CN206910869U - The dichloromethane extraction equipment of wet method barrier film manufacture - Google Patents

The dichloromethane extraction equipment of wet method barrier film manufacture Download PDF

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Publication number
CN206910869U
CN206910869U CN201720895427.1U CN201720895427U CN206910869U CN 206910869 U CN206910869 U CN 206910869U CN 201720895427 U CN201720895427 U CN 201720895427U CN 206910869 U CN206910869 U CN 206910869U
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China
Prior art keywords
extraction equipment
barrier film
wet method
dichloromethane extraction
baffle plate
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CN201720895427.1U
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Chinese (zh)
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周吕松
彭立群
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SUZHOU GREENPOWER NEW ENERGY MATERIALS CO Ltd
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SUZHOU GREENPOWER NEW ENERGY MATERIALS CO Ltd
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Abstract

The utility model provides a kind of dichloromethane extraction equipment of wet method barrier film manufacture, and its flooding velocity is very fast.A kind of dichloromethane extraction equipment of wet method barrier film manufacture, groove including offering multiple recovery ports, the front portion of the groove is further opened with extractant entrance, in the groove multiple baffle plates are arranged at intervals with from A-P, each baffle plate has a upper surface for being used for overflowing for tank liquid respectively, and the upper surface of the baffle plate of front side higher than the baffle plate of rear side upper surface and in it is preceding it is high after it is low stepped.

Description

The dichloromethane extraction equipment of wet method barrier film manufacture
Technical field
The utility model belongs to wet method lithium battery diaphragm manufacturing equipment field, and in particular to a kind of wet method barrier film manufacture Dichloromethane extraction equipment.
Background technology
In lithium battery industry wet method barrier film manufacturing process, extraction process is that the barrier film cavity technique of current main flow prepares skill Art.In order to analyze the auxiliary material contained in barrier film paraffin oil from product, extraction process is essential link. Due to production line balance, the starting paraffin oil contained in product can constantly be extracted agent(Dichloromethane)Extract, mix In extractant so that oil content is more and more in extractant, will soon have influence on the effect of extracting of extractant.So adding While the internal circulating load of big extractant, improving the flushing effect of extract in extraction equipment can cause extractant to keep connecting well Continue stable extraction, the stability that can also allow product to keep.
The content of the invention
In view of the above-mentioned problems, the dichloromethane extraction that the purpose of this utility model is to provide a kind of wet method barrier film manufacture is set Standby, its flooding velocity is very fast.
In order to solve the above technical problems, the technical solution adopted in the utility model is:
A kind of dichloromethane extraction equipment of wet method barrier film manufacture, including the groove of multiple recovery ports is offered, the groove Front portion be further opened with extractant entrance, is arranged at intervals with multiple baffle plates from A-P in the groove, each baffle plate difference With the upper surface for being overflowed for tank liquid, and the upper surface of the baffle plate of front side is upper higher than the baffle plate of rear side End face and in low stepped after preceding high.
Preferably, the number of the baffle plate is n, and the groove is divided into n+1 overflow unit.
It is highly preferred that being offered on the baffle plate allows tank liquid to flow to i+1 overflow list from i-th of overflow unit The hole of member, wherein i are the positive integer less than or equal to n-1.
It is highly preferred that the bottom of each overflow unit offers described recovery port respectively.
It is highly preferred that the dichloromethane extraction equipment also includes the recovery tube for connecting the recovery port.
Further, the dichloromethane extraction equipment includes multiple for connecting the recovery tube and each recovery port Branch pipe, be respectively arranged with tapping valve on each branch pipe.
Preferably, the height of each baffle plate is 7-10m.
The utility model uses above-mentioned technical proposal, has the following advantages that compared with prior art:
Extractant dichloromethane is to flow to behind rear end to be extracted what Recovery and recycle utilized from the front end of groove, and is extracted Starting paraffin oil due to density ratio extractant dichloromethane it is small, dichloromethane upper surface is floated over, according to liquid from eminence The principle of lower is flow to, the overflow unit of step-like arrangement is gone out by the barrier partitions just to differ, using Ladder Overflow method, Extractant can overflow to increasingly lower step along first step of highest, and the paraffin oil on extractant surface also can be most thorough Bottom along step step by step overflow to last overflow unit, be finally recovered, overflow is enhanced, and flooding velocity is fast, The circulation of extractant is preferable.
Brief description of the drawings
, below will be to needed for embodiment description in order to illustrate more clearly of the technical scheme in the embodiment of the utility model The accompanying drawing to be used is briefly described, it should be apparent that, drawings in the following description are only some realities of the present utility model Example is applied, for those of ordinary skill in the art, on the premise of not paying creative work, can also be according to these accompanying drawings Other accompanying drawings are obtained, wherein:
Fig. 1 is a kind of structural representation of dichloromethane extraction equipment.
Wherein, 1, groove;10th, overflow unit;2nd, extractant entrance;3rd, recovery port;4th, baffle plate;40th, upper surface;5th, reclaim Pipe;6th, it is in charge of;7th, tapping valve.
Embodiment
Preferred embodiment of the present utility model is described in detail below in conjunction with the accompanying drawings, so that the advantages of the utility model It can be easier to be understood by the person skilled in the art with feature, it is apparent bright so as to be made to the scope of protection of the utility model True defines.The right side of paper, left side in Fig. 1 are corresponded respectively to before and after being addressed in the utility model.
The present embodiment provides a kind of dichloromethane extraction equipment of wet method barrier film manufacture, and it is used for barrier film Central Plains work stone Wax oil extract and on barrier film pore-forming.Shown in reference picture 1, a kind of dichloromethane extraction equipment of wet method barrier film manufacture, Groove 1 including offering multiple recovery ports 3, the front portion of groove 1 are further opened with extractant entrance 2, and extractant is specially dichloromethane. Multiple baffle plates 4 are provided with equal intervals from A-P in groove 1.Baffle plate 4 is fixed in groove 1 vertically, and each baffle plate 4 has respectively to be used for The upper surface 40 overflowed for liquid in groove 1, in addition to upper surface 40, other end faces of each baffle plate 4 and the inwall of groove 1 connect. The upper surface 40 of the baffle plate 4 of front side is higher than the upper surface 40 of the baffle plate 4 of rear side, in other words, the upper surface of above-mentioned multiple baffle plates 4 40 reduce successively from A-P, form in ladder low after preceding height.
The number of baffle plate 4 is n, and groove 1 is divided into n+1 overflow unit 10.Corresponding in Fig. 1, n=5, then the sky in groove 1 Between by 5 baffle plates 4 be separated into 6 overflow units 10.Being offered on baffle plate 4 allows liquid in groove 1 to be flowed from i-th of overflow unit 10 To the hole of i+1 overflow unit 10, wherein i is the positive integer less than or equal to n-1, that is to say, that is opened on each baffle plate 4 Located at hole.Direction shown in oil slick and debris along each arrow positioned at upper strata is successively from the overflow of upper surface 40 of each baffle plate 4 under One overflow unit 10, and the dichloromethane extractant positioned at lower floor then flows into next overflow unit 10 by the hole on baffle plate 4.
The recovery port 3 that the bottom of each overflow unit 10 offers respectively.Dichloromethane extraction equipment also includes connecting back The recovery tube 5 of closing in 3.Dichloromethane extraction equipment include it is multiple be used to connect recovery tube 5 and the branch pipe 6 of each recovery port 3, each Tapping valve 7 is respectively arranged with pipe 6.
If such as prior art, overall liquid level in groove 1 is all horizontal, and whole liquid level joins together, and area is big, no But overflow is slow, and the oil slick of extractant upper surface can due to adhesion to act on being internally formed for extraction equipment many quiet Dead angle only, oil slick and debris are difficult thoroughly to be overflowed to be recovered below.Based on this, dichloromethane extraction of the present utility model Taking equipment is designed to that the height of baffle plate 4 between several overflow units 10 is different, forms the step of same gradient, such extractant enters After entering extraction equipment, because the extractant of circulation can only enter first namely liquid level highest overflow unit 10 at first, this The extractant of sample miscella paraffin oil will be quickly overflow into second, the 3rd ... a to the last overflow Groove 1, and the paraffin oil and debris of extractant upper surface also due to flow velocity accelerate and thoroughly with extractant overflow to the end And be finally recycled, so recycling of the Ladder Overflow method to extractant in extraction equipment can improve 300% effect.
In extraction equipment, extractant dichloromethane is after one end of slave unit flows to the other end with extractant at leisure It is extracted what Recovery and recycle utilized, and the starting paraffin oil extracted is because density ratio extractant dichloromethane is small, is floating In dichloromethane upper surface, so being to solve extraction to allow the paraffin oil of extractant upper surface to overflow as soon as possible and be recovered The fundamental way of problem is taken, so flowing to the principle of lower from eminence according to liquid, enters from extractant in equipment and uses rank Terraced press over system, groove 1 is separated into several overflow units 10, and the upper end of baffle plate 4 forms the different step of height, and according to The relation of hydrodynamics and flowing velocity, the rate equation of liquid flowing be p+ ρ gh+ (1/2) * ρ v^2=c, p, ρ, v difference in formula For the pressure of fluid, density and speed;H is plumb height;G is acceleration of gravity;C is constant, in the same situation of p, ρ, v Under, h is bigger, and fluid velocity is faster, can only be maximum in the finiteness and the finiteness of instrument size in view of extractant usage amount The raising h of limit improves overflow, and such extractant can overflow to increasingly lower step along first step of highest, and The paraffin oil on extractant surface also most can thoroughly overflow to last groove 1 a step by a step along step, finally be recovered machine Recovery, and h considers cost and volume in device fabrication, typically in 7-10mm.Thus, the height of each baffle plate 4 is 7-10m, And the difference in height of arbitrary neighborhood baffle plate 4 is consistent.
Above-described embodiment is a kind of preferred embodiment only to illustrate technical concepts and features of the present utility model, its mesh Be to allow person skilled in the art to understand content of the present utility model and implement according to this, can not limit this with this The protection domain of utility model.All equivalent change or modifications made according to Spirit Essence of the present utility model, should all cover Within the scope of protection of the utility model.

Claims (7)

1. a kind of dichloromethane extraction equipment of wet method barrier film manufacture, including the groove of multiple recovery ports is offered, the groove Front portion is further opened with extractant entrance, it is characterised in that:Multiple baffle plates are arranged at intervals with from A-P in the groove, it is each described Baffle plate has the upper surface for being used for overflowing for tank liquid respectively, and the upper surface of the baffle plate of front side is described higher than rear side The upper surface of baffle plate and in low stepped after preceding high.
2. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 1, it is characterised in that:The baffle plate Number be n, the groove is divided into n+1 overflow unit.
3. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 2, it is characterised in that:The baffle plate On offer and allow tank liquid to flow to the hole of i+1 overflow unit from i-th of overflow unit, wherein i for less than or equal to N-1 positive integer.
4. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 2, it is characterised in that:It is each described The bottom of overflow unit offers described recovery port respectively.
5. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 2, it is characterised in that:The dichloro Methane extraction equipment also includes the recovery tube for connecting the recovery port.
6. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 5, it is characterised in that:The dichloro Methane extraction equipment is used to connect the recovery tube and the branch pipe of each recovery port including multiple, is set respectively on each branch pipe It is equipped with tapping valve.
7. the dichloromethane extraction equipment of wet method barrier film manufacture according to claim 1, it is characterised in that:Each gear The height of plate is 7-10m.
CN201720895427.1U 2017-07-21 2017-07-21 The dichloromethane extraction equipment of wet method barrier film manufacture Active CN206910869U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720895427.1U CN206910869U (en) 2017-07-21 2017-07-21 The dichloromethane extraction equipment of wet method barrier film manufacture

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720895427.1U CN206910869U (en) 2017-07-21 2017-07-21 The dichloromethane extraction equipment of wet method barrier film manufacture

Publications (1)

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CN206910869U true CN206910869U (en) 2018-01-23

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110038319A (en) * 2019-02-13 2019-07-23 江苏北星新材料科技有限公司 A kind of wet process lithium ion battery separator extraction equipment overflow mechanism

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110038319A (en) * 2019-02-13 2019-07-23 江苏北星新材料科技有限公司 A kind of wet process lithium ion battery separator extraction equipment overflow mechanism
CN110038319B (en) * 2019-02-13 2023-12-26 江苏北星新材料科技有限公司 Overflow device for wet lithium ion battery diaphragm extraction equipment

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