CN206783315U - A kind of spray burning device - Google Patents

A kind of spray burning device Download PDF

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Publication number
CN206783315U
CN206783315U CN201720501250.2U CN201720501250U CN206783315U CN 206783315 U CN206783315 U CN 206783315U CN 201720501250 U CN201720501250 U CN 201720501250U CN 206783315 U CN206783315 U CN 206783315U
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air guide
atomizer
cavity
utility
model
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CN201720501250.2U
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黄云
王述浩
蓝志鹏
王娜峰
杨庆利
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Institute of Process Engineering of CAS
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Institute of Process Engineering of CAS
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Abstract

A kind of spray burning device is the utility model is related to, described device includes gun body, air guide and atomizer;The gun body includes a cavity;The air guide is arranged in the cavity, can be slided along the cavity is relative;The atomizer is arranged in the air guide, can be slided with air guide along the cavity;The air guide is connected with the air inlet of imflammable gas, and the atomizer is connected with the inlet of liquid precursor.Above-mentioned spray burning device can realize spraying and optimal matching of burning;The problems such as effectively avoiding drop during spray burning, particle adhesion wall to block cavity simultaneously;It is simple and quick, shorten technological process and preparation time;The nano-oxide product pattern of preparation, size are controllable, and quality is good and added value is high.

Description

A kind of spray burning device
Technical field
It the utility model is related to nano material synthesis field, and in particular to a kind of spray burning device.
Background technology
Metal oxide, especially transition metal oxide show prominent property in optics, electromagnetism, catalysis etc. Can, thus occupied an important position in related application.As nano material preparation technology develops, various new patterns, new construction Nano-oxide be synthesized, be assembled into device, show good application performance.Flame synthesis is that a step quickly prepares nanometer The typical method of material, due to its equipment is simple, easily amplify the features such as, turn into the nano material manufacture work for having much industrial prospect Skill.
Flame synthesis nanometer oxide material generally requires specific device spraying and prepared, such as CN203373422U Disclose " a kind of spray burning device ", CN103305810A discloses a kind of spray burning and prepares setting for film and spray patterns It is standby, a kind of patent CN102614862A " flame plasma synthetic method and its plasma torch burnings of doped yttrium cerium zirconium sosoloid Device ", but above-mentioned synthesizer is generally only applicable to the liquid precursor containing organic component;It is difficult and modular construction is fixed Structural parameters during with to spraying are effectively adjusted;Drop and particle, which easily adhere to wall, in spray process blocks cavity.
The content of the invention
In view of problems of the prior art, the utility model provides a kind of spray burning device, can realize pair Effective regulation of spray burning device parameter, form optimal spray burning system;Simultaneously effectively avoid drop in spray process, The problems such as particle adhesion wall blocks cavity;Operate simpler quick, shorten technological process and preparation time;Make preparation Nano-oxide product pattern, size it is controllable.
To use following technical scheme up to this purpose, the utility model:
The utility model provides a kind of spray burning device, and described device includes gun body, air guide and atomizer;Institute Stating gun body includes a cavity;The air guide is arranged in the cavity, can be slided along the cavity is relative;The atomization Nozzle is arranged in the air guide, can be slided with air guide along the cavity;The air guide and imflammable gas Air inlet is connected, and the atomizer is connected with the inlet of liquid precursor.
In the utility model, the air guide is connected with the air inlet of imflammable gas, and the imflammable gas is by can Combustion property gas supply device provides, and is burnt by air guide in the port of gun body.Air guide can control imflammable gas Flow, realize effective regulation to flame temperature with reference to the adjustment to gas component.
In the utility model, the atomizer is connected with the inlet of liquid precursor, and the liquid precursor is by liquid State predecessor feedway is provided, and warm area is sprayed to by atomizer.
The utility model sets air guide and atomizer simultaneously in spray burning device, can utilize flammable gas Body produces stable warm area, while liquid precursor can be directly atomized into micron-sized drop, it is not necessary to extra atomization Device, save space and cost;Apparatus structure is simple, compact in design, makes operation simpler quick, shortens technological process And preparation time.
The utility model is arranged in air guide and sets atomizer, and atomizer and air guide are as entirety Structure, can along gun body cavity it is relative slide, distance (H) of the air guide close to the end face of liquid outlet and gun body port during spraying It is adjustable with the ratio of the diameter of section (D) of air guide, while the spray angle (θ) of atomizer is also adjustable, by above-mentioned The control of parameter, burning can be made smoothly to carry out, at the same the micron order drop uniform, controllable for making to be formed after atomization be sprayed onto fire On flame face, spraying and optimal matching of burning are realized, optimal spray burning system is formed, so as to obtain more high quality production Product.
Further, since air guide is arranged in atomizer and gun body annular space, imflammable gas air-flow in spray process Twice dispersing is carried out to atomized drop, with reference to the above-mentioned regulation to parameter, can effectively be avoided droplets from, particle adhesion wall blocks Cavity.
The utility model is to the shape of the cavity of the gun body and without particular determination, it is preferable that the gun body includes One tubular cavity.
According to the utility model, the air guide is any one in distribution grid, guiding gutter or honeycomb ceramics.
According to the utility model, the atomizer is pressure atomized fog jet or double fluid atomization nozzle.When using double-current , it is necessary to be passed through gas dispersion into atomizer accordingly during body atomizer.The gas dispersion is air, oxygen or nitrogen In any one or at least two combination, preferably air.
The utility model, can basis to the relative position of the atomizer and air guide and without particular determination Actual conditions are adjusted, it is preferable that the atomizer is arranged in the center position of the air guide.
According to the utility model, the air guide is bonded with the inwall of the gun body, and can be relatively sliding along the cavity It is dynamic.
According to the utility model, the imflammable gas is in methane, ethane, propane, acetylene, carbon monoxide or hydrogen Any one or at least two combination, such as can be any in methane, ethane, propane, acetylene, carbon monoxide or hydrogen It is a kind of;Typical but non-limiting is combined as:Methane and ethane;Propane and acetylene;Carbon monoxide and hydrogen;Methane, ethane and Propane;Ethane, propane and acetylene etc., as space is limited and for concise consideration, the utility model no longer exclusive list.It is described can Combustion property gas is preferably methane.
The utility model can selectivity nitrogen and/or inert gas are added into the imflammable gas as dilution Gas.
The utility model can selectivity oxidant gas, the oxidant gas are added into the imflammable gas For oxygen and/or air.
Using spray burning device provided by the utility model synthesis nanometer oxide material method be:By flammable gas Body exports from the air guide of the spray burning device, and in the port of gun body, burning produces flame warm area;By liquid precursor The flame warm area is sprayed to from the atomizer of the spray burning device, obtains nanometer oxide material.
According to the utility model, the pressure of the spraying is 0.5-10bar, for example, can be 0.5bar, 1bar, 2bar, Specific point value between 3bar, 4bar, 5bar, 6bar, 7bar, 8bar, 9bar or 10bar, and above-mentioned numerical value, as space is limited And the consideration for simplicity, the specific point value that scope described in the utility model no longer exclusive list includes.
According to the utility model, the spray angle θ of atomizer is 20-90 ° during the spraying, such as can be 20 °, Specific point value between 30 °, 40 °, 50 °, 60 °, 70 °, 80 ° or 90 °, and above-mentioned numerical value, as space is limited and for simplicity Consider, the specific point value that scope described in the utility model no longer exclusive list includes.
According to the utility model, during the spraying air guide close to the end face H of liquid outlet and the distance of gun body port with The diameter of section D of air guide ratio is 1-4, such as can be 1,1.5,2,2.5,3,3.5 or 4, and above-mentioned numerical value it Between specific point value, as space is limited and for simplicity consideration, the tool that scope described in the utility model no longer exclusive list includes Body point value.
Compared with prior art, the utility model at least has the advantages that:
(1) spray burning device provided by the utility model produces flame using imflammable gas, can produce stabilization Warm area;Other extra atomising devices are not needed, save space and cost;Apparatus structure is simple, compact in design, makes operation more Simple and fast, shorten technological process and preparation time;The nano-oxide product pattern of preparation, size are controllable, good quality, Added value of product is high.
(2) the utility model can ensure the even running of device, realize spraying and combustion by the regulation to device parameter Optimal matching is burnt, forms optimal spray burning system, improves the quality of product, while effectively avoid liquid in spray process Drop, particle adhesion wall are blocked the problems such as blocking cavity, are had a good application prospect.
Brief description of the drawings
Fig. 1 is the structural representation of the gun body of sprayer unit provided by the utility model, in figure:1- gun bodies, 2- water conservancy diversion structures Part, 3- atomizers, θ-spray angle, H- air guides are close to the distance of the end face of liquid outlet and gun body port, D- water conservancy diversion structures The diameter of section of part;
Fig. 2 is nanoscale CeO prepared by the utility model embodiment 12The SEM photograph of powder;
Fig. 3 is nanoscale Al prepared by the utility model embodiment 22O3The SEM photograph of powder.
The utility model is further described below.But following examples is only simple example of the present utility model Son, does not represent or limits rights protection scope of the present utility model, the scope of protection of the utility model using claims as It is accurate.
Embodiment
For the utility model is better described, the technical solution of the utility model is readily appreciated, below to the utility model It is further described.But following embodiments is only simple example of the present utility model, invention is not represented or limited Rights protection scope, the scope of protection of the utility model are defined by claims.
The utility model specific embodiment part provides a kind of spray burning device, and described device includes gun body 1, water conservancy diversion Component 2 and atomizer 3;The gun body 1 includes a cavity;The air guide 2 is arranged in the cavity, can be along described Cavity is relative to be slided;The atomizer 3 is arranged in the air guide 2, can be slided with air guide 2 along the cavity;Institute State air guide 2 with the air inlet of imflammable gas to be connected, the atomizer 3 is connected with the inlet of liquid precursor.
Preferably, the gun body 1 includes a tubular cavity.
Preferably, the air guide 2 is any one in distribution grid, guiding gutter or honeycomb ceramics.
Preferably, the atomizer 3 is pressure atomized fog jet or double fluid atomization nozzle.
Preferably, the atomizer 3 is arranged in the center position of the air guide 2.
Using spray burning device provided by the utility model synthesis nanometer oxide material method be:By flammable gas Body exports from the air guide of the spray burning device, and in the port of gun body, burning produces flame warm area;By liquid precursor The flame warm area is sprayed to from the atomizer of the spray burning device, obtains nanometer oxide material.
Typical but non-limiting embodiment of the present utility model is as follows:
Embodiment 1
As shown in figure 1, present embodiments providing a kind of spray burning device, described device includes gun body 1, air guide 2 With atomizer 3;The gun body 1 includes a cavity;The air guide 2 is arranged in the cavity, can be along the cavity It is relative to slide;The atomizer 3 is arranged in the air guide 2, can be slided with air guide 2 along the cavity;It is described to lead Stream component 2 is connected with the air inlet of imflammable gas, and the atomizer 3 is connected with the inlet of liquid precursor.
The air guide 2 is distribution grid;The atomizer 3 is double fluid atomization nozzle;The gun body 1 includes one Tubular cavity;The atomizer 3 is arranged in the center position of the air guide 2.
The spray burning device synthesis nano CeO provided using the present embodiment2The method of powder is:Prepare 0.5M Ce (NO3)3·6H2The O aqueous solution;Methane is exported from the air guide of above-mentioned spray burning device, burns and produces in the port of gun body 2000-2500 DEG C stable of flame warm area;By Ce (NO3)3·6H2Atomizer of the O aqueous solution from the spray burning device The flame warm area is sprayed to, obtains CeO2Powder.As shown in Fig. 2 obtained CeO2Powder is Nano grade.
Embodiment 2
A kind of spray burning device is present embodiments provided, described device is in addition to air guide 2 is guiding gutter, other groups Part and structure are identical with the spray burning device in embodiment 1.
The spray burning device synthesizing micron-grade Al provided using the present embodiment2O3The method of powder is:Prepare 0.5M Al (NO3)3·9H2The O aqueous solution, the gaseous mixture of methane, oxygen and argon gas is exported from the air guide of above-mentioned spray burning device, In the port of gun body, burning produces 1000 DEG C or so stable of warm area, by Al (NO3)3·9H2The O aqueous solution fires from the spraying The atomizer for burning device is sprayed to the flame warm area, obtains Al2O3Powder.As shown in figure 3, obtained Al2O3Powder is micro- Scale particles.
Embodiment 3
Present embodiments provide a kind of spray burning device, described device is honeycomb ceramics except air guide 2, the atomization Nozzle 3 is that other assemblies and structure are identical with the spray burning device in embodiment 1 outside pressure atomized fog jet.
Applicant states that the utility model illustrates detailed construction feature of the present utility model by above-described embodiment, but The utility model is not limited to above-mentioned detailed construction feature, that is, does not mean that the utility model has to rely on above-mentioned detailed construction Feature could be implemented.Person of ordinary skill in the field is new to this practicality it will be clearly understood that to any improvement of the present utility model The equivalence replacement of part selected by type and the increase of accessory, the selection of concrete mode etc., all fall within of the present utility model Within the scope of protection domain and disclosure.
Preferred embodiment of the present utility model described in detail above, still, the utility model is not limited to above-mentioned reality The detail in mode is applied, in range of the technology design of the present utility model, the technical solution of the utility model can be entered The a variety of simple variants of row, these simple variants belong to the scope of protection of the utility model.
It is further to note that each particular technique feature described in above-mentioned embodiment, in not lance In the case of shield, it can be combined by any suitable means, in order to avoid unnecessary repetition, the utility model is to each The possible combination of kind no longer separately illustrates.
In addition, it can also be combined between a variety of embodiments of the present utility model, as long as it is not disobeyed Thought of the present utility model is carried on the back, it should equally be considered as content disclosed in the utility model.

Claims (5)

1. a kind of spray burning device, it is characterised in that described device includes gun body (1), air guide (2) and atomizer (3);The gun body (1) includes a cavity;The air guide (2) is arranged in the cavity, can be relative along the cavity Slide;The atomizer (3) is arranged in the air guide (2), can be slided with air guide (2) along the cavity;It is described Air guide (2) is connected with the air inlet of imflammable gas, and the atomizer (3) is connected with the inlet of liquid precursor.
2. spray burning device as claimed in claim 1, it is characterised in that the gun body (1) includes a tubular cavity.
3. spray burning device as claimed in claim 1, it is characterised in that the air guide (2) is distribution grid, guiding gutter Or any one in honeycomb ceramics.
4. spray burning device as claimed in claim 1, it is characterised in that the atomizer (3) is pressure atomized fog jet Or double fluid atomization nozzle.
5. spray burning device as claimed in claim 1, it is characterised in that the atomizer (3) is arranged in the water conservancy diversion The center position of component (2).
CN201720501250.2U 2017-05-05 2017-05-05 A kind of spray burning device Active CN206783315U (en)

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106976845A (en) * 2017-05-05 2017-07-25 中国科学院过程工程研究所 A kind of method of spray burning device and synthesis of metal oxide powder of spraying
CN112664936A (en) * 2020-12-29 2021-04-16 华中科技大学 System for synthesizing nano-particles by multi-nozzle spray combustion

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN106976845A (en) * 2017-05-05 2017-07-25 中国科学院过程工程研究所 A kind of method of spray burning device and synthesis of metal oxide powder of spraying
CN106976845B (en) * 2017-05-05 2023-08-01 中国科学院过程工程研究所 Spray combustion device and method for synthesizing metal oxide powder by spraying
CN112664936A (en) * 2020-12-29 2021-04-16 华中科技大学 System for synthesizing nano-particles by multi-nozzle spray combustion
CN112664936B (en) * 2020-12-29 2023-03-24 华中科技大学 System for synthesizing nano-particles by multi-nozzle spray combustion

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