21 fastens, and first opens air outlet valve 42 and air outlet valve 44, then, opens intake valve 52 and intake valve 54, is tried with nitrogen displacement
Gas in agent bottle 11, after a period of time, intake valve 52 and intake valve 53 are closed, closes air outlet valve 42 and air outlet valve 44, then instead
Multiple pull vacuum extractor 61 several times, reduce pressure in reagent bottle 11, then turn on liquid feed valve 32 and liquid feed valve 33, at one section
Between after, close liquid feed valve 32, liquid feed valve 33, finally, reagent bottle 11 is screwed off from reagent bottle end socket 21, detection of taking away.
Claims (5)
1. the detection means of iron content in a kind of carbonyl nickel liquid, it is characterised in that the device includes reagent bottle, reagent bottle seals
Head, vacuum extractor, air inlet pipe, feed tube and escape pipe, the reagent bottle end socket is covered on the reagent bottle, and reagent bottle bottle
Sealing ring is provided between mouth and reagent bottle end socket；The vacuum extractor, air inlet pipe, feed tube and escape pipe are respectively by described
Reagent bottle end socket be connected with reagent bottle；Valve is equipped with described air inlet pipe, feed tube and escape pipe.
2. detection means according to claim 1, it is characterised in that in described air inlet pipe, by media flow in pipe
Direction, it is sequentially provided with intake valve, non-return valve and intake valve；Two liquid feed valves are provided with described feed tube；Go out in described
On tracheae, by media flow direction in pipe, air outlet valve, non-return valve and air outlet valve are sequentially provided with.
3. detection means according to claim 1, it is characterised in that the reagent bottle top is provided with external screw thread, the examination
Agent bottle end socket is provided with the internal thread to match with the external screw thread, and described reagent bottle and reagent bottle end socket are connected through a screw thread.
4. detection means according to claim 1, it is characterised in that the air inlet pipe is connected with nitrogen pipeline, it is described enter
Liquid pipe is connected with the system that need to be detected, and the escape pipe is connected with waste line.
5. detection means according to claim 1, it is characterised in that the body of the reagent bottle is provided with double complementary quarter
Degree.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720863377.9U CN206960445U (en) | 2017-07-17 | 2017-07-17 | The detection means of iron content in a kind of carbonyl nickel liquid |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720863377.9U CN206960445U (en) | 2017-07-17 | 2017-07-17 | The detection means of iron content in a kind of carbonyl nickel liquid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206960445U true CN206960445U (en) | 2018-02-02 |
Family
ID=61383944
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720863377.9U Active CN206960445U (en) | 2017-07-17 | 2017-07-17 | The detection means of iron content in a kind of carbonyl nickel liquid |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206960445U (en) |
-
2017
- 2017-07-17 CN CN201720863377.9U patent/CN206960445U/en active Active
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20240204 Address after: 737100 No. 2 Lanzhou Road, Beijing Road Street, Jinchuan District, Jinchang City, Gansu Province Patentee after: Jinchuan Group Nickel Cobalt Co.,Ltd. Country or region after: China Address before: 737103 No. 98, Jinchuan Road, Jinchang, Gansu Patentee before: JINCHUAN GROUP Co.,Ltd. Country or region before: China |
|
| TR01 | Transfer of patent right |