CN206799555U - A kind of Novel anti-blockage desulfurizer - Google Patents
A kind of Novel anti-blockage desulfurizer Download PDFInfo
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- CN206799555U CN206799555U CN201720370357.8U CN201720370357U CN206799555U CN 206799555 U CN206799555 U CN 206799555U CN 201720370357 U CN201720370357 U CN 201720370357U CN 206799555 U CN206799555 U CN 206799555U
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- Prior art keywords
- gate valve
- leakage fluid
- fluid dram
- inlet
- sulphur
- Prior art date
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- 239000007788 liquid Substances 0.000 claims abstract description 86
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims abstract description 77
- 239000005864 Sulphur Substances 0.000 claims abstract description 72
- 238000010521 absorption reaction Methods 0.000 claims abstract description 51
- 239000006260 foam Substances 0.000 claims abstract description 33
- 239000012530 fluid Substances 0.000 claims description 113
- 238000005086 pumping Methods 0.000 claims description 21
- 238000001802 infusion Methods 0.000 claims description 9
- 239000007787 solid Substances 0.000 claims description 9
- 238000009423 ventilation Methods 0.000 claims description 9
- 238000007599 discharging Methods 0.000 claims description 7
- 238000000926 separation method Methods 0.000 claims description 4
- 239000003795 chemical substances by application Substances 0.000 abstract description 22
- 230000003009 desulfurizing effect Effects 0.000 abstract description 21
- 238000006477 desulfuration reaction Methods 0.000 abstract description 7
- 238000001556 precipitation Methods 0.000 abstract description 7
- 230000023556 desulfurization Effects 0.000 abstract description 4
- 230000001376 precipitating effect Effects 0.000 abstract description 2
- 239000000126 substance Substances 0.000 abstract description 2
- 239000007789 gas Substances 0.000 description 27
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 16
- RWSOTUBLDIXVET-UHFFFAOYSA-N Dihydrogen sulfide Chemical compound S RWSOTUBLDIXVET-UHFFFAOYSA-N 0.000 description 13
- 229910000037 hydrogen sulfide Inorganic materials 0.000 description 11
- 239000003345 natural gas Substances 0.000 description 8
- 229910052717 sulfur Inorganic materials 0.000 description 7
- 239000011593 sulfur Substances 0.000 description 7
- 238000000034 method Methods 0.000 description 4
- 230000008569 process Effects 0.000 description 4
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 description 3
- 238000005516 engineering process Methods 0.000 description 3
- 238000011069 regeneration method Methods 0.000 description 3
- 230000009286 beneficial effect Effects 0.000 description 2
- 230000008859 change Effects 0.000 description 2
- 230000007423 decrease Effects 0.000 description 2
- 230000007812 deficiency Effects 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 238000007254 oxidation reaction Methods 0.000 description 2
- 230000008929 regeneration Effects 0.000 description 2
- 239000002912 waste gas Substances 0.000 description 2
- 239000002699 waste material Substances 0.000 description 2
- 206010017740 Gas poisoning Diseases 0.000 description 1
- LSDPWZHWYPCBBB-UHFFFAOYSA-N Methanethiol Chemical compound SC LSDPWZHWYPCBBB-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 239000003054 catalyst Substances 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000012535 impurity Substances 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 230000003993 interaction Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 238000010079 rubber tapping Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- 150000003568 thioethers Chemical class 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
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- Treating Waste Gases (AREA)
Abstract
The utility model belongs to chemical industry technical field of desulfurization, specifically, it is related to a kind of Novel anti-blockage desulfurizer, including admission line, absorption tower, surge tank, regenerator, sulphur foam tank, solid-liquid separator, return sulphur pipeline, reservoir, knockout drum and outlet line, admission line, absorption tower, surge tank, regenerator, sulphur foam tank, solid-liquid separator is sequentially connected, absorption tower is connected with knockout drum, knockout drum is provided with outlet line, surge tank, regenerator is connected with sulphur foam tank by returning sulphur pipeline with solid-liquid separator, reservoir is respectively and knockout drum, solid-liquid separator and surge tank are connected.The sulphur acquisition rate of the Novel anti-blockage desulfurizer is high, the secondary precipitation of desulfurizing agent lean solution in surge tank, on the one hand the desulfuration efficiency of the desulfurizer is improved, the sulphur that on the other hand also can effectively prevent from not precipitating completely in desulfurizing agent lean solution enters in absorption tower, blocks absorption tower pipeline.
Description
Technical field
A kind of Novel anti-blockage desulfurizer is the utility model is related to, belongs to chemical industry technical field of desulfurization.
Background technology
The natural gas of reservoir extraction contains some sour gas generally in addition to containing vapor, toward contact, these sour gas
Body is usually the gaseous impurities such as hydrogen sulfide, mercaptan, thioether, and wherein hydrogen sulfide is the maximum acidic components of natural gas Poisoning.My god
Hydrogen sulfide content becomes with geographical diversity in right gas, and China Main Natural Gas field belongs to high sulfur-containing natural gas (GB17820-
2012《Natural gas》Mandatory national standards provide, in second category of commodities natural gas H2S contents it is necessary≤20mg/m3.Class I goods
In natural gas H2S contents it is necessary≤6mg/m3), hydrogen sulfide not only has very strong toxicity, while also has very strong corrosivity,
Gas transmission line is easily done great damage, therefore desulfurization process must all be carried out to the sulfur-containing gas of reservoir extraction.
In common sulfur removal technology, without buffer unit between absorption tower and regenerator, cause the thin pipe of desulfurizer
Often there is Severe blockage situation.
Utility model content
The utility model provides a kind of Novel anti-blockage desulfurizer, it is intended that solving to exist in the prior art
Above mentioned problem.
The technical solution of the utility model is as follows:
The utility model provides a kind of Novel anti-blockage desulfurizer, including admission line, absorption tower, surge tank, again
Raw tower, sulphur foam tank, solid-liquid separator, return sulphur pipeline, reservoir, knockout drum and outlet line, admission line, absorption tower,
Surge tank, regenerator, sulphur foam tank, solid-liquid separator are sequentially connected, and absorption tower is connected with knockout drum, is set on knockout drum
There is an outlet line, surge tank, regenerator and sulphur foam tank are connected by returning sulphur pipeline with solid-liquid separator, and reservoir is respectively and gas-liquid
Knockout drum, solid-liquid separator and surge tank are connected.
In embodiment provided by the utility model, above-mentioned absorption tower is provided with the first air inlet, the first gas outlet, first
Inlet and the first leakage fluid dram;First air inlet is connected with admission line, and admission line is in one end away from absorption tower along air inlet
Direction is sequentially provided with the first gate valve and first pressure table, and first pressure table is provided with first throttle valve;First gas outlet is gentle
Liquid knockout drum is connected, and the second gate valve is provided with the first gas outlet;First inlet is connected with surge tank;First leakage fluid dram and regeneration
Tower is connected, and the 3rd gate valve is provided with the first leakage fluid dram, pumping equipment is provided between the 3rd gate valve and the first leakage fluid dram.
In embodiment provided by the utility model, above-mentioned knockout drum is provided with the second gas outlet, the second air inlet
With the second leakage fluid dram;Second gas outlet is connected with outlet line, and the 4th gate valve is provided with the second gas outlet, and outlet line is provided with
Second pressure gauge, and second pressure gauge is provided with second throttle;Second air inlet is connected with absorption tower;Second leakage fluid dram and storage
Liquid bath is connected, and the 5th gate valve is provided with the second leakage fluid dram.
In embodiment provided by the utility model, above-mentioned surge tank is provided with the 3rd leakage fluid dram, the 4th leakage fluid dram, second
Inlet and the 3rd inlet;3rd leakage fluid dram is connected with absorption tower, and the 6th gate valve, and the 6th gate valve are provided with the 3rd leakage fluid dram
Between absorption tower circulating pump, the 3rd pressure gauge, the first stop valve and the 7th gate valve, and are sequentially provided with along liquid flow direction
Three pressure gauges are provided with the 3rd choke valve;4th leakage fluid dram is connected with sulphur pipeline is returned, and the 8th gate valve is provided with the 4th leakage fluid dram, and
Pumping equipment is provided between 8th gate valve and the 4th leakage fluid dram;Second inlet is connected with regenerator;3rd inlet and liquid storage
Groove is connected, and the 9th gate valve, lean pump, the 4th pressure are sequentially provided with along liquid flow direction between the 3rd inlet and reservoir
Table, the second stop valve and the tenth gate valve, and the 4th pressure gauge is provided with the 4th choke valve.
In embodiment provided by the utility model, above-mentioned regenerator is provided with the 4th inlet, the 5th leakage fluid dram, the 6th
Leakage fluid dram, the 7th leakage fluid dram, the 3rd air inlet and the 3rd gas outlet;4th inlet is connected with absorption tower, at the 4th inlet
Provided with the 11st gate valve;5th leakage fluid dram is connected with surge tank, and the 12nd gate valve is provided with the 5th leakage fluid dram;6th leakage fluid dram and
Return sulphur pipeline to be connected, the 13rd gate valve is provided with the 6th leakage fluid dram, and discharge opeing is provided between the 13rd gate valve and the 6th leakage fluid dram
Device;7th leakage fluid dram is connected with sulphur foam tank;3rd air inlet is provided with ventilation line, and ventilation line free end is along airintake direction
Air blower, the 5th pressure gauge, the 3rd stop valve and the 14th gate valve are sequentially provided with, and the 5th pressure gauge is provided with the 5th throttling
Valve;3rd gas outlet and atmosphere.
In embodiment provided by the utility model, above-mentioned sulphur foam tank is provided with the 5th inlet and the 8th leakage fluid dram;The
Five inlets are connected with regenerator, and the 15th gate valve is provided with the 5th inlet;8th leakage fluid dram is connected with sulphur pipeline is returned, and the 8th
The 16th gate valve is provided with leakage fluid dram, and pumping equipment is provided between the 16th gate valve and the 8th leakage fluid dram.
In embodiment provided by the utility model, above-mentioned solid-liquid separator be provided with the 6th inlet, solid outlet and
9th leakage fluid dram;6th inlet is connected with sulphur pipeline is returned, and returns sulphur pipeline between the 16th gate valve and solid-liquid separator along liquid
Body flow direction is sequentially provided with the 17th gate valve, sulphur foam pump, the 6th pressure gauge, the 4th stop valve and the 18th gate valve, and the 6th
Pressure gauge is provided with the 6th choke valve;Solid outlet exports for sulphur;9th leakage fluid dram is connected with reservoir, at the 9th leakage fluid dram
Provided with the 19th gate valve.
In embodiment provided by the utility model, above-mentioned reservoir is provided with the 7th inlet, the 8th inlet, the 9th
Inlet and the tenth leakage fluid dram;7th inlet is connected with knockout drum;8th inlet is connected with solid-liquid separator;9th
Inlet is provided with fluid infusion pipeline, and fluid infusion pipeline is provided with the 20th gate valve;Tenth leakage fluid dram is connected with surge tank, the tenth discharge opeing
Pumping equipment is provided with mouthful.
In embodiment provided by the utility model, above-mentioned knockout drum, absorption tower, surge tank, regenerator and sulphur foam
Liquid level emasuring device is additionally provided with tank, liquid level emasuring device includes the 21st gate valve, the 22nd gate valve, the 23rd gate valve
And liquid level gauge, the 21st gate valve and the 22nd gate valve are connected into the 23rd gate valve after being connected in parallel, liquid level gauge is located at second
Between 11 gate valves and the 22nd gate valve.
In embodiment provided by the utility model, above-mentioned pumping equipment includes discharging tube and the 24th gate valve, discharge opeing
Pipe is provided with the 24th gate valve
Above-mentioned liquid level emasuring device is used to measure the liquid level in coupled device, when liquid level deficiency, passes through above-mentioned storage
Liquid level after decline is supplemented to normal level height by liquid bath or fluid infusion pipeline in time.
In embodiment provided by the utility model, above-mentioned pumping equipment includes discharging tube and the 25th gate valve, discharge opeing
Pipe is provided with the 25th gate valve.
Above-mentioned tapping line device is used for the raffinate for clearing up coupled device or as the outlet of debugging liquid.
The beneficial effects of the utility model are:The sulphur acquisition rate of the Novel anti-blockage desulfurizer is high, passes through surge tank
Desulfurizing agent lean solution in regenerator can not only be subjected to secondary precipitation, moreover it is possible to by the desulfurizing agent in surge tank after secondary precipitation
Lean solution is transmitted back in absorption tower again, so as to complete desulfurizing agent from the recycle stream on absorption tower-regenerator-surge tank-absorption tower
It is dynamic, reduce the generation of waste liquid in sweetening process, waste gas;In addition, in surge tank desulfurizing agent lean solution secondary precipitation, on the one hand carry
The high desulfuration efficiency of the desulfurizer, the sulphur that on the other hand also can effectively prevent from not precipitating completely in desulfurizing agent lean solution enter
In absorption tower, absorption tower pipeline is blocked.
Brief description of the drawings
, below will be to required in embodiment in order to illustrate more clearly of the technical scheme of the utility model embodiment
The accompanying drawing used is briefly described, it will be appreciated that and the following drawings illustrate only some embodiments of the present utility model, therefore not
The restriction to scope is should be considered as, for those of ordinary skill in the art, on the premise of not paying creative work,
Other related accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 Novel anti-blockage desulfurizer structure charts provided by the utility model;
Fig. 2 liquid level emasuring device structure charts provided by the utility model;
Fig. 3 pumping equipment structure charts provided by the utility model.
Shown in figure:100- Novel anti-blockage desulfurizers;1- admission lines;The gate valves of 10- first;11- first pressure tables;
110- first throttle valves;2- knockout drums;The gas outlets of 20- second;The gate valves of 200- the 4th;The air inlets of 21- second;22- second
Leakage fluid dram;The gate valves of 220- the 5th;3- absorption towers;The air inlets of 30- first;The gas outlets of 31- first;The gate valves of 310- second;32- first
Inlet;The leakage fluid drams of 33- first;The gate valves of 330- the 3rd;34- circulating pumps;The pressure gauges of 35- the 3rd;The choke valves of 350- the 3rd;36-
First stop valve;The gate valves of 37- the 7th;4- surge tanks;The leakage fluid drams of 40- the 3rd;The gate valves of 400- the 6th;The leakage fluid drams of 41- the 4th;410-
8th gate valve;The inlets of 42- second;The inlets of 43- the 3rd;The gate valves of 44- the 9th;45- lean pumps;The pressure gauges of 46- the 4th;460-
4th choke valve;The stop valves of 47- second;The gate valves of 48- the tenth;5- regenerators;The inlets of 50- the 4th;The gate valves of 500- the 11st;
The leakage fluid drams of 51- the 5th;The gate valves of 510- the 12nd;The leakage fluid drams of 52- the 6th;The gate valves of 520- the 13rd;The leakage fluid drams of 53- the 7th;54-
Three air inlets;The gas outlets of 55- the 3rd;56- ventilation lines;The gate valves of 560- the 14th;57- air blowers;The pressure gauges of 58- the 5th;
The choke valves of 580- the 5th;The stop valves of 59- the 3rd;6- sulphur foam tanks;The inlets of 60- the 5th;The gate valves of 600- the 15th;The rows of 61- the 8th
Liquid mouth;The gate valves of 610- the 16th;7- solid-liquid separators;The inlets of 70- the 6th;71- solid outlets;The leakage fluid drams of 72- the 9th;720-
19th gate valve;8- returns sulphur pipeline;The gate valves of 80- the 17th;81- sulphur foam pumps;The pressure gauges of 82- the 6th;The choke valves of 820- the 6th;
The stop valves of 83- the 4th;The gate valves of 84- the 18th;9- reservoirs;The inlets of 90- the 7th;The inlets of 91- the 8th;The feed liquors of 92- the 9th
Mouthful;The leakage fluid drams of 93- the tenth;94- fluid infusion pipelines;The gate valves of 940- the 20th;12- pumping equipments;120- discharging tubes;121- the 20th
Four gate valves;13- liquid level emasuring devices;The gate valves of 130- the 21st;The gate valves of 131- the 22nd;The gate valves of 132- the 23rd;
133- liquid level gauges;14- outlet lines;15- second pressure gauges;150- second throttle.
Embodiment
The utility model is further illustrated with reference to the accompanying drawings and examples.
To make the purpose, technical scheme and advantage of the utility model embodiment clearer, below in conjunction with this practicality
Accompanying drawing in new embodiment, the technical scheme in the utility model embodiment is clearly and completely described, shown
So, described embodiment is a part of embodiment of the utility model, rather than whole embodiments.Therefore, below
It is new that the detailed description of embodiment of the present utility model to providing in the accompanying drawings is not intended to limit this claimed practicality
The scope of type, but it is merely representative of selected embodiment of the present utility model.Based on the embodiment in the utility model, ability
All other embodiment that domain those of ordinary skill is obtained under the premise of creative work is not made, belongs to this practicality
Novel protected scope.
In description of the present utility model, it is to be understood that the term of indicating position or position relationship is based on accompanying drawing
Shown orientation or position relationship, it is for only for ease of description the utility model and simplifies description, rather than indicates or imply institute
The equipment or element of finger must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that to this reality
With new limitation.
In the utility model, unless otherwise clearly defined and limited, term " installation ", " connected ", " connection ", " Gu
It is fixed " etc. term should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, or integrally;Can be
Mechanically connect or electrically connect;Can be joined directly together, can also be indirectly connected by intermediary, can be two
The connection of element internal or the interaction relationship of two elements.For the ordinary skill in the art, can basis
Concrete condition understands concrete meaning of the above-mentioned term in the utility model.
In the utility model, unless otherwise clearly defined and limited, fisrt feature is on or below second feature
Can directly it be contacted including the first and second features, it is not directly to contact but pass through it that can also include the first and second features
Between other characterisation contact.Moreover, fisrt feature is on second feature, top and above include fisrt feature the
Directly over two features and oblique upper, or be merely representative of fisrt feature level height and be higher than second feature.Fisrt feature is special second
Under sign, lower section and fisrt feature included below are immediately below second feature and obliquely downward, or are merely representative of fisrt feature level
Highly it is less than second feature.
Embodiment:
Such as Fig. 1, a kind of Novel anti-blockage desulfurizer 100, including admission line 1, gas-liquid separation are present embodiments provided
Tank 2, absorption tower 3, surge tank 4, regenerator 5, sulphur foam tank 6, solid-liquid separator 7, time sulphur pipeline 8, the outlet line 14 of reservoir 9,
Admission line 1, absorption tower 3, surge tank 4, regenerator 5, sulphur foam tank 6, solid-liquid separator 7 are sequentially connected, absorption tower 3 and gas-liquid point
It is connected from tank 2, knockout drum 2 is provided with outlet line 14, and surge tank 4, regenerator 5 and sulphur foam tank 6 are by returning the and of sulphur pipeline 8
Solid-liquid separator 7 is connected, and reservoir 9 is connected with knockout drum 2, solid-liquid separator 7 and surge tank 4 respectively.
Absorption tower 3 is provided with the first air inlet 30, the first gas outlet 31, the first inlet 32 and the first leakage fluid dram 33;The
One air inlet 30 is connected with admission line 1, and admission line 1 is sequentially provided with first in one end away from absorption tower 3 along airintake direction
Gate valve 10 and first pressure table 11, and first pressure table 11 is provided with first throttle valve 110;First gas outlet 31 and gas-liquid separation
Tank 2 is connected, and the second gate valve 310 is provided with the first gas outlet 31;First inlet 32 is connected with surge tank 4;First leakage fluid dram 33
It is connected with regenerator 5, the 3rd gate valve 330 is provided with the first leakage fluid dram 33, is provided between the 3rd gate valve 330 and the first leakage fluid dram 33
Pumping equipment 12.
Above-mentioned first pressure table 11 is used to measure the pressure in admission line 1, when first pressure table is changed or overhauled to needs
When 11, above-mentioned first throttle valve 110 is closed.
Knockout drum 2 is provided with the second gas outlet 20, the second air inlet 21 and the second leakage fluid dram 22;The He of second gas outlet 20
Outlet line 14 is connected, and the 4th gate valve 200 is provided with the second gas outlet 20, and outlet line 14 is provided with second pressure gauge 15, and
Second pressure gauge 15 is provided with second throttle 150;Second air inlet 21 is connected with absorption tower 3;Second leakage fluid dram 22 and liquid storage
Groove 9 is connected, and the 5th gate valve 220 is provided with the second leakage fluid dram 22.
Above-mentioned second pressure gauge 15 is used to measure the pressure in outlet line 14, when second pressure gauge is changed or overhauled to needs
When 115, above-mentioned first throttle valve 150 is closed.
Surge tank 4 is provided with the 3rd leakage fluid dram 40, the 4th leakage fluid dram 41, the second inlet 42 and the 3rd inlet 43;3rd
Leakage fluid dram 40 is connected with absorption tower 3, and the 6th gate valve 400 is provided with the 3rd leakage fluid dram 40;And the 6th gate valve 400 and absorption tower 3 it
Between along liquid flow direction be sequentially provided with circulating pump 34, the 3rd pressure gauge 35, the first stop valve 36 and the 7th gate valve 37, and the 3rd
Pressure gauge 35 is provided with the 3rd choke valve 350;4th leakage fluid dram 41 is connected with sulphur pipeline 8 is returned, provided with the at the 4th leakage fluid dram 41
Eight gate valves 410, and pumping equipment 12 is provided between the 8th gate valve 410 and the 4th leakage fluid dram 41;Second inlet 42 and regenerator 5
It is connected;3rd inlet 43 is connected with reservoir 9, is set successively along liquid flow direction between the 3rd inlet 43 and reservoir 9
There are the 9th gate valve 44, lean pump 45, the 4th pressure gauge 46, the second stop valve 47 and the tenth gate valve 48, and on the 4th pressure gauge 46
Provided with the 4th choke valve 460.
Above-mentioned 3rd pressure gauge 35 is used for the pressure for measuring the exit of circulating pump 34, when the 3rd pressure is changed or overhauled to needs
During table 35, above-mentioned 3rd choke valve 350 is closed.
Above-mentioned 4th pressure gauge 46 is used for the pressure for measuring the exit of lean pump 45, when the 4th pressure is changed or overhauled to needs
During table 46, above-mentioned 4th choke valve 460 is closed.
Regenerator 5 is provided with the 4th inlet 50, the 5th leakage fluid dram 51, the 6th leakage fluid dram 52, the 7th leakage fluid dram the 53, the 3rd and entered
The gas outlet 55 of gas port 54 and the 3rd;4th inlet 50 is connected with absorption tower 3, and the 11st gate valve is provided with the 4th inlet 50
500;5th leakage fluid dram 51 is connected with surge tank 4, and the 12nd gate valve 510 is provided with the 5th leakage fluid dram 51;The He of 6th leakage fluid dram 52
Return sulphur pipeline 8 to be connected, be provided with the 13rd gate valve 520 at the 6th leakage fluid dram 52, and the 13rd gate valve 520 and the 6th leakage fluid dram 52 it
Between be provided with pumping equipment 12;7th leakage fluid dram 53 is connected with sulphur foam tank 6;3rd air inlet 54 is provided with ventilation line 56, ventilation
The free end of pipeline 56 is sequentially provided with machine 57, the 5th pressure gauge 58, the 3rd stop valve 59 and the 14th gate valve windward along airintake direction
560, and the 5th pressure gauge 58 is provided with the 5th choke valve 580;3rd gas outlet 55 and atmosphere.
Above-mentioned 5th pressure gauge 58 is used to measure the pressure in ventilation line 56, when the 5th pressure gauge is changed or overhauled to needs
When 58, above-mentioned 5th choke valve 580 is closed.
Sulphur foam tank 6 is provided with the 5th inlet 60 and the 8th leakage fluid dram 61;5th inlet 60 is connected with regenerator 5, and the 5th
The 15th gate valve 600 is provided with inlet 60;8th leakage fluid dram 61 is connected with sulphur pipeline 8 is returned, provided with the at the 8th leakage fluid dram 61
16 gate valves 610, and pumping equipment 12 is provided between the 16th gate valve 610 and the 8th leakage fluid dram 61.
Solid-liquid separator 7 is provided with the 6th inlet 70, the leakage fluid dram 72 of solid outlet 71 and the 9th;6th inlet 70 and return
Sulphur pipeline 8 is connected, and returns sulphur pipeline 8 and is sequentially provided with the along liquid flow direction between the 16th gate valve 610 and solid-liquid separator 7
17 gate valves 80, sulphur foam pump 81, the 6th pressure gauge 82, the 4th stop valve 83 and the 18th gate valve 84, and on the 6th pressure gauge 82
Provided with the 6th choke valve 820;Solid outlet 71 exports for sulphur;9th leakage fluid dram 72 is connected with reservoir 9, the 9th leakage fluid dram 72
Place is provided with the 19th gate valve 720.
Above-mentioned 6th pressure gauge 82 is used for the pressure for measuring the exit of sulphur foam pump 81, when the 6th pressure is changed or overhauled to needs
During table 82, above-mentioned 6th choke valve 820 is closed.
Reservoir 9 is provided with the 7th inlet 90, the 8th inlet 91, the 9th inlet 92 and the tenth leakage fluid dram 93;7th
Inlet 90 is connected with knockout drum 2;8th inlet 91 is connected with solid-liquid separator 7;9th inlet 92, which is provided with, to be mended
Liquid pipe line 94, fluid infusion pipeline 94 are provided with the 20th gate valve 940;Tenth leakage fluid dram 93 is connected with surge tank 4, the tenth leakage fluid dram 93
Place is provided with pumping equipment 12.
Specifically, above-mentioned reservoir 9 is used to supplement desulfurizing agent to surge tank 4.
Such as Fig. 2, knockout drum 2, absorption tower 3, surge tank 4, regenerator 5 and sulphur foam tank 6 are additionally provided with liquid level emasuring device
13, liquid level emasuring device 13 includes the 21st gate valve 130, the 22nd gate valve 131, the 23rd gate valve 132 and liquid level gauge
133, the 21st gate valve 130 and the 22nd gate valve 131 are connected into the 23rd gate valve 132, liquid level gauge 133 after being connected in parallel
Between the 21st gate valve 130 and the 22nd gate valve 131.
Specifically, above-mentioned liquid level emasuring device 13 is used to measure the liquid level in coupled device, when liquid level deficiency, lead to
Cross above-mentioned reservoir 9 or fluid infusion pipeline 94 and the liquid level after decline is supplemented to normal level height in time.
Such as Fig. 3, pumping equipment 12 includes the gate valve 121 of discharging tube 120 and the 24th, and discharging tube 120 is provided with the 20th
Four gate valves 121.
Specifically, above-mentioned pumping equipment 12 is used for the raffinate for clearing up coupled device or ensures each dress when debugging initial stage
Put interior liquid level line and be in certain altitude.
The operation principle of Novel anti-blockage desulfurizer 100 provided by the utility model is:First, when sulfur-containing gas with
After admission line 1 enters absorption tower 3, hydrogen sulfide and other sulfide are absorbed by the desulfurizing agent in absorption tower 3, by sulfur-containing gas
In hydrogen sulfide remove, natural gas after purification is by knockout drum 2, after removing the moisture in purified gas, into follow-up work
Industry produces or storage;Meanwhile desulfurizing agent rich solution (desulfurizing agent containing a large amount of hydrogen sulfide and other sulfide) is from the bottom of absorption tower 3
It is transported to by circulating pump 35 in regenerator 5, desulfurizing agent rich solution enters from the top of regenerator 5, using air blower 57 by air
It is delivered to through ventilation line 56 in regenerator 5, the efficient composite catalyst in regenerator 5 of the oxygen in desulfurizing agent rich solution and air
In the presence of oxidation regeneration reaction occurs, the hydrogen sulfide in sulfur removing pregnant solution and other sulfide-oxidations is rich into sulphur, desulfurizing agent
Liquid becomes lean solution, and now the sulphur foam in regenerator 5, which flows automatically, enters sulphur foam tank 6, and the sulphur in sulphur foam sinks naturally in sulphur foam tank 6
Form sediment, the lean solution in regenerator 5 flows automatically to surge tank 4, sulphur natural sedimentation in surge tank 4 in lean solution, when in surge tank 4
Lean solution therein is pumped into absorption tower 3 by circulating pump 34 when lean solution reaches certain liquid level and continues to absorb in sulfur-containing gas
Hydrogen sulfide and other sulfide;Finally, the sulphur of regenerator 5, sulphur foam tank 6 and the bottom of surge tank 4 is deposited in, passes through sulphur foam pump
81, which pass through back sulphur pipeline 8, enters solid-liquid separator 7, and the lean solution isolated enters reservoir 9, and the sulphur solid particle isolated is through solid
Body outlet 71 is removed;In addition, the Novel anti-blockage desulfurizer 100 in sweetening process due to the band liquid and water of drusen
Evaporation, the desulfurizing agent in each retort can produce partition losses, and the desulfurizing agent of loss can be supplemented by reservoir 9, when
When liquid level in reservoir 9 is relatively low, then the desulfurizing agent of suitable dosage is supplemented to reservoir 9 in time by fluid infusion pipeline 94.
Novel anti-blockage desulfurizer provided by the utility model has the beneficial effect that:The Novel anti-blockage desulfurizer
Sulphur acquisition rate is high, the desulfurizing agent lean solution in regenerator can not only be carried out into secondary precipitation by surge tank, moreover it is possible to will buffer
Desulfurizing agent lean solution in tank after secondary precipitation is transmitted back in absorption tower again, so as to complete desulfurizing agent from absorption tower-regeneration
Circulating for tower-surge tank-absorption tower, reduces the generation of waste liquid in sweetening process, waste gas;In addition, desulfurization in surge tank
The secondary precipitation of agent lean solution, the desulfuration efficiency of the desulfurizer is on the one hand improved, on the other hand also can effectively prevent desulfurizing agent
The sulphur not precipitated completely in lean solution enters in absorption tower, blocks absorption tower pipeline.
It is described above, not make any formal limitation to the utility model, although the utility model passes through embodiment
It is disclosed above, but the utility model is not limited to, any person skilled in the art is new not departing from this practicality
In the range of type technical scheme, when the technology contents using the disclosure above make a little change or are modified to the equivalent of equivalent variations
Embodiment, as long as being the content without departing from technical solutions of the utility model, according to the technical essence of the utility model to real above
Any simple modification, equivalent change and modification that example is made is applied, in the range of still falling within technical solutions of the utility model.
Claims (10)
1. a kind of Novel anti-blockage desulfurizer, it is characterised in that including admission line, absorption tower, surge tank, regenerator, sulphur
Foam tank, solid-liquid separator, return sulphur pipeline, reservoir, knockout drum and outlet line, admission line, absorption tower, surge tank,
Regenerator, sulphur foam tank, solid-liquid separator are sequentially connected, and absorption tower is connected with knockout drum, and knockout drum is provided with outlet
Pipeline, surge tank, regenerator and sulphur foam tank are connected by returning sulphur pipeline with solid-liquid separator, and reservoir is respectively and gas-liquid separation
Tank, solid-liquid separator and surge tank are connected.
2. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the absorption tower is entered provided with first
Gas port, the first gas outlet, the first inlet and the first leakage fluid dram;
First air inlet is connected with admission line, and the admission line is sequentially provided with one end away from absorption tower along airintake direction
First gate valve and first pressure table, and first pressure table is provided with first throttle valve;
First gas outlet is connected with knockout drum, and the second gate valve is provided with the first gas outlet;
First inlet is connected with surge tank;
First leakage fluid dram is connected with regenerator, the 3rd gate valve is provided with the first leakage fluid dram, between the 3rd gate valve and the first leakage fluid dram
Provided with pumping equipment.
3. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the knockout drum is provided with the
Two gas outlets, the second air inlet and the second leakage fluid dram;
Second gas outlet is connected with outlet line, and the 4th gate valve is provided with the second gas outlet, and outlet line is provided with second pressure
Table, and second pressure gauge is provided with second throttle;
Second air inlet is connected with absorption tower;
Second leakage fluid dram is connected with reservoir, and the 5th gate valve is provided with the second leakage fluid dram.
4. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the surge tank is provided with the 3rd row
Liquid mouth, the 4th leakage fluid dram, the second inlet and the 3rd inlet;
3rd leakage fluid dram is connected with absorption tower, and the 6th gate valve, and edge between the 6th gate valve and absorption tower are provided with the 3rd leakage fluid dram
Liquid flow direction is sequentially provided with circulating pump, the 3rd pressure gauge, the first stop valve and the 7th gate valve, and the 3rd pressure gauge is provided with
3rd choke valve;
4th leakage fluid dram is connected with sulphur pipeline is returned, and the 8th gate valve, and the 8th gate valve and the 4th leakage fluid dram are provided with the 4th leakage fluid dram
Between be provided with pumping equipment;
Second inlet is connected with regenerator;
3rd inlet is connected with reservoir, and the 9th lock is sequentially provided with along liquid flow direction between the 3rd inlet and reservoir
Valve, lean pump, the 4th pressure gauge, the second stop valve and the tenth gate valve, and the 4th pressure gauge is provided with the 4th choke valve.
5. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the regenerator enters provided with the 4th
Liquid mouth, the 5th leakage fluid dram, the 6th leakage fluid dram, the 7th leakage fluid dram, the 3rd air inlet and the 3rd gas outlet;
4th inlet is connected with absorption tower, and the 11st gate valve is provided with the 4th inlet;
5th leakage fluid dram is connected with surge tank, and the 12nd gate valve is provided with the 5th leakage fluid dram;
6th leakage fluid dram is connected with sulphur pipeline is returned, and the 13rd gate valve, and the 13rd gate valve and the 6th row are provided with the 6th leakage fluid dram
Pumping equipment is provided between liquid mouth;7th leakage fluid dram is connected with sulphur foam tank;
3rd air inlet is provided with ventilation line, and the ventilation line free end is sequentially provided with air blower, the 5th along airintake direction
Pressure gauge, the 3rd stop valve and the 14th gate valve, and the 5th pressure gauge is provided with the 5th choke valve;
3rd gas outlet and atmosphere.
6. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the sulphur foam tank enters provided with the 5th
Liquid mouth and the 8th leakage fluid dram;
5th inlet is connected with regenerator, and the 15th gate valve is provided with the 5th inlet;
8th leakage fluid dram is connected with sulphur pipeline is returned, and the 16th gate valve, and the 16th gate valve and the 8th row are provided with the 8th leakage fluid dram
Pumping equipment is provided between liquid mouth.
7. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the solid-liquid separator is provided with the
Six inlets, solid outlet and the 9th leakage fluid dram;
6th inlet is connected with sulphur pipeline is returned, and returns sulphur pipeline between the 16th gate valve and solid-liquid separator along liquid flowing side
To being sequentially provided with the 17th gate valve, sulphur foam pump, the 6th pressure gauge, the 4th stop valve and the 18th gate valve, and on the 6th pressure gauge
Provided with the 6th choke valve;
Solid outlet exports for sulphur;
9th leakage fluid dram is connected with reservoir, and the 19th gate valve is provided with the 9th leakage fluid dram.
8. Novel anti-blockage desulfurizer according to claim 1, it is characterised in that the reservoir enters provided with the 7th
Liquid mouth, the 8th inlet, the 9th inlet and the tenth leakage fluid dram;
7th inlet is connected with knockout drum;
8th inlet is connected with solid-liquid separator;
9th inlet is provided with fluid infusion pipeline, and the fluid infusion pipeline is provided with the 20th gate valve;
Tenth leakage fluid dram is connected with surge tank, and pumping equipment is provided with the tenth leakage fluid dram.
9. the Novel anti-blockage desulfurizer according to any one of claim 1 to 8, it is characterised in that the gas-liquid separation
Liquid level emasuring device is additionally provided with tank, absorption tower, surge tank, regenerator and sulphur foam tank, the liquid level emasuring device includes second
11 gate valves, the 22nd gate valve, the 23rd gate valve and liquid level gauge, the 21st gate valve and the 22nd gate valve are connected in parallel
After be connected into the 23rd gate valve, liquid level gauge is between the 21st gate valve and the 22nd gate valve.
10. according to the Novel anti-blockage desulfurizer described in claim 2,4,5,6 or 8, it is characterised in that the pumping equipment
Including discharging tube and the 24th gate valve, the discharging tube is provided with the 24th gate valve.
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CN201720370357.8U CN206799555U (en) | 2017-04-11 | 2017-04-11 | A kind of Novel anti-blockage desulfurizer |
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CN201720370357.8U CN206799555U (en) | 2017-04-11 | 2017-04-11 | A kind of Novel anti-blockage desulfurizer |
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