CN206837539U - A kind of matricariaester production fractionating device - Google Patents
A kind of matricariaester production fractionating device Download PDFInfo
- Publication number
- CN206837539U CN206837539U CN201720525295.3U CN201720525295U CN206837539U CN 206837539 U CN206837539 U CN 206837539U CN 201720525295 U CN201720525295 U CN 201720525295U CN 206837539 U CN206837539 U CN 206837539U
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- China
- Prior art keywords
- fractionating
- tank
- heat supply
- fixed
- rotating shaft
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of matricariaester production fractionating device, including heat supply tank, transmission device, charging aperture, fractionating tank, visor and pressure gauge, ear mount is installed at left and right sides of the top of the fractionating tank, and it is provided with steam (vapor) outlet above the left side of fractionating tank, the bottom of the heat supply tank is provided with support frame, and it is provided with jet chimney above heat supply tank, rotating shaft is provided with below the transmission device, and rotating shaft is fixed on the inside of fractionating tank, the bottom both sides of the rotating shaft, which are provided with, smashes rod, feed pipe is installed below the charging aperture, and feed pipe is fixed on the inside of fractionating tank by fixed cover, the fixed cover is fixed on the inwall of fractionating tank, and the outer wall of fractionating tank is provided with heat-insulation layer, the surface of the fractionating tank is provided with visor and pressure gauge, and pressure gauge is installed on the right side of visor.The matricariaester production fractionating device, overall structure is simple, and high insulating effect, service life length, meets the demand of matricariaester production.
Description
Technical field
Matricariaester production equipment technology is the utility model is related to, specially a kind of matricariaester production fractionating device.
Background technology
Matricariaester is a kind of very extensive daily chemical essence of purposes, can be as the perfume additive of articles for washing;May be used also
As manufacture a kind of industrial chemicals of medicine etc., there are good market prospects, in the prior art mainly by 2 methyl pentanal
Oxidation reaction occurs with oxygen, generates 2 methyl valeric acid, 2 methyl valeric acid occurs esterification with ethanol and obtains matricariaester(2- first
Base ethyl valerate)Crude product, matricariaester finished product is obtained by purification(>99.95%), in the production process of conventional matricariaester very
Easily there is side reaction, product content is relatively low, and the difficult and raw material availability for causing fractionation to purify is low, and of the prior art point
Distillation unit fractionating effect difference and practicality be not strong, while heat insulation effect is bad, and feed pipe service life is short, therefore we have proposed
A kind of matricariaester production fractionating device, it is above-mentioned middle in order to solve the problems, such as.
Utility model content
The purpose of this utility model is to provide a kind of matricariaester production fractionating device, to solve in above-mentioned background technology
The problem of fractionating effect difference and practicality of proposition be not strong, while heat insulation effect is bad, and feed pipe service life is short.
To achieve the above object, the utility model provides following technical scheme:A kind of matricariaester production fractionating device, bag
Heat supply tank, transmission device, charging aperture, fractionating tank, visor and pressure gauge are included, ear is installed at left and right sides of the top of the fractionating tank
Frame, and steam (vapor) outlet is provided with above the left side of fractionating tank, the bottom of the heat supply tank is provided with support frame, and heat supply tank is upper
Side is provided with jet chimney, fixing device is provided with the right side of the heat supply tank, and heat supply tank passes through fixing device and fractionating tank
It is connected, rotating shaft is provided with below the transmission device, and rotating shaft is fixed on the inside of fractionating tank, the bottom two of the rotating shaft
Side, which is provided with, smashes rod, feed pipe is provided with below the charging aperture, and feed pipe is fixed on fractionating tank by fixed cover
Inside, the fixed cover are fixed on the inwall of fractionating tank, and the outer wall of fractionating tank is provided with heat-insulation layer, the table of the fractionating tank
Face is provided with visor and pressure gauge, and pressure gauge is provided with the right side of visor.
Preferably, the ear mount is provided with two, and it is symmetrical on the axis of fractionating tank.
Preferably, the jet chimney is connected with heat supply tank and fractionating tank.
Preferably, the heat supply tank includes water tank and heater, and heater is fixed with below water tank.
Preferably, the fixed cover and fractionating tank are integral type structure.
Preferably, the material of the heat-insulation layer is lime white.
Preferably, the rod of smashing is provided with everywhere, and it is evenly distributed in the bottom surrounding of rotating shaft.
Compared with prior art, the beneficial effects of the utility model are:The matricariaester production fractionating device, overall structure
Simply, and high insulating effect, service life are grown, and meet the demand of matricariaester production, provided with ear mount, can fix whole device
Suspension somewhere uses, and greatly improves the practicality of whole device, provided with heat supply tank, can be easy to enter the inside of fractionating tank
Row constantly heating, in order to more easily carry out fractionation work, feed pipe is fixed on the inside of fractionating device, avoided
Outside due to it is incorrect operation influence its service life situation, the setting of visor, be easy to observation inside fractionation situation,
In order to which people make correct operation, increase the efficiency of fractionation.
Brief description of the drawings
Fig. 1 is the utility model structure diagram.
Fig. 2 is the utility model fractionating tank surface structure schematic diagram.
Fig. 3 is the utility model heat supply jar structure schematic diagram.
In figure:1st, steam (vapor) outlet, 2, ear mount, 3, jet chimney, 4, fixing device, 5, heat supply tank, 501, water tank, 502 plus
Thermal, 6, support frame, 7, transmission device, 8, charging aperture, 9, rotating shaft, 10, fixed cover, 11, feed pipe, 12, heat-insulation layer, 13,
Smash rod, 14, fractionating tank, 15, visor, 16, pressure gauge.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belong to the scope of the utility model protection.
Fig. 1-3 are referred to, the utility model provides a kind of technical scheme:A kind of matricariaester production fractionating device, including
Steam (vapor) outlet 1, ear mount 2, jet chimney 3, fixing device 4, heat supply tank 5, water tank 501, heater 502, support frame 6, transmission
Device 7, charging aperture 8, rotating shaft 9, fixed cover 10, feed pipe 11, heat-insulation layer 12, smash rod 13, fractionating tank 14, visor 15 and pressure
Table 16, the top left and right sides of fractionating tank 14 is provided with ear mount 2, and is provided with steam (vapor) outlet 1, ear above the left side of fractionating tank 14
Frame 2 is provided with two, and it is symmetrical on the axis of fractionating tank 14 so that the outward appearance of whole device is more attractive in appearance, heat supply tank 5
Bottom is provided with support frame 6, and the top of heat supply tank 5 is provided with jet chimney 3, jet chimney 3 and heat supply tank 5 and fractionating tank 14
It is connected, the right side of heat supply tank 5 is provided with fixing device 4, and heat supply tank 5 is connected by fixing device 4 with fractionating tank 14,
Heat supply tank 5 includes water tank 501 and heater 502, and the lower section of water tank 501 is fixed with heater 502, transmission device 7
Lower section be provided with rotating shaft 9, and rotating shaft 9 is fixed on the inside of fractionating tank 14, and the bottom both sides of rotating shaft 9, which are provided with, smashes rod 13,
Rod 13 is smashed to be provided with everywhere, and it is evenly distributed in the bottom surrounding of rotating shaft 9, the lower section of charging aperture 8 is provided with feed pipe 11,
And feed pipe 11 is fixed on the inside of fractionating tank 14 by fixed cover 10, fixed cover 10 and fractionating tank 14 are integral type structure, drop
Low manufacturing cost, fixed cover 10 are fixed on the inwall of fractionating tank 14, and the outer wall of fractionating tank 14 is provided with heat-insulation layer 12, are protected
The material of warm layer 12 is lime white so that heat insulation effect more preferably, and also has the function that certain sterilization and desinsection, fractionating tank 14
Surface be provided with visor 15 and pressure gauge 16, and the right side of visor 15 is provided with pressure gauge 16.
Operation principle:When using the matricariaester production fractionating device, first to the matricariaester production fractionating device
Structure carries out a simple understanding, in use, raw material is put into fractionating tank 14 at charging aperture 8 by feed pipe 11,
Start transmission device 7 so that the drive of rotating shaft 9 is smashed rod 13 and worked, and raw material is decomposed, in order to more easily be divided
Work is evaporated, now recycles heater 502 to heat the water inside water tank 501, the vapor in heating process passes through
Jet chimney 3 is flowed into fractionating tank 14, in order to providing corresponding temperature in fractional distillation process, the setting of visor, be easy to see
The fractionation situation of inside is examined, in order to which people make correct operation, the material of heat-insulation layer 12 is lime white so that heat insulation effect
More preferably, and also there is certain sterilization and desinsection, feed pipe 11 is fixed on the inside of fractionating tank 14, avoided in outside
Use, because incorrect operation influences the situation of its service life, used here it is the matricariaester production with fractionating device
Whole process.
While there has been shown and described that embodiment of the present utility model, for the ordinary skill in the art,
It is appreciated that these embodiments can be carried out with a variety of changes in the case where not departing from principle of the present utility model and spirit, repaiied
Change, replace and modification, the scope of the utility model are defined by the appended claims and the equivalents thereof.
Claims (7)
1. a kind of matricariaester production fractionating device, including heat supply tank(5), transmission device(7), charging aperture(8), fractionating tank
(14), visor(15)And pressure gauge(16), it is characterised in that:The fractionating tank(14)Top at left and right sides of ear mount is installed
(2), and fractionating tank(14)Left side above be provided with steam (vapor) outlet(1), the heat supply tank(5)Bottom support frame is installed
(6), and heat supply tank(5)Top be provided with jet chimney(3), the heat supply tank(5)Right side be provided with fixing device(4),
And heat supply tank(5)Pass through fixing device(4)With fractionating tank(14)It is connected, the transmission device(7)Lower section be provided with rotating shaft
(9), and rotating shaft(9)It is fixed on fractionating tank(14)Inside, the rotating shaft(9)Bottom both sides be provided with and smash rod(13), institute
State charging aperture(8)Lower section feed pipe is installed(11), and feed pipe(11)Pass through fixed cover(10)It is fixed on fractionating tank(14)
Inside, the fixed cover(10)It is fixed on fractionating tank(14)Inwall on, and fractionating tank(14)Outer wall be provided with heat-insulation layer
(12), the fractionating tank(14)Surface be provided with visor(15)And pressure gauge(16), and visor(15)Right side pressure is installed
Power table(16).
A kind of 2. matricariaester production fractionating device according to claim 1, it is characterised in that:The ear mount(2)It is provided with
At two, and it is on fractionating tank(14)Axis it is symmetrical.
A kind of 3. matricariaester production fractionating device according to claim 1, it is characterised in that:The jet chimney(3)
With heat supply tank(5)And fractionating tank(14)It is connected.
A kind of 4. matricariaester production fractionating device according to claim 1, it is characterised in that:The heat supply tank(5)Bag
Include water tank(501)And heater(502), and water tank(501)Lower section be fixed with heater(502).
A kind of 5. matricariaester production fractionating device according to claim 1, it is characterised in that:The fixed cover(10)With
Fractionating tank(14)For integral type structure.
A kind of 6. matricariaester production fractionating device according to claim 1, it is characterised in that:The heat-insulation layer(12)'s
Material is lime white.
A kind of 7. matricariaester production fractionating device according to claim 1, it is characterised in that:It is described to smash rod(13)If
Have everywhere, and it is evenly distributed in rotating shaft(9)Bottom surrounding.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201720525295.3U CN206837539U (en) | 2017-05-12 | 2017-05-12 | A kind of matricariaester production fractionating device |
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CN201720525295.3U CN206837539U (en) | 2017-05-12 | 2017-05-12 | A kind of matricariaester production fractionating device |
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CN206837539U true CN206837539U (en) | 2018-01-05 |
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CN201720525295.3U Expired - Fee Related CN206837539U (en) | 2017-05-12 | 2017-05-12 | A kind of matricariaester production fractionating device |
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112473165A (en) * | 2020-11-06 | 2021-03-12 | 常德天盛电化有限公司 | Efficient fractionating tower system |
-
2017
- 2017-05-12 CN CN201720525295.3U patent/CN206837539U/en not_active Expired - Fee Related
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN112473165A (en) * | 2020-11-06 | 2021-03-12 | 常德天盛电化有限公司 | Efficient fractionating tower system |
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GR01 | Patent grant | ||
GR01 | Patent grant | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20180105 Termination date: 20190512 |