CN206631595U - HMDS preparation reactor based on cooldown rate control - Google Patents
HMDS preparation reactor based on cooldown rate control Download PDFInfo
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- CN206631595U CN206631595U CN201720231875.1U CN201720231875U CN206631595U CN 206631595 U CN206631595 U CN 206631595U CN 201720231875 U CN201720231875 U CN 201720231875U CN 206631595 U CN206631595 U CN 206631595U
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Abstract
The utility model discloses a kind of HMDS preparation reactor based on cooldown rate control, it includes reactor kettle；Multiple cooling jackets extended in the horizontal direction are provided between the outer wall and inwall of the reactor kettle, multiple cooling jacket in the vertical directions are sequentially distributed, each cooling jacket is conducted to by cooling pipe among the cryogen tank being arranged on outside reactor kettle respectively, and magnetic valve is provided with inside each cooling pipe；The above-mentioned HMDS preparation reactor based on cooldown rate control can pass through the Uniform Control for material cooldown rate before and after cooling stage in reactor kettle, so that its overall cooling effect is improved, and it is improved HMDS finished product accuracy.
Description
Technical field
It the utility model is related to field of fine chemical, especially a kind of HMDS based on cooldown rate control
Preparation reactor.
Background technology
HMDS prepare be both needed in being prepared by cooling treatment with obtain HMDS into
Product.Existing HMDS is often handled in actual cooling procedure using traditional natural cooling, however, due to thing
There is some difference with its cooldown rate at a lower temperature for material cooldown rate at relatively high temperatures, and its actual cools down is spent
Bad phenomenon be present, and then the precision of its actual cooling gained finished product is affected.
Utility model content
The technical problems to be solved in the utility model is to provide a kind of HMDS preparation reactor, and it can be
Correlative carries out Homogenization Treatments of the cooling stage realization for its cooldown rate, and then the effect and finished product being allowed to cool
Precision be improved.
In order to solve the above technical problems, it the utility model is related to a kind of HMDS based on cooldown rate control
Preparation reactor, it includes reactor kettle；It is provided between the outer wall and inwall of the reactor kettle multiple in water
Square cooling jacket upwardly extended, multiple cooling jacket in the vertical directions are sequentially distributed, and each cooling jacket leads to respectively
Supercooling pipeline is conducted among the cryogen tank being arranged on outside reactor kettle, is provided with inside each cooling pipe
Magnetic valve.
As a kind of improvement of the present utility model, at least four is provided between the inwall and outer wall of the reactor kettle
Cooling jacket.Using above-mentioned technical proposal, it can be configured so that reactor kettle top with by multiple cooling jackets
Portion obtain and cooling treatment.
As it is of the present utility model it is a kind of improve, the cooling jacket include multiple top cooling jackets and it is multiple under
Portion's cooling jacket, multiple bottom cooling jackets are set in turn in below the cooling jacket of top；The top cooling jacket uses ring
Shape structure, the bottom cooling jacket is using the ripple struction extended in the horizontal direction.Using above-mentioned technical proposal, it can make
The top cooling jacket of loop configuration must be used to cool off the Fast Filling of agent, and then achieve quick cooling treatment；Together
When, using the bottom cooling jacket of ripple struction it can be made to be improved relative to the contact area of reactor inner wall of kettle, entered
And it is set to cause the overall thing in reactor kettle for realizing efficient cooling treatment positioned at the material of reactor autoclave body bottom
The cooling of material, which is spent, to be improved.
As a kind of improvement of the present utility model, each cooling jacket is respectively connected with two cooling pipes, and it is on anti-
The axis of kettle kettle is answered into symmetrically；Each cooling pipe tilts upward by the link position of itself and cooling jacket to be prolonged
Stretch.Using above-mentioned technical proposal, it quickly can uniformly be filled by the cooling agent that is configured so that of multiple cooling pipes
To cooling jacket, its cooling effectiveness is caused to be improved；At the same time, the direction of cooling pipe sets and then may be such that cooling
Agent is quickly circulated when flowing to inside cooling jacket, further to improve its cooling effectiveness.
Using the HMDS preparation reactor based on cooldown rate control of above-mentioned technical proposal, it can lead to
Cross and be arranged on multiple cooling jackets inside reactor kettle to realize for reactor kettle materials inside step by step at cooling
Reason；When reactor kettle materials inside is under temperature higher state, it only turns on cooling agent inside single cooling jacket, and then
Cooling treatment step by step is able on the premise of avoiding material from being able to quick refrigeration；When temperature of charge is relatively low, using single cooling
Chuck is relatively low to its cooling effectiveness, and multiple cooling jackets among aforesaid reaction vessel kettle can then sequentially turn on cooling agent, and then
So that material can keep uniform cooldown rate in real time in front and rear cooling procedure in reactor kettle.It is above-mentioned to be based on cooldown rate
The HMDS preparation of control can be by cooling down with reactor for material in reactor kettle before and after cooling stage
The Uniform Control of speed, so that its overall cooling effect is improved, and carried HMDS finished product accuracy
It is high.
Brief description of the drawings
Fig. 1 is the utility model schematic diagram；
Fig. 2 is the utility model middle and upper part cooling jacket schematic diagram；
Fig. 3 is the utility model middle and lower part cooling jacket schematic diagram；
Reference numerals list：
1-reactor kettle, 2-cooling jacket, 3-cooling pipe, 301-top cooling jacket, the cooling of 302-bottom
Chuck, 4-cryogen tank, 5-magnetic valve.
Embodiment
With reference to the accompanying drawings and detailed description, the utility model is furtherd elucidate, it should be understood that following specific embodiment parties
Formula is merely to illustrate the utility model rather than limitation the scope of the utility model.It should be noted that make below in description
Word "front", "rear", "left", "right", "up" and "down" refer to the direction in accompanying drawing, and word " interior " and " outer " refer to respectively
Be directed towards or the direction away from particular elements geometric centers.
Embodiment 1
A kind of HMDS preparation reactor based on cooldown rate control as shown in Figure 1, it includes
Reactor kettle 1；Multiple cooling folders extended in the horizontal direction are provided between the outer wall and inwall of the reactor kettle 1
Set 2, multiple in the vertical directions of cooling jacket 2 are sequentially distributed, and each cooling jacket 2 is conducted to by cooling pipe 3 respectively
It is arranged among the cryogen tank 4 outside reactor kettle 1, magnetic valve 5 is provided with inside each cooling pipe 3.
As a kind of improvement of the present utility model, at least four is provided between the inwall and outer wall of the reactor kettle 1
Cooling jacket 3.Using above-mentioned technical proposal, it can be configured so that reactor kettle top with by multiple cooling jackets
Portion obtain and cooling treatment.
Using the HMDS preparation reactor based on cooldown rate control of above-mentioned technical proposal, it can lead to
Cross and be arranged on multiple cooling jackets inside reactor kettle to realize for reactor kettle materials inside step by step at cooling
Reason；When reactor kettle materials inside is under temperature higher state, it only turns on cooling agent inside single cooling jacket, and then
Cooling treatment step by step is able on the premise of avoiding material from being able to quick refrigeration；When temperature of charge is relatively low, using single cooling
Chuck is relatively low to its cooling effectiveness, and multiple cooling jackets among aforesaid reaction vessel kettle can then sequentially turn on cooling agent, and then
So that material can keep uniform cooldown rate in real time in front and rear cooling procedure in reactor kettle.It is above-mentioned to be based on cooldown rate
The HMDS preparation of control can be by cooling down with reactor for material in reactor kettle before and after cooling stage
The Uniform Control of speed, so that its overall cooling effect is improved, and carried HMDS finished product accuracy
It is high.
Embodiment 2
As it is of the present utility model it is a kind of improve, as shown in Figure 1, Figure 2 with shown in Fig. 3, the cooling jacket 2 includes on multiple
Portion's cooling jacket 201 and multiple bottom cooling jackets 202, multiple bottom cooling jackets 202 are set in turn in top cooling folder
The lower section of set 201；The top cooling jacket 201 uses loop configuration, and the bottom cooling jacket 202 is using in the horizontal direction
The ripple struction of extension.Using above-mentioned technical proposal, it may be such that cools off agent using the top cooling jacket of loop configuration
Fast Filling, and then achieve quick cooling treatment；Meanwhile using the bottom cooling jacket of ripple struction its can be made relative
It is improved in the contact area of reactor inner wall of kettle, and then makes it high for being realized positioned at the material of reactor autoclave body bottom
The cooling treatment of effect, cause the cooling of the overall material in reactor kettle to spend and be improved.
The remaining features and advantages of the present embodiment are same as Example 1.
Embodiment 3
As it is of the present utility model it is a kind of improve, each cooling jacket 2 is respectively connected with two cooling pipes 3, its on
The axis of reactor kettle 1 is into symmetrically；Each cooling pipe 3 is tilted towards by the link position of itself and cooling jacket 2
Upper extension.Using above-mentioned technical proposal, it can be quick and uniform by the cooling agent that is configured so that of multiple cooling pipes
Among filling to cooling jacket, its cooling effectiveness is caused to be improved；At the same time, the direction of cooling pipe sets and then may be such that
Quickly circulated when coolant flow is to cooling jacket inside, further to improve its cooling effectiveness.
The remaining features and advantages of the present embodiment are same as Example 2.
Claims (4)
1. a kind of HMDS preparation reactor based on cooldown rate control, it includes reactor kettle；Its
It is characterised by, multiple cooling jackets extended in the horizontal direction is provided between the outer wall and inwall of the reactor kettle,
Multiple cooling jacket in the vertical directions are sequentially distributed, and each cooling jacket is conducted to by cooling pipe respectively to be arranged on instead
Among answering the cryogen tank outside kettle kettle, magnetic valve is provided with inside each cooling pipe.
2. according to the HMDS preparation reactor based on cooldown rate control described in claim 1, its feature
It is, at least four cooling jacket is provided between the inwall and outer wall of the reactor kettle.
3. according to the HMDS preparation reactor based on cooldown rate control described in claim 1 or 2, it is special
Sign is that the cooling jacket includes multiple top cooling jackets and multiple bottom cooling jackets, multiple bottom cooling folders
Set is set in turn in below the cooling jacket of top；The top cooling jacket uses loop configuration, and the bottom cooling jacket is adopted
With the ripple struction extended in the horizontal direction.
4. according to the HMDS preparation reactor based on cooldown rate control described in claim 1 or 2, it is special
Sign is that each cooling jacket is respectively connected with two cooling pipes, its on reactor kettle axis into rotational symmetry；Often
One cooling pipe tilts upward extension by the link position of itself and cooling jacket.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720231875.1U CN206631595U (en) | 2017-03-10 | 2017-03-10 | HMDS preparation reactor based on cooldown rate control |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720231875.1U CN206631595U (en) | 2017-03-10 | 2017-03-10 | HMDS preparation reactor based on cooldown rate control |
Publications (1)
| Publication Number | Publication Date |
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| CN206631595U true CN206631595U (en) | 2017-11-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CN201720231875.1U Active CN206631595U (en) | 2017-03-10 | 2017-03-10 | HMDS preparation reactor based on cooldown rate control |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109751834A (en) * | 2019-02-28 | 2019-05-14 | 南通中集安瑞科食品装备有限公司 | Jacket type storage tank |
-
2017
- 2017-03-10 CN CN201720231875.1U patent/CN206631595U/en active Active
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN109751834A (en) * | 2019-02-28 | 2019-05-14 | 南通中集安瑞科食品装备有限公司 | Jacket type storage tank |
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