CN206676376U - A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging - Google Patents
A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging Download PDFInfo
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- CN206676376U CN206676376U CN201720371337.2U CN201720371337U CN206676376U CN 206676376 U CN206676376 U CN 206676376U CN 201720371337 U CN201720371337 U CN 201720371337U CN 206676376 U CN206676376 U CN 206676376U
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Abstract
The utility model belongs to field of chemical equipment, more particularly to a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging, it, which is formed, includes closed cylinder reaction staving, support, transmission system, sealing system, vacuum and the aerating mouth and temperature and pressure measurement apparatus for supporting reaction staving in axial unsymmetric structure, charge door and discharging opening, chuck, baffle plate is provided with reaction container body, wherein, described cylinder reaction staving is rotatable, and described cylinder reaction staving is set with rotary shaft in 10~60 ° of oblique angles.It is more that the utility model can effectively solve residual material existing for prior art, it is necessary to is cleared up, the problem of so as to extend the operation cycle of reactor, after the completion of reaction, discharging is convenient, and it is clean that material is able to discharge, so as to improve the efficiency of reactor.
Description
Technical field
The utility model belongs to field of chemical equipment, and in particular to a kind of rotation suitable for gas-solid phase reaction of convenient discharging
Rotatable reactor, available for preparing chlorosulfonated polyethylene, haloflex, chliorinated polyvinyl chloride, chlorosulfonation reclaimed rubber.
Background technology
It is to be placed in the high polymer material for intending participating in reaction instead that gas-solid phase reaction, which prepares chlorination or chlorosulfonation high polymer material,
Answer in device, be passed through chlorine or sulfur dioxide/chlorine gaseous mixture is reacted and is made, the reactor used at present is that fluid bed is anti-
Device or fixed bed reactors, such as Patent No. ZL 2,016 2 0579368.2 novel practical are answered to invent the rotary of report
Reactor.Such reactor is that powdery high polymer material is placed in the rotary barrel of reactor, and cylinder rotation produces material
Flip-like flows, and is passed through reaction gas and is reacted.Problems be present in such reactor：Due to reactor rotary barrel and rotation
Axle is in symmetrical horizontal structure so that and after the completion of reaction, discharging produces difficulty, and material is difficult to discharge totally, and residual material is more,
It must be cleared up, so as to extend the operation cycle of reactor, have impact on the efficiency of reactor.
The content of the invention
In order to solve the above-mentioned problems of the prior art, the utility model aims to provide a kind of can realize and discharged conveniently,
Discharging is clean, suitable for the rotary reactor of gas-solid phase reaction, can be considered ZL 201620579368.2 improvement.On the one hand
Can solve the problems, such as the dust problem of the circulatory system and course of reaction materials from bonding incipient scorch, on the other hand can also solve reactor
Discharge difficult problem.
To realize goal of the invention, inventor provides following technical scheme：
A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging, it, which is formed, includes closed being in that axial direction is non-
The cylinder of symmetrical structure reacts staving, the support for supporting reaction staving, reacts staving powered rotation for cylinder
The transmission system supported with transmission, the sealing system being connected with support (configure, for sealing instead to ensure to react staving pressure
Answer staving), for vacuumized inside reaction container body temperature with the vacuum of aerating and aerating mouth and course of reaction monitoring and
Baffle plate (to drive solid material to be overturn in bucket) is configured with device for pressure measurement, cylindrical reaction container body, reaction staving is set
Have charge door and discharging opening and react staving outer wall be provided with heating and cooling chuck (be used for staving to reaction heating or cooling), its
In, it is described closed rotatable in the cylinder reaction staving of axial unsymmetric structure, described cylinder reaction staving with
Rotary shaft is set in 10~60 ° of oblique angles.
Rotary reactor provided by the utility model suitable for gas-solid phase reaction can be used for gas-solid phase reaction production chlorine
Sulfonated polyethylene, haloflex, chliorinated polyvinyl chloride, chlorosulfonation reclaimed rubber etc..The utility model uses built-in ultraviolet
Light source, institute it is baffled material is stirred upwards, double material stirring effect, at the same be equipped with temperature and pressure measurement apparatus with
And sealing system, make it possible production large-scale, and can solve the dust problem of the circulatory system and course of reaction material glues
The problem of coking is burnt.It is more prominent, cylinder reaction staving and rotary shaft of the present utility model in 10~60 ° of oblique angles this
Kind is set, and can be caused after the completion of reaction, and discharging is convenient, and material is able to discharge totally, so as to improve the efficiency of reactor.
Preferably, in the utility model, described baffle plate is 2~6 pieces, axially uniform along reaction inner wall of barrel,
Avoid discharging opening and manhole simultaneously.
Preferably, in the utility model, the draw ratio of described cylinder reaction staving is 1：0.5~2.
Preferably, in the utility model, described cylinder reaction staving is by motor through reductor and transmission
System drives rotation, and rotating speed is 0~50 rev/min.
Preferably, in the utility model, the design operation pressure of described cylinder reaction staving for -0.1~
0.5Mpa, reaction container are provided with chuck in vitro, and chuck design pressure is 0.5Mpa.
Preferably, in the utility model, the both ends of described cylinder reaction staving use ellipse head.
Preferably, in the utility model, the inwall and baffle plate of described cylinder reaction staving are used and are resistant to
By chlorine, hydrogen chloride, sulfur dioxide steel material.Further, can also be in steel if necessary using resistant material preservative treatment
Preservative treatment is done on prepared material, such as serves as a contrast ultra-high molecular weight polyethylene, spraying polytetrafluoroethylene (PTFE), silicon nitride, acid-resistant epoxy resin.
Preferably, in the utility model, described sealing system is mechanical sealing system, is to ensure reaction container
The mechanical sealing system that body pressure is configured.
Preferably, in the utility model, the top of described cylinder reaction staving is provided with manhole.
Compared with prior art, have the advantages of the utility model：
Chlorine reaction is placed in confined space and carried out by the rotary reactor of the present utility model suitable for gas-solid phase reaction,
This set of cylinder reaction staving with rotary shaft in 10~60 ° of oblique angles, it can make it that after the completion of reaction, discharging is convenient,
Material is able to discharge totally, so as to improve the efficiency of reactor.Using built-in ultraviolet light source, solves the circulatory system
The exposure dose control problem of dust problem and external light source, it can effectively control the reaction speed of chlorosulfonation so that reactor
Maximization is possibly realized.Meanwhile the design of baffle plate can drive solid material to be overturn in bucket, make material mixing more uniform, stir
Mix effect to double, solve the problems, such as course of reaction materials from bonding incipient scorch.
Brief description of the drawings
Fig. 1 is the structural representation of the rotary reactor of the utility model,
In figure, 1 is the closed cylinder reaction staving in axial unsymmetric structure, and 2 be support, and 3 be transmission system, 4
It is closed system, 5 be vacuum and aerating mouth, and 6 be temperature and pressure measurement apparatus, and 7 be baffle plate, and 8 be charge door, and 9 be discharging opening,
10 be chuck.
Embodiment
With reference to the accompanying drawings and examples, content of the present utility model is further illustrated.It should be appreciated that the utility model
Implementation be not limited to the following examples, any formal accommodation for being made to the utility model and/or change all will
Fall into scope of protection of the utility model.
Embodiment 1
As shown in figure 1, a kind of rotary reactor suitable for gas-solid phase reaction, its form include it is closed in axial non-
(draw ratio of reaction staving is 1 to the cylinder reaction staving 1 of symmetrical structure:0.8), for supporting the support 2 of reaction staving, being
Cylinder reaction staving powered rotation and transmission support transmission system 3, be connected with support mechanical sealing system 4 (for
Ensure react staving pressure and configure), for being vacuumized inside reaction container body and the vacuum of aerating and aerating mouth 5, course of reaction
The temperature and pressure measurement apparatus 6 of monitoring, being provided with the inner wall arrangement for launching material mouth has baffle plate 7 (to drive solid material to exist
Overturn in bucket), described baffle plate is 2 pieces, uniform along reaction inner wall of barrel, while avoids discharging opening and manhole, and reaction staving is set
There are charge door 8 and discharging opening 9, be provided with the outer wall of reaction staving for the chuck 10 for reacting staving heating or cooling and instead
Answer and be provided with manhole at the top of staving, the both ends of described reaction staving use ellipse head, wherein, it is described it is closed be in axial non-
The cylinder reaction staving of symmetrical structure is rotatable, and described cylinder reaction staving is set with rotary shaft in 60 ° of oblique angles to be installed.
Citing, in production, haloflex powder and antitack agent are added in rotary reactor, irradiated in ultraviolet
Under staving Stirring, reaction staving drives rotation by motor through reductor and transmission system, and rotating speed is 0~50 rev/min
Clock, be passed through by sulfur dioxide and chlorine obtained gaseous mixture by a certain percentage, react the design operation pressure of staving for -0.1~
0.5Mpa, reaction container are provided with chuck in vitro, and chuck design pressure is 0.5Mpa, and chlorosulfonation occurs under certain pressure and temperature
Reaction, after reaction terminates, product is put and rinsed in water to remove acidic by-products, then through dehydrating to obtain chlorosulfonation
Polyethylene powders.Do not occur the problem of dust problem and course of reaction materials from bonding incipient scorch in production process.After the completion of reaction,
Discharging is convenient, and material is able to discharge totally, so as to improve the efficiency of reactor, it is more not to occur residual material, it is necessary to carry out
Cleaning, the problem of so as to extend the operation cycle of reactor.
Although inventor has done more detailed elaboration and enumerated to the technical solution of the utility model, should manage
Solution, for the those skilled in the art of this area one, above-described embodiment is modified and/or flexible or use is equivalent
Alternative solution be obvious, can not all depart from the essence of spirit of the present invention, the term occurred in the utility model is used for this
The elaboration and understanding of utility model technical scheme, can not be formed to limitation of the present utility model.
Claims (9)
1. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging, it, which is formed, includes closed being in that axial direction is non-right
The cylinder reaction staving (1) of structure, the support (2) for supporting reaction staving, it is referred to as that cylinder reaction staving rotation provides
Transmission system (3) that power and transmission are supported, the sealing system (4) being connected with support, for being vacuumized inside reaction container body and
The vacuum and aerating mouth (5) of aerating and the temperature and pressure measurement apparatus (6) of course of reaction monitoring, cylinder reaction staving
Inside it is configured with baffle plate (7), reaction staving is provided with charge door (8) and discharging opening (9) and the outer wall of reaction staving is provided with heating and cooling
Chuck (10), it is characterised in that described closed, institute rotatable in the cylinder reaction staving (1) of axial unsymmetric structure
The cylinder reaction staving stated is set with rotary shaft in 10~60 ° of oblique angles.
2. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, described baffle plate (7) is 2~6 pieces, axially uniform along reaction inner wall of barrel, while avoids discharging opening and manhole.
3. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, the draw ratio of described cylinder reaction staving (1) is 1：0.5~2.
4. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, described cylinder reaction staving (1) drives rotation by motor through reductor and transmission system, and rotating speed is 0~50 turn/
Minute.
5. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, the design operation pressure of described cylinder reaction staving (1) is -0.1~0.5Mpa, and reaction container is provided with chuck in vitro
(10), chuck design pressure is 0.5Mpa.
6. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, the both ends of described cylinder reaction staving (1) use ellipse head.
7. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, the inwall and baffle plate of described cylinder reaction staving (1) are using tolerable chlorine, hydrogen chloride, the steel of sulfur dioxide
Material.
8. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, described sealing system (4) is mechanical sealing system.
9. a kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging according to claim 1, its feature
It is, the top of described cylinder reaction staving (1) is provided with manhole.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720371337.2U CN206676376U (en) | 2017-04-11 | 2017-04-11 | A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720371337.2U CN206676376U (en) | 2017-04-11 | 2017-04-11 | A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging |
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| CN206676376U true CN206676376U (en) | 2017-11-28 |
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| CN201720371337.2U Active CN206676376U (en) | 2017-04-11 | 2017-04-11 | A kind of rotary reactor suitable for gas-solid phase reaction of convenient discharging |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111690450A (en) * | 2020-06-30 | 2020-09-22 | 陈柽 | Natural gas purification treatment tower convenient to clearance |
-
2017
- 2017-04-11 CN CN201720371337.2U patent/CN206676376U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN111690450A (en) * | 2020-06-30 | 2020-09-22 | 陈柽 | Natural gas purification treatment tower convenient to clearance |
| CN111690450B (en) * | 2020-06-30 | 2021-04-02 | 阳城县舜天达天然气有限公司 | Natural gas purification treatment tower convenient to clearance |
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