CN206688685U - A kind of anhydrous sodium acetate production device - Google Patents
A kind of anhydrous sodium acetate production device Download PDFInfo
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- CN206688685U CN206688685U CN201720421092.XU CN201720421092U CN206688685U CN 206688685 U CN206688685 U CN 206688685U CN 201720421092 U CN201720421092 U CN 201720421092U CN 206688685 U CN206688685 U CN 206688685U
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- sodium acetate
- retort
- stirring motor
- anhydrous sodium
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Abstract
The utility model discloses a kind of anhydrous sodium acetate production device, including：Retort, the retort upper center is provided with stirring motor, the side of the stirring motor is provided with sodium acetate inlet, the stirring motor is provided with soda ash charging aperture away from sodium acetate inlet, the rotary head of the stirring motor is provided with agitating shaft, the agitating shaft is interspersed in the inside of retort, and one end both sides of the agitating shaft away from stirring motor are equipped with multiple rotary scrapings；The retort lower end is provided with liquid outlet, and the liquid outlet is connected by pipeline with electric pump.The utility model is by soda ash and goes out sour calcium reaction, the reaction is irreversible reaction, acted on by rotary scraping, accelerate reactant reaction, again by filter, the lower removing insoluble impurities of active carbon adsorber effect and soluble impurity, anhydrous sodium acetate is finally made in the presence of dehydrating kettle, substantially increases the yield of sodium acetate, while improve purity.
Description
Technical field
It the utility model is related to the production technical field of anhydrous sodium acetate, more particularly to a kind of anhydrous sodium acetate production dress
Put.
Background technology
Anhydrous sodium acetate CH3COONa, colourless transparent crystal is widely used, can make esterifying agent and the photography of organic synthesis
Many aspects such as medicine, medicine, printing and dyeing mordant, buffer, chemical reagent, meat anticorrosion, pigment, tanning.Anhydrous sodium acetate
It is divided into technical grade, food-grade, pharmaceutical grade and SILVER REAGENT.Its production method is to carry out preparing acetic acid using the reaction of soda ash and acetic acid
Sodium, but the bad control of proportioning in device for acetic acid and dietary alkali, be put into acetic acid it is more or less when, can all cause to react
The waste of thing, and the stable content of product is also poor.
Through retrieval, the publication number of Chinese granted patent：CN202181269U；Denomination of invention：One kind production anhydrous sodium acetate
Device, it includes reactor, and reactor is provided with feed pipe and discharge nozzle, it is characterised in that：It is additionally provided with acetic acid head tank,
Described acetic acid head tank includes cell body, and cell body is provided with charging aperture, and the bottom of cell body is provided with discharging opening, discharging opening and reactor
Feed pipe between connected by pipeline, the sidepiece of cell body is connected with tank gage.The utility model by using acetic acid head tank,
Acetic acid is flowed into naturally in reactor from acetic acid head tank, reach continuous balanced reaction, while acetic acid is measured by tank gage
Amount, make acetic acid and dietary alkali proportion speed, the product quality stabilization of manufacture.Its is reasonable in design, simple and reasonable, user
Just, acetic acid is reacted appropriate with dietary alkali, improve product quality, reduce defect rate；But acetic acid is to belong to weak acid, it reacts
For reversible reaction, obtained sodium acetate purity is not very high, makes generated product content not high.
Utility model content
The utility model is intended to one of technical problem at least solving in correlation technique to a certain extent.Therefore, this reality
It is to propose a kind of anhydrous sodium acetate production device with a new purpose, the process units is anti-with going out sour calcium by soda ash
Should, the reaction is irreversible reaction, is acted on by rotary scraping, accelerates reactant reaction, then by filter, charcoal absorption
Device effect is lower to remove insoluble impurities and soluble impurity, and anhydrous sodium acetate is finally made in the presence of dehydrating kettle, carries significantly
The high yield of sodium acetate, while improve purity.
According to a kind of anhydrous sodium acetate production device of the utility model embodiment, including：Retort, in the retort
End middle part is provided with stirring motor, and the side of the stirring motor is provided with sodium acetate inlet, and the stirring motor is away from sodium acetate
Inlet is provided with soda ash charging aperture, and the rotary head of the stirring motor is provided with agitating shaft, and the agitating shaft is interspersed in retort
Inside, one end both sides of the agitating shaft away from stirring motor are equipped with multiple rotary scrapings；The retort lower end is provided with out
Liquid mouth, the liquid outlet are connected by pipeline with electric pump, and the drain pipe mouth of the electric pump connects with filter pipes, the filtering
The drain pipe mouth of device and active carbon adsorber pipeline communication, drain pipe mouth and the dehydrating kettle pipeline of the active carbon adsorber connect
It is logical.
In some embodiments of the utility model, the retort lower end is provided with support frame.
In other embodiments of the present utility model, the side wall of the retort is provided with observation panel.
In other embodiments of the present utility model, the observation panel is provided with transparent PC material plate.
In other embodiments of the present utility model, the liquid outlet is provided with magnetic valve.
Beneficial effect in the utility model is：Retort upper end both sides are respectively equipped with calcium acetate inlet and fed with soda ash
Mouthful, reacted using calcium acetate and soda ash, generation has white opacity solid and sodium acetate solution, and retort is provided with stirring electricity
Machine, stirring motor drive the rotary scraping of agitating shaft bottom to be rotated, reactant is sufficiently mixed, observation panel observable
Response situation, the mixed liquor after the completion of reaction flow out from the liquid outlet of retort, enter filter, filter under electric pump effect
Precipitation in mixed solution is removed, the sodium acetate solution of clarification flows out from filter drain pipe mouth, into active carbon adsorber
In under the suction-operated of activated carbon, slough its color, solution is bleached or micro white, then the drain pipe from active carbon adsorber
Mouth is flowed into dehydrating kettle, is dehydrated, that is, anhydrous sodium acetate is made；The utility model is by soda ash and goes out sour calcium reaction, and this is anti-
Irreversible reaction is should be, is acted on by rotary scraping, accelerates reactant reaction, then act on by filter, active carbon adsorber
Lower removing insoluble impurities and soluble impurity, anhydrous sodium acetate is finally made in the presence of dehydrating kettle, substantially increases vinegar
The yield of sour sodium, while improve purity.
Brief description of the drawings
Accompanying drawing is used for providing further understanding to of the present utility model, and a part for constitution instruction, with this practicality
New embodiment is used to explain the utility model together, does not form to limitation of the present utility model.In the accompanying drawings：
Fig. 1 be the utility model proposes a kind of anhydrous sodium acetate production device structural representation.
In figure：1- retort, 2- soda ash charging aperture, 3- calcium acetates inlet, 4- stirring motors, 5- agitating shafts, 6- rotations
Scraping blade, 7- support frames, 8- magnetic valves, 9- pipelines, 10- electric pumps, 11- filters, 12- active carbon adsorbers, 13- dehydrating kettles.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the embodiment of the utility model is carried out
Clearly and completely describing, it is clear that described embodiment is only the utility model part of the embodiment, rather than whole
Embodiment.
The example of the embodiment is shown in the drawings, wherein same or similar label represents identical or class from beginning to end
As element or with same or like function element.The embodiments described below with reference to the accompanying drawings are exemplary, purport
For explaining the utility model, and it is not intended that to limitation of the present utility model.
In description of the present utility model, it is to be understood that term " " center ", " longitudinal direction ", " transverse direction ", " length ", " width
Degree ", " thickness ", " on ", " under ", "front", "rear", "left", "right", " vertical ", " level ", " top ", " bottom " " interior ", " outer ", " suitable
The orientation or position relationship of the instruction such as hour hands ", " counterclockwise ", " axial direction ", " radial direction ", " circumference " are based on orientation shown in the drawings
Or position relationship, be for only for ease of description the utility model and simplify and describe, rather than instruction or imply signified device or
Element must have specific orientation, with specific azimuth configuration and operation, therefore it is not intended that to limit of the present utility model
System.
In addition, term " first ", " second " are only used for describing purpose, and it is not intended that instruction or hint relative importance
Or the implicit quantity for indicating indicated technical characteristic.Thus, define " first ", the feature of " second " can be expressed or
Implicitly include one or more this feature.In description of the present utility model, " multiple " are meant that two or two
More than, unless otherwise specifically defined.
In the utility model, unless otherwise clearly defined and limited, term " installation ", " connected ", " connection ", " Gu
It is fixed " etc. term should be interpreted broadly, for example, it may be fixedly connected or be detachably connected, or integrally；Can be
Mechanically connect or electrically connect；Can be joined directly together, can also be indirectly connected by intermediary, can be two
The connection of element internal or the interaction relationship of two elements.For the ordinary skill in the art, can basis
Concrete condition understands concrete meaning of the above-mentioned term in the utility model.
Reference picture 1, a kind of anhydrous sodium acetate production device, including：Retort 1, the upper center of retort 1 are provided with stirring
Motor 4, the model Y315S-2 of stirring motor 4, the side of stirring motor 4 are provided with sodium acetate inlet 3, and stirring motor 4 is remote
Sodium acetate inlet 3 is provided with soda ash charging aperture 2, and the rotary head of stirring motor 4 is provided with agitating shaft 5, and agitating shaft 5 is interspersed in retort
1 inside, one end both sides of the agitating shaft 5 away from stirring motor 4 are equipped with multiple rotary scrapings 6；The lower end of retort 1 is provided with out liquid
Mouthful, liquid outlet connected by pipeline 9 with electric pump 10, the model QY200-12-7.5 of electric pump 10, the drain pipe mouth of electric pump 10 and
The pipeline communication of filter 11, drain pipe mouth and the pipeline communication of active carbon adsorber 12 of filter 11, active carbon adsorber 12
Drain pipe mouth and the pipeline communication of dehydrating kettle 13；The lower end of retort 1 is provided with support frame 7；The side wall of retort 1 is provided with observation panel；
Observation panel is provided with transparent PC plate of material；Liquid outlet is provided with magnetic valve 8, the model 4M310 of magnetic valve 8.
The upper end both sides of retort 1 are respectively equipped with calcium acetate inlet 3 and soda ash charging aperture 2, are entered using calcium acetate and soda ash
Row reaction, generation have white opacity solid and sodium acetate solution, and retort 1 is provided with stirring motor 4, and stirring motor 4 drives and stirred
The rotary scraping 6 for mixing the bottom of axle 5 is rotated, and reactant is sufficiently mixed, observation panel observable response situation, reaction
After the completion of mixed liquor flowed out from the liquid outlet of retort 1, filter 11 is entered under the effect of electric pump 10, filter 11 will mixing
Precipitation in solution removes, and the sodium acetate solution of clarification flows out from the drain pipe mouth of filter 11, into active carbon adsorber 12
Under the suction-operated of activated carbon, its color is sloughed, solution is bleached or micro white, then the drain pipe from active carbon adsorber 12
Mouth is flowed into dehydrating kettle 13, is dehydrated, that is, anhydrous sodium acetate is made；The utility model is by soda ash and goes out sour calcium reaction, should
React for irreversible reaction, acted on by rotary scraping 6, accelerate reactant reaction, then by filter 11, active carbon adsorber
12 effects are lower to remove insoluble impurities and soluble impurity, anhydrous sodium acetate is finally made in the presence of dehydrating kettle 13, significantly
The yield of sodium acetate is improved, while improves purity.
Production procedure of the present utility model is：Added by calcium acetate inlet 3 and soda ash charging aperture 2 toward retort 1 is interior
Material, after charging, stirring motor 4 starts, and stirring motor 4 drives the rotary scraping 6 on agitating shaft 5 to move in a circle, and promotes
Reactant hybrid reaction, the extent of reaction in observation panel observable retort 1, after completion of the reaction, open magnetic valve 8, electric pump 10
Start, mixed liquor is from liquid outlet by the inflow filter 11 of pipeline 9, entering back into active carbon adsorber 12, by mixed liquor
It is soluble to be removed with insolubility impurity, finally enter in dehydrating kettle 13, slough moisture under the effect of dehydrating kettle 13, that is, nothing is made
Water acetic acid sodium, the anhydrous sodium acetate purity is higher, and yield is larger, can meet the needs of market is to anhydrous sodium acetate.
In the utility model, unless otherwise clearly defined and limited, fisrt feature is "above" or "below" second feature
Can be that the first and second features directly contact, or the first and second features pass through intermediary mediate contact.Moreover, first is special
Sign second feature " on ", " top " and " above " can be fisrt feature directly over second feature or oblique upper, or only
Represent that fisrt feature level height is higher than second feature.Fisrt feature second feature " under ", " lower section " and " below " can be with
Be fisrt feature immediately below second feature or obliquely downward, or be merely representative of fisrt feature level height and be less than second feature.
In the description of this specification, reference term " one embodiment ", " some embodiments ", " example ", " specifically show
The description of example " or " some examples " etc. means specific features, structure, material or the spy for combining the embodiment or example description
Point is contained at least one embodiment or example of the present utility model.In this manual, to the schematic table of above-mentioned term
State and be not necessarily referring to identical embodiment or example.Moreover, specific features, structure, material or the feature of description can be
Combined in an appropriate manner in any one or more embodiments or example.
It is described above, the only preferable embodiment of the utility model, but the scope of protection of the utility model is not
This is confined to, any one skilled in the art is in the technical scope that the utility model discloses, according to this practicality
New technical scheme and its utility model design are subject to equivalent substitution or change, should all cover in protection model of the present utility model
Within enclosing.
Claims (5)
- A kind of 1. anhydrous sodium acetate production device, it is characterised in that including：Retort, the retort upper center are provided with stirring motor, and the side of the stirring motor is provided with sodium acetate inlet, The stirring motor is provided with soda ash charging aperture away from sodium acetate inlet, and the rotary head of the stirring motor is provided with agitating shaft, institute The inside that agitating shaft is interspersed in retort is stated, one end both sides of the agitating shaft away from stirring motor are equipped with multiple rotations and scraped Piece；The retort lower end is provided with liquid outlet, and the liquid outlet is connected by pipeline with electric pump, the drain pipe mouth of the electric pump Connected with filter pipes, drain pipe mouth and the active carbon adsorber pipeline communication of the filter, the active carbon adsorber Drain pipe mouth and dehydrating kettle pipeline communication.
- A kind of 2. anhydrous sodium acetate production device according to claim 1, it is characterised in that：The retort lower end is provided with Support frame.
- A kind of 3. anhydrous sodium acetate production device according to claim 1, it is characterised in that：In the side wall of the retort Provided with observation panel.
- A kind of 4. anhydrous sodium acetate production device according to claim 3, it is characterised in that：The observation panel is provided with saturating Bright PC plate of material.
- A kind of 5. anhydrous sodium acetate production device according to claim 1, it is characterised in that：The liquid outlet is provided with electricity Magnet valve.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720421092.XU CN206688685U (en) | 2017-04-20 | 2017-04-20 | A kind of anhydrous sodium acetate production device |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720421092.XU CN206688685U (en) | 2017-04-20 | 2017-04-20 | A kind of anhydrous sodium acetate production device |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206688685U true CN206688685U (en) | 2017-12-01 |
Family
ID=60445667
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720421092.XU Expired - Fee Related CN206688685U (en) | 2017-04-20 | 2017-04-20 | A kind of anhydrous sodium acetate production device |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206688685U (en) |
-
2017
- 2017-04-20 CN CN201720421092.XU patent/CN206688685U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CP01 | Change in the name or title of a patent holder | ||
| CP01 | Change in the name or title of a patent holder |
Address after: The North Industrial Park of Ji'an city of Jiangxi province Xingan County 331300 Patentee after: Jiangxi Shuangjia Technology Co.,Ltd. Address before: The North Industrial Park of Ji'an city of Jiangxi province Xingan County 331300 Patentee before: JIANGXI SHUANGJIA TECHNOLOGY DEVELOPMENT Co.,Ltd. |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20171201 Termination date: 20210420 |