CN206897394U - A kind of normal-pressure balance kettle - Google Patents

A kind of normal-pressure balance kettle Download PDF

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Publication number
CN206897394U
CN206897394U CN201720504126.1U CN201720504126U CN206897394U CN 206897394 U CN206897394 U CN 206897394U CN 201720504126 U CN201720504126 U CN 201720504126U CN 206897394 U CN206897394 U CN 206897394U
Authority
CN
China
Prior art keywords
kettle
agitating shaft
stirring rod
water pump
side wall
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720504126.1U
Other languages
Chinese (zh)
Inventor
王群乐
吕起
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Jiangxi Pinhan Chemical Industry Co Ltd
Original Assignee
Jiangxi Pinhan Chemical Industry Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Jiangxi Pinhan Chemical Industry Co Ltd filed Critical Jiangxi Pinhan Chemical Industry Co Ltd
Priority to CN201720504126.1U priority Critical patent/CN206897394U/en
Application granted granted Critical
Publication of CN206897394U publication Critical patent/CN206897394U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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  • Mixers Of The Rotary Stirring Type (AREA)
  • Physical Or Chemical Processes And Apparatus (AREA)

Abstract

The utility model discloses a kind of normal-pressure balance kettle, including kettle and agitating shaft, charging aperture and condenser interface are provided with the top of the kettle, the side wall of the kettle is provided with inlet and liquid outlet, the top of the kettle side wall is provided with the first sample tap, the bottom of the kettle side wall is provided with the second sample tap, the agitating shaft is hollow structure, stirring rod is fixedly connected with the outer circumference surface of the agitating shaft, the stirring rod is hollow structure and connected with the agitating shaft, the stirring rod is provided with some through holes, the opening direction of the through hole is consistent with the direction of rotation of the agitating shaft, bottom in the kettle is provided with pedestal, water pump is provided with the pedestal, one end of the water pump connects with the agitating shaft, the upper surface that the other end of the water pump passes through pedestal described in pipeline communication.The liquid of different height liquid level in equilibrium still is stirred by the utility model, while is sucked bottom and circulated, and is improved to highly viscous fluid mixing effect, is accelerated reaction speed.

Description

A kind of normal-pressure balance kettle
Technical field
A kind of reactor is the utility model is related to, is specifically related to a kind of normal-pressure balance kettle.
Background technology
Reactor is usually used in the industries such as petrochemical industry, rubber, agricultural chemicals, medicine, to complete sulfonation, nitrification, hydrogenation, hydrocarbon The technical process such as change, polymerization, condensation, and the consersion unit of many other technical process of organic dyestuff and intermediate.Solid-liquid It is to solve the problems, such as the indispensable basic data of actual Crystallization Separation to balance each other, and Liquid-liquid equilibrium data are the main of extracting operation Foundation, the acquisition of equilibrium criterion depend on measuring at present, and equilibrium still is the important experimental facilities for determining equilibrium criterion.
For equilibrium still common at present more using temperature survey is carried out in thermometer intercalation reaction kettle, measurement error is larger, and It is easily damaged, the big agitation for influenceing agitating device in reactor of space-consuming, it is impossible to the portion of reaction gas reactor, liquid layered Divide and be measured respectively.In addition, the more of existing reactor carry out stirring in a certain aspect using general stirring apparatus to liquid Mix, it is impossible to superposed layering and the layering of bottom is quickly uniformly mixed, it is not ideal to highly viscous fluid mixing effect, Stirring needs time-consuming longer.
The content of the invention
The utility model devises a kind of normal-pressure balance kettle in view of the shortcomings of the prior art.
The utility model is realizes object above, using following scheme:A kind of normal-pressure balance kettle, including kettle and stirring Axle, the kettle top are provided with charging aperture and condenser interface, and the side wall of the kettle is provided with inlet and liquid outlet, the kettle The top of body sidewall is provided with the first sample tap, and the bottom of the kettle side wall is provided with the second sample tap, and the agitating shaft is hollow Structure, stirring rod is fixedly connected with the outer circumference surface of the agitating shaft, the stirring rod is vertical with the agitating shaft, described to stir Rod is mixed as hollow structure and is connected with the agitating shaft, the stirring rod is provided with some through holes, the opening direction of the through hole Consistent with the direction of rotation of the agitating shaft, the bottom in the kettle is provided with pedestal, and water pump, the water are provided with the pedestal One end of pump connects with the agitating shaft, the upper surface that the other end of the water pump passes through pedestal described in pipeline communication.
Further, the top and bottom in the kettle are respectively equipped with the first temperature sensor and second temperature sensing Device, for measuring the temperature of upper gas and lower liquid, and small volume respectively, the rotation of agitating device is not influenceed.
Further, the kettle is stainless steel.
Further, the stirring rod is 2 groups, is separately positioned on the upper and lower part of the agitating shaft, in same aspect Stirring rod can set 2 or more than 2, being spaced certain angle between horizontally adjacent stirring rod is uniformly arranged.
Compared to the prior art the utility model, has the following advantages that and beneficial effect:By different height liquid in equilibrium still The liquid in face is stirred, while is sucked bottom and circulated, and is improved to highly viscous fluid mixing effect, is accelerated reaction speed.
Brief description of the drawings
Fig. 1 is the utility model structure diagram;
Fig. 2 is agitating shaft and the A-A views of stirring rod in Fig. 1.
Embodiment
With reference to Fig. 1 and Fig. 2, a kind of normal-pressure balance kettle, including kettle 1 and agitating shaft 2, agitating shaft 2 are driven by motor, can Rotated in one direction in kettle 1, the top of kettle 1 is provided with charging aperture 11 and condenser interface 12, the side wall of the kettle 1 Provided with inlet 13 and liquid outlet 14, the top of the kettle side wall is provided with the first sample tap 15, the bottom of the kettle side wall Provided with the second sample tap 16, the agitating shaft 2 is hollow structure, and stirring is fixedly connected with the outer circumference surface of the agitating shaft 2 Rod 3, the stirring rod 3 is vertical with the agitating shaft 2, and the stirring rod 3 is hollow structure and connected with the agitating shaft 2, institute State stirring rod 3 and be provided with some through holes 31, the opening direction of the through hole 31 is consistent with the direction of rotation of the agitating shaft 2, institute State the bottom in kettle 1 and be provided with pedestal 4, be provided with water pump 5 in the pedestal 4, one end of the water pump 5 connects with the agitating shaft 2 Upper surface logical, that the other end of the water pump 5 passes through pedestal described in pipeline communication 4.Top and bottom difference in the kettle 1 Provided with the first temperature sensor 61 and second temperature sensor 62, temperature sensor is connected to the pertinent instruments outside kettle 1, is used for Observe the temperature of diverse location in kettle 1.The kettle 1 is stainless steel, firm corrosion-resistant.The stirring rod 3 is 2 groups, It is separately positioned on the upper and lower part of the agitating shaft 2.
When agitating shaft 2 rotates in one direction, the opening of the through hole 31 in stirring rod 3 is consistent with direction of rotation, makes kettle Liquid in body 1 is easier to enter in stirring rod 3, passes sequentially through agitating shaft 2, water pump 5, pipeline and reaches the bottom of kettle 1, in formation Lower circulation loop, the liquid on the top of kettle 1 is entered the bottom of kettle 1, be sufficiently mixed it, reach balance, accelerate the reaction time.
Described above is only preferred embodiment of the present utility model, it is noted that for the common skill of the art For art personnel, on the premise of the utility model technical principle is not departed from, some improvement and modification can also be made, these change Enter and also should be regarded as the scope of protection of the utility model with modification.

Claims (4)

1. a kind of normal-pressure balance kettle, including kettle(1)And agitating shaft(2), the kettle(1)Top is provided with charging aperture(11)With it is cold Condenser interface(12), the kettle(1)Side wall be provided with inlet(13)And liquid outlet(14), the top of the kettle side wall is set There is the first sample tap(15), the bottom of the kettle side wall is provided with the second sample tap(16), it is characterised in that:The agitating shaft (2)For hollow structure, the agitating shaft(2)Outer circumference surface on be fixedly connected with stirring rod(3), the stirring rod(3)With institute State agitating shaft(2)Vertically, the stirring rod(3)For hollow structure and with the agitating shaft(2)Connection, the stirring rod(3)On Provided with some through holes(31), the through hole(31)Opening direction and the agitating shaft(2)Direction of rotation it is consistent, the kettle (1)Interior bottom is provided with pedestal(4), the pedestal(4)It is interior to be provided with water pump(5), the water pump(5)One end and the agitating shaft (2)Connection, the water pump(5)The other end pass through pedestal described in pipeline communication(4)Upper surface.
A kind of 2. normal-pressure balance kettle as claimed in claim 1, it is characterised in that:The kettle(1)Interior top and bottom point She You not the first temperature sensor(61)And second temperature sensor(62).
A kind of 3. normal-pressure balance kettle as claimed in claim 1, it is characterised in that:The kettle(1)For stainless steel.
A kind of 4. normal-pressure balance kettle as claimed in claim 1, it is characterised in that:The stirring rod(3)For 2 groups, set respectively In the agitating shaft(2)Upper and lower part.
CN201720504126.1U 2017-05-08 2017-05-08 A kind of normal-pressure balance kettle Expired - Fee Related CN206897394U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720504126.1U CN206897394U (en) 2017-05-08 2017-05-08 A kind of normal-pressure balance kettle

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720504126.1U CN206897394U (en) 2017-05-08 2017-05-08 A kind of normal-pressure balance kettle

Publications (1)

Publication Number Publication Date
CN206897394U true CN206897394U (en) 2018-01-19

Family

ID=61288565

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720504126.1U Expired - Fee Related CN206897394U (en) 2017-05-08 2017-05-08 A kind of normal-pressure balance kettle

Country Status (1)

Country Link
CN (1) CN206897394U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113123767A (en) * 2019-12-27 2021-07-16 中国石油天然气股份有限公司 Oil-gas periodic huff-puff simulation system and method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113123767A (en) * 2019-12-27 2021-07-16 中国石油天然气股份有限公司 Oil-gas periodic huff-puff simulation system and method

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CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20180119

Termination date: 20200508