CN206930616U - A kind of Film electrode dissolved oxygen meter on-line calibration device - Google Patents
A kind of Film electrode dissolved oxygen meter on-line calibration device Download PDFInfo
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- CN206930616U CN206930616U CN201720799531.0U CN201720799531U CN206930616U CN 206930616 U CN206930616 U CN 206930616U CN 201720799531 U CN201720799531 U CN 201720799531U CN 206930616 U CN206930616 U CN 206930616U
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- reactive tank
- appendix
- electrode
- dissolved oxygen
- oxygen
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- 239000001301 oxygen Substances 0.000 title claims abstract description 41
- 229910052760 oxygen Inorganic materials 0.000 title claims abstract description 41
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 title claims abstract description 40
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000003756 stirring Methods 0.000 claims abstract description 13
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 12
- 238000006243 chemical reaction Methods 0.000 claims abstract description 7
- 239000011521 glass Substances 0.000 claims description 4
- 239000007789 gas Substances 0.000 abstract description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 4
- 239000007788 liquid Substances 0.000 description 3
- 238000000034 method Methods 0.000 description 3
- 230000005540 biological transmission Effects 0.000 description 2
- 238000002848 electrochemical method Methods 0.000 description 2
- 238000005516 engineering process Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000005273 aeration Methods 0.000 description 1
- 238000004458 analytical method Methods 0.000 description 1
- 238000006701 autoxidation reaction Methods 0.000 description 1
- 230000004071 biological effect Effects 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 238000004737 colorimetric analysis Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000002795 fluorescence method Methods 0.000 description 1
- 230000014759 maintenance of location Effects 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000010865 sewage Substances 0.000 description 1
- 239000010802 sludge Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
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- Sampling And Sample Adjustment (AREA)
Abstract
The utility model discloses a kind of Film electrode dissolved oxygen meter on-line calibration device, it is related to Film electrode dissolved oxygen meter field, including reactive tank, the reactive tank is externally provided with oxygen cylinder and nitrogen cylinder, the oxygen cylinder bottleneck and nitrogen cylinder bottleneck are respectively equipped with flow control switch, the flow control switch top is connected with appendix, the appendix is stretched into reactive tank, and stretch out reactive tank along reaction tank bottom, appendix upper surface in reactive tank is provided with some apertures, solution to be measured is filled in the reactive tank, stirring rod is placed with the solution, normal electrode and it is calibrated electrode.The controlling switch on oxygen cylinder and nitrogen cylinder is opened simultaneously, and the flow of gas is controlled, after two gases is mixed, the concentration of oxygen is not more than the concentration after solution oxygen saturation to be measured, measure record standard electrode and be calibrated electrode reading, two group number-readings of contrast to calibration electrodes to calibrating.
Description
Technical field
Film electrode dissolved oxygen meter field is the utility model is related to, specially a kind of Film electrode dissolved oxygen meter
On-line calibration device.
Background technology
Oxygen content in water can fully show the degree of water self-cleaning.For the biological treatment plant using activated sludge,
It is extremely important to understand the oxygen content of aeration tank, dirty dissolved oxygen in water increase, the biological activity in addition to anaerobe can be promoted, because
And volatile materials can be removed and be easy to the ion of autoxidation, it is purified sewage, measure oxygen content mainly there are three kinds of sides
Method:Automatic colorimetric analysis and chemical analysis measurement, are typically adopted along magnetic survey, electrochemical measurement, fluorescence method, dissolved oxygen in water
With electrochemical measurement, conventional calibration methods existence time is long, efficiency is low, dissolved oxygen standard value is unstable, uneven, finally leads
Measurement is caused deviation occur.
Utility model content
The utility model purpose is to provide a kind of Film electrode dissolved oxygen meter on-line calibration device, above-mentioned to solve
The problem of being proposed in background technology.
A kind of Film electrode dissolved oxygen meter on-line calibration device, including reactive tank, the reactive tank are externally provided with oxygen
Bottle and nitrogen cylinder, the oxygen cylinder bottleneck and nitrogen cylinder bottleneck are respectively equipped with flow control switch, on the flow control switch
Portion is connected with appendix, and the appendix is stretched into reactive tank, and stretches out reactive tank along reaction tank bottom, the gas transmission in reactive tank
Pipe upper surface is provided with some apertures, and solution to be measured is filled in the reactive tank, be placed with the solution stirring rod, normal electrode and
It is calibrated electrode.
Preferably, the reactive tank is isothermal reaction groove.
Preferably, the stirring rod is glass stirring rod.
Preferably, the appendix is rubber hose.
The utility model has the advantage of:It is simple in construction, it is easy to operate, intuitively it can find out whether be calibrated electrode very
Standard, while the controlling switch on oxygen cylinder and nitrogen cylinder is opened, and the flow of gas is controlled, two gases is mixed
Afterwards, the concentration of oxygen is not more than the concentration after solution oxygen saturation to be measured, and mixed gas is passed through in reactive tank along appendix,
Gas transmission pipe surface, which is provided with some apertures, can be such that mixed gas maximumlly enters in solution, and stirring rod can help oxygen quick
Solve homogeneously in prepare liquid, improve operating efficiency, saved the time.
Brief description of the drawings
Fig. 1 is a kind of Film electrode dissolved oxygen meter on-line calibration structure drawing of device described in the utility model.
Wherein:1-reactive tank, 2-oxygen cylinder, 3-nitrogen cylinder, 4-flow control switch, 5-appendix, 6-by school
Collimator electrode, 7-calibration electrodes, 8-stirring rod.
Embodiment
To be easy to understand technological means, creation characteristic, reached purpose and effect of the present utility model, with reference to
Embodiment, the utility model is expanded on further.
As shown in figure 1, a kind of Film electrode dissolved oxygen meter on-line calibration device, including reactive tank 1, the reactive tank
1 is externally provided with oxygen cylinder 2 and nitrogen cylinder 3, and the bottleneck of oxygen cylinder 2 and nitrogen cylinder 3 bottleneck is respectively equipped with flow control switch 4, institute
State the top of flow control switch 4 and be connected with appendix 5, the appendix 5 is stretched into reactive tank 1, and is stretched along the bottom of reactive tank 1
Go out reactive tank 1, the upper surface of appendix 5 in reactive tank 1 is provided with some apertures, and solution to be measured is filled in the reactive tank 1, described
Stirring rod 8, normal electrode 7 are placed with solution and is calibrated electrode 6.
In the present embodiment, the reactive tank 1 is isothermal reaction groove, and isothermal reaction groove has solution temperature in retention groove permanent
The characteristics of determining, avoid because the change of solution temperature causes the difference of oxygen content.
In the present embodiment, the stirring rod 8 is glass stirring rod, and glass bar is not easy to react with solution.
In the present embodiment, the appendix 5 is rubber hose.
Operation principle and methods:The controlling switch 4 on oxygen cylinder 2 and nitrogen cylinder 3 is opened simultaneously, and controls gas
Flow, after two gases is mixed, the concentration of oxygen is not more than the concentration after solution oxygen saturation to be measured, by mixed gas
It is passed through along appendix 5 in reactive tank 1, the surface of appendix 5, which is provided with some apertures, can make mixed gas maximumlly into molten
In liquid, stirring rod 8 can help oxygen Quick uniform to be dissolved in prepare liquid, improve operating efficiency, save the time, will mark
Collimator electrode 7 is placed in solution to be measured, observes the reading of simultaneously record standard electrode, then will be calibrated electrode 6 and be placed in solution to be measured,
Observe and record and be calibrated electrode reading, adjust mixed gas concentration, measure again, obtain two group number-readings and contrasted, if
Reading is consistent, then is calibrated the accuracy of reading of electrode 6, if it is different, then explanation is calibrated the read untrue of electrode 6.
As known by the technical knowledge, the utility model can pass through other essence without departing from its spirit or the reality of essential feature
Scheme is applied to realize.Therefore, embodiment disclosed above, for each side, all it is merely illustrative, is not only
's.It is all in the scope of the utility model or in the change being equal in the scope of the utility model by the utility model bag
Contain.
Claims (4)
1. a kind of Film electrode dissolved oxygen meter on-line calibration device, including reactive tank, it is characterised in that outside the reactive tank
Provided with oxygen cylinder and nitrogen cylinder, the oxygen cylinder bottleneck and nitrogen cylinder bottleneck are respectively equipped with flow control switch, the flow control
System switch top is connected with appendix, and the appendix is stretched into reactive tank, and stretches out reactive tank, reactive tank along reaction tank bottom
Interior appendix upper surface is provided with some apertures, and solution to be measured is filled in the reactive tank, and stirring rod, mark are placed with the solution
Collimator electrode and it is calibrated electrode.
2. a kind of Film electrode dissolved oxygen meter on-line calibration device according to claim 1, it is characterised in that described
Reactive tank is isothermal reaction groove.
3. a kind of Film electrode dissolved oxygen meter on-line calibration device according to claim 1, it is characterised in that described
Stirring rod is glass stirring rod.
4. a kind of Film electrode dissolved oxygen meter on-line calibration device according to claim 1, it is characterised in that described
Appendix is rubber hose.
Priority Applications (1)
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CN201720799531.0U CN206930616U (en) | 2017-07-03 | 2017-07-03 | A kind of Film electrode dissolved oxygen meter on-line calibration device |
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CN201720799531.0U CN206930616U (en) | 2017-07-03 | 2017-07-03 | A kind of Film electrode dissolved oxygen meter on-line calibration device |
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Publication Number | Publication Date |
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CN206930616U true CN206930616U (en) | 2018-01-26 |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110082488A (en) * | 2019-04-19 | 2019-08-02 | 山西省计量科学研究院 | A kind of dissolved oxygen metering calibrating installation and method |
CN112858613A (en) * | 2021-01-20 | 2021-05-28 | 北京华科仪科技股份有限公司 | Device for calibrating trace dissolved oxygen monitor on line and operation method thereof |
CN113916849A (en) * | 2021-09-10 | 2022-01-11 | 山东省科学院海洋仪器仪表研究所 | Calibration method and calibration device for optical dissolved oxygen sensor |
-
2017
- 2017-07-03 CN CN201720799531.0U patent/CN206930616U/en active Active
Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110082488A (en) * | 2019-04-19 | 2019-08-02 | 山西省计量科学研究院 | A kind of dissolved oxygen metering calibrating installation and method |
CN112858613A (en) * | 2021-01-20 | 2021-05-28 | 北京华科仪科技股份有限公司 | Device for calibrating trace dissolved oxygen monitor on line and operation method thereof |
CN112858613B (en) * | 2021-01-20 | 2023-08-22 | 北京华科仪科技股份有限公司 | Device for calibrating trace dissolved oxygen monitor on line and operation method thereof |
CN113916849A (en) * | 2021-09-10 | 2022-01-11 | 山东省科学院海洋仪器仪表研究所 | Calibration method and calibration device for optical dissolved oxygen sensor |
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Address after: Room B01-02, Room 401, Building 1, No. 1 Nanxiang Second Road, Huangpu District, Guangzhou City, Guangdong Province, 510670 Patentee after: Guangzhou Guangwei Metrology Testing Technology Co.,Ltd. Country or region after: China Address before: Room 202, Building 2, No. 232 Kezhu Road, Science City, Guangzhou Economic and Technological Development Zone, Guangdong Province, 510000 Patentee before: GUANGDONG PUBIAO TECHNOLOGY RESEARCH CO.,LTD. Country or region before: China |