CN206730803U - A kind of graphite falling film absorber - Google Patents

A kind of graphite falling film absorber Download PDF

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Publication number
CN206730803U
CN206730803U CN201720255527.8U CN201720255527U CN206730803U CN 206730803 U CN206730803 U CN 206730803U CN 201720255527 U CN201720255527 U CN 201720255527U CN 206730803 U CN206730803 U CN 206730803U
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China
Prior art keywords
graphite
cylinder
annular groove
feed zone
material hole
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CN201720255527.8U
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Chinese (zh)
Inventor
姚松年
肖杰
丁明权
王瑞
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Nantong Shanjian Anticorrosion Technology Co Ltd
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Nantong Shanjian Anticorrosion Technology Co Ltd
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Abstract

The utility model discloses a kind of graphite falling film absorber, it includes the feed zone being vertically connected with and cooling down absorption segment, cooling down absorption segment is provided with graphite block, the material hole run through up and down is offered on graphite block, laterally offers and is not attached to logical Cooling Holes with material hole;Feed zone is provided with graphite cylinder, the lower surface of graphite cylinder is sealed against in the upper surface of graphite block, short transverse is provided with annular groove in the upper surface of the cylinder of graphite cylinder, cylinder is divided into inner cylinder and the outer barrel on the outside of inner cylinder by annular groove;The upper end of inner cylinder is formed as triangular-notch weir;Feed zone is provided with inlet, the inlet connects annular groove;The graphite cover plate covered on graphite cylinder is additionally provided with feed zone, the air inlet of connection graphite cylinder is offered on the graphite cover plate.The utility model can enable absorbing liquid be uniformly distributed in the inner chamber of graphite cylinder, then into the material hole of graphite block.

Description

A kind of graphite falling film absorber
Technical field
It the utility model is related to a kind of graphite falling film absorber.
Background technology
Graphitic absorber is the reactor for producing the acid such as hydrochloric acid, current, referring to Fig. 2, conventional graphite falling liquid film Absorber is provided with the upper cover for being used for air-liquid charging including graphite tube 100, is provided with and opens in the cylinder of graphite tube 100 The annular groove 101 of mouth down, liquid-inlet 102 connect annular groove 101, and absorbing liquid enters from liquid-inlet through annular groove 101 In upper cover, gas is entered in upper cover together with absorbing liquid through overflow pipe through the gas feed 104 at the top of graphitic absorber 103, which enter graphite block absorption condensation section, carries out contacting absorption and cooling.
It is opening down due to annular groove, the absorbing liquid entered from liquid-inlet 102 under gravity can immediately under Sink in the hybrid chamber of liquid-inlet side, not only cause liquid in overflow pipe area skewness, but also portion can be caused Divide in overflow pipe and be distributed without absorbing liquid, partial material hole in graphite block is distributed without absorbing liquid film-like, cause graphite falling liquid film to inhale Receive the falling film absorption function of graphite falling film absorber can not play completely under the efficiency of device.
Utility model content
The purpose of the application is to solve the above problems, there is provided a kind of graphite falling liquid film that can give full play to absorber function Absorber, avoid as follows without the few phenomenon of absorbing liquid or absorbing liquid, specific technical scheme in generation partial material hole:
A kind of graphite falling film absorber, it includes the feed zone being vertically connected with and cooling down absorption segment, set in cooling down absorption segment Graphite block is equipped with, the material hole run through up and down is offered on graphite block, laterally offers and is not attached to logical Cooling Holes with material hole; Feed zone is provided with graphite cylinder, the lower surface of the graphite cylinder is sealed against in the upper surface of graphite block, graphite cylinder The space of the upper surface of inner peripheral surface and graphite block institute corral forms hybrid chamber, and the top of the cylinder of graphite cylinder is provided with annular Groove, the annular groove is recessed downwards along short transverse by the upper surface of cylinder and is formed, and the top of cylinder is divided into interior by annular groove Cylinder and the outer barrel on the outside of inner cylinder;The upper end of the inner cylinder is formed as triangular-notch weir;Feed zone is provided with inlet, it is described enter Liquid mouth connects annular groove;The graphite cover plate covered on graphite cylinder is additionally provided with feed zone, the company of offering on the graphite cover plate The air inlet of the inner chamber of logical graphite cylinder.
The utility model sets the outlet of annular groove upward, and absorbing liquid, can be along ring after inlet enters annular groove Shape groove is distributed, and is overflowed to after absorbing liquid is full of annular groove from the top end face of inner cylinder in graphite cylinder, due to absorbing liquid edge The top end face of inner cylinder is overflowed in hybrid chamber, and absorbing liquid can be uniformly distributed in hybrid chamber, then into graphite block In material hole.In the utility model, the top end face of inner cylinder is also arranged to triangular-notch weir, triangular-notch weir can make absorbing liquid more equal Overflow to evenly in hybrid chamber.
Further, the top end face of the inner cylinder is less than the top end face of outer barrel, and the graphite cover plate is resisted against the top of outer barrel On face.This is designed to ensure that the top end face of inner cylinder has the liquid film of certain altitude, ensures that absorbing liquid can be evenly into mixed Close intracavitary.
Further, overflow pipe, the inner chamber connection material hole of overflow pipe are provided with the upper surface of graphite block.Overflow pipe is set Putting can ensure that the intracavity bottom of graphite cylinder has certain liquid storage amount, to ensure the time of contact of gas and liquid, improve gas The efficiency of liquid mixing.
The utility model can be such that absorbing liquid is circumferentially uniformly distributed along inwall, improve the uniform cloth liquid effect of overflow pipe, increase The falling film absorption ability of addition platform equipment;Absorption area is also add simultaneously, turn avoid wound of the high-temperature gas to graphite cylinder Evil, protects graphite cylinder.
Brief description of the drawings
Fig. 1 is schematic diagram of the present utility model.
Fig. 2 is the Local map of graphitic absorber of the prior art.
Embodiment
The utility model is described in further detail below in conjunction with the accompanying drawings.
Embodiment 1:
Referring to Fig. 1, a kind of graphite falling film absorber, it includes the feed zone being vertically connected with and cooling down absorption segment, cold But absorber portion is provided with graphite block 21, and the material hole 23 run through up and down is offered on graphite block 21, laterally offers and material hole 23 are not attached to logical Cooling Holes 22;Feed zone is provided with the graphite cylinder 10 of a upper and lower opening, the lower end of the graphite cylinder 10 Face is sealed against in the space of the upper surface of graphite block 21, the inner peripheral surface of graphite cylinder 10 and 24 corrals in upper surface of graphite block Form hybrid chamber, be provided with annular groove 11 on the top of the cylinder of graphite cylinder 10, the annular groove 11 by cylinder upper surface Recessed and is formed downwards along short transverse, the top of cylinder is divided into inner cylinder 16 and the outer barrel on the outside of inner cylinder 16 by annular groove 11 15;Be formed as triangular-notch weir 14 in the upper end of inner cylinder 16;Feed zone is provided with inlet 12, inlet 12 connects annular groove 11; The graphite cover plate 19 covered on graphite cylinder 10 is additionally provided with feed zone, connection graphite cylinder is offered on the graphite cover plate 19 Inner chamber air inlet 17, i.e., air inlet 17 connect hybrid chamber.
In the present embodiment, the top end face of inner cylinder 16 is less than the top end face of outer barrel 15, and the graphite cover plate 19 is resisted against outer On the top end face of cylinder 15.Overflow pipe 13, the inner chamber connection material hole 23 of overflow pipe 13 are provided with the upper surface of graphite block 21.
Distance L of the top of triangular-notch weir apart from the lower surface of graphite cover plate is 30-60mm, and the height of the triangular-notch weir is 40-60mm.Specific in the present embodiment, L 50mm, the height of triangular-notch weir is 60mm.
The depth A1 of annular groove be inner cylinder top end face to the distance A2 of the upper surface of graphite block 35-55%.Specific to A1 is the 45% of A2 in the present embodiment.
When the present embodiment is run, gas is entered in hybrid chamber by air inlet 17, and absorbing liquid enters through inlet 12 In annular groove 11, then overflowed to along triangular-notch weir 14 in hybrid chamber, in hybrid chamber, through overflow pipe after absorbing liquid and gas mixing 13 are entered in material hole 23, and then the liquid outlet 18 through graphite falling film absorber lower end is discharged.Coolant is through refrigerant import 32 Enter in the Cooling Holes 22 of graphite block 21, discharged after being exchanged heat with the liquid in material hole through refrigerant exit 34.

Claims (3)

1. a kind of graphite falling film absorber, it is characterised in that including the feed zone and cooling down absorption segment being vertically connected with, inhaled in cooling Receive section be provided with graphite block, the material hole run through up and down is offered on graphite block, laterally offer be not attached to material hole it is logical Cooling Holes;Feed zone is provided with graphite cylinder, the lower surface of the graphite cylinder is sealed against in the upper surface of graphite block, graphite The space of the inner peripheral surface of cylinder and the upper surface institute corral of graphite block forms hybrid chamber, is set on the top of the cylinder of graphite cylinder There is an annular groove, the annular groove is recessed downwards along short transverse by the upper surface of cylinder and is formed, and annular groove is by the top of cylinder It is divided into inner cylinder and the outer barrel on the outside of inner cylinder;The upper end of the inner cylinder is formed as triangular-notch weir;Feed zone is provided with inlet, The inlet connects annular groove;The graphite cover plate covered on graphite cylinder is additionally provided with feed zone, is opened on the graphite cover plate It is communicated with the air inlet of the inner chamber of graphite cylinder.
2. graphite falling film absorber according to claim 1, it is characterised in that the top end face of the inner cylinder is less than outer barrel Top end face, the graphite cover plate are resisted against on the top end face of outer barrel.
3. graphite falling film absorber according to claim 1, it is characterised in that the upper surface of graphite block is provided with overflow Pipe, the inner chamber connection material hole of overflow pipe.
CN201720255527.8U 2017-03-16 2017-03-16 A kind of graphite falling film absorber Active CN206730803U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720255527.8U CN206730803U (en) 2017-03-16 2017-03-16 A kind of graphite falling film absorber

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720255527.8U CN206730803U (en) 2017-03-16 2017-03-16 A kind of graphite falling film absorber

Publications (1)

Publication Number Publication Date
CN206730803U true CN206730803U (en) 2017-12-12

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CN201720255527.8U Active CN206730803U (en) 2017-03-16 2017-03-16 A kind of graphite falling film absorber

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114699881A (en) * 2022-03-10 2022-07-05 北京航化节能环保技术有限公司 Self-cooling graphite quenching absorber and absorbing device
CN115228246A (en) * 2022-07-26 2022-10-25 南通星球石墨股份有限公司 Round block hole type multi-section distribution efficient falling film absorber

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN114699881A (en) * 2022-03-10 2022-07-05 北京航化节能环保技术有限公司 Self-cooling graphite quenching absorber and absorbing device
CN114699881B (en) * 2022-03-10 2024-05-31 北京航化节能环保技术有限公司 Self-cooling graphite quenching absorber and absorption device
CN115228246A (en) * 2022-07-26 2022-10-25 南通星球石墨股份有限公司 Round block hole type multi-section distribution efficient falling film absorber
CN115228246B (en) * 2022-07-26 2023-08-11 南通星球石墨股份有限公司 Round block hole type multi-section distribution high-efficiency falling film absorber

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