CN206627410U - Coal body permeability test device under hot cold shock - Google Patents

Coal body permeability test device under hot cold shock Download PDF

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Publication number
CN206627410U
CN206627410U CN201720427889.0U CN201720427889U CN206627410U CN 206627410 U CN206627410 U CN 206627410U CN 201720427889 U CN201720427889 U CN 201720427889U CN 206627410 U CN206627410 U CN 206627410U
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China
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pipe
cold
heat
end cap
hot
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CN201720427889.0U
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Chinese (zh)
Inventor
王登科
孙刘涛
刘淑敏
吕瑞环
李文睿
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Henan University of Technology
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Henan University of Technology
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Abstract

The utility model discloses coal body permeability test device under a kind of hot cold shock, including hot device for cooling, permeability apparatus, gas flow testing device and gas supply device.Hot device for cooling, which includes liquid nitrogen container, hot-air blower, the cold pipe of note and heat injection pipe, gas flow testing device, includes blast pipe, the second stop valve and gas flow meter;Permeability apparatus includes filling in coal sample tank, end cap, the cold pipe of heat, plectane and end cap, and gas supply device includes high pressure gas gas cylinder, airway tube, pressure-reducing valve and air gauge.The utility model can be realized to the anti-reflection of coal body by the cold alternate means of heat, and measures the permeability size for destroying coal body, so as to quantitatively illustrate the antireflective effect of the fracturing technique.Carry out antireflective effect of the analysis temperature impact to coal body using the permeability of coal body, obtain optimal temperature shock parameter, improve the efficiency of colliery operation.

Description

Coal body permeability test device under hot cold shock
Technical field
It the utility model is related to coal-mining technique field, more particularly to a kind of coal body permeability test device and method of testing.
Background technology
CBM Fracturing is the core and key that cbm development utilizes.In recent years, coal bed fracturing technically has very Much progress, ideal effect is being obtained using upper, but also exposing some problems, it would be highly desirable to solved, it is necessary to use nonconventional approaches(Heat Cold shock)Solve the technical barrier and bottleneck of cbm development, really realize the effect of increasing production of coal bed gas.In order to study temperature punching The pressure break effect to coal body is hit, researcher devises many devices, but rarely has the device of quantitative test coal mass fracture effect, lacks The permeability testing experimental system of coal under few hot cold shock.
Utility model content
The purpose of this utility model is solve weak point of the prior art, there is provided one kind can pass through the cold alternating of heat Means, realize to the anti-reflection of coal body, and measure destroy coal body permeability size hot cold shock under coal body permeability test Experimental provision.
To achieve the above object, under hot cold shock of the present utility model coal body permeability test device include hot device for cooling, Permeability apparatus, gas flow testing device and gas supply device;
Hot device for cooling, which includes liquid nitrogen container, hot-air blower, the cold pipe of note and heat injection pipe, hot-air blower, has fan switch;Liquid nitrogen The tank connection cold pipe of note, notes the one end that cold pipe is connected with liquid nitrogen container and is provided with pressure charging valve and liquid feed valve;Hot-air blower connects The heat injection pipe, heat injection pipe are provided with the first stop valve;
Gas flow testing device includes blast pipe, and blast pipe is provided with the second stop valve and gas flow meter;
Permeability apparatus includes filling in coal sample tank, end cap, the cold pipe of heat, plectane and end cap, and the lower end of the cold pipe of heat is solid vertically downward It is scheduled at the center of plectane, part of the plectane positioned at the cold caliber of heat laterally is evenly arranged with permeable hole penetrating up and down;End Lid coordinates with the sealing of coal sample tank top, is provided with the support level of annular in coal sample tank in side wall and bottom wall joint, and plectane is set up It is connected on support level and with the madial wall of coal sample tank;Plectane surrounds permeable chamber with coal sample tank bottom wall below, permeable Chamber side wall is connected with air water discharge pipe, and the part that air water discharge pipe stretches out permeable chamber has connected up the blast pipe and connected downwards Drainpipe is connected to, drainpipe is provided with the 3rd stop valve;The bottom of plug is provided with up big and down small prismoid section in end cap, and prismoid section is inserted Enter the cold pipe crimping sealing of the cold Guan Bingyu heat of heat;
Heat injection pipe and the cold pipe of note, which are each passed through, to be filled in and stretches into end cap in the cold pipe of heat, in heat injection pipe and the cold Guan Junyu end caps of note Plug sealing coordinates;The pipeline section side wall of heat injection pipe and the cold pipe of note in the cold pipe of heat is uniformly provided with radial direction through hole respectively;Filled in end cap On communicating pipe for discharging nitrogen and hot blast is vertically installed, communicating pipe bottom stretch into hot cold pipe and the upward external part in its top Filled in lid;
Gas supply device includes high pressure gas gas cylinder, is switched at the top of high pressure gas gas cylinder by gas outlet and is connected with air guide Pipe, airway tube are provided with pressure-reducing valve and air gauge.
The end cap is coordinated with coal sample tank top by following sealing structure:
The cylindrical place of end cap is convexly equipped with downwards connection annulus, and connection annulus bottom surface is provided with annular groove, coal sample tank top outer wall footpath To the raised connecting plate for being provided with annular, connecting plate and it is connected the underrun bolt of annulus and is detachably fixed and link together, company Coal sample pot sidewall more than fishplate bar is connected in annular groove, and pressure is provided with close between the side wall top of coal sample tank and the cell wall of annular groove Seal washer;Sealing ring is less than end cap lower surface, and inlet chamber is surrounded between end cap lower surface and coal sample upper end.
The airway tube is provided with the 4th stop valve.
The utility model has the following advantages:
The utility model can be realized to the anti-reflection of coal body, and measure and destroy oozing for coal body by the cold alternate means of heat Saturating rate size, so as to quantitatively illustrate the antireflective effect of the fracturing technique.
After the permeability that coal body is calculated by apparatus and method of the present utility model, it can be come using the permeability of coal body Assay temperature shock obtains optimal temperature shock parameter by experiment, carried for colliery operation to the antireflective effect of coal body For instructing, the efficiency of colliery operation is improved.
In order to preferably accurately measure the permeability of coal body, the coal in coal sample tank is not from raw coal, but special coal Sample;Because the thermal conductivity factor of cement and coal is very close, transmission of the heat in coal body is influenceed less, so according to certain ratio By cement, coal dust and water mix, mixture dehydration solidification dry after can approximation regard coal as, in case experiment.Mixture solidifies During caused water flowed down by the permeable hole on plectane, discharged by drainpipe.If being not added with cement, and coal is used only Powder, then it is difficult to prepare the integral coal sample of solidification, it is difficult to go out the coal body of underground solidification in laboratory simulation, so as to be difficult to Permeability is tested.
The utility model proposes a kind of preparation method for simulating coal sample, is highly convenient for laboratory use, for oozing for coal body Saturating rate experiment provides basis.
Seal washer in the utility model plays sealing function, and plug can block the cold pipe of heat in end cap, thereby ensure that After methane gas in airway tube enters inlet chamber, coal body can only be penetrated into by coal column upper surface, and from coal column lower surface Plectane flows out, and is discharged by blast pipe and digital display gas flowmeter.The utility model solves the seepage flow of Gas seepage well Approach, it is ensured that methane gas can only be flowed out by coal sample, so as to provide basis for the accurate coal sample permeability that calculates.
Plug is inserted with communicating pipe in end cap of the present utility model, the nitrogen vaporized in the cold pipe of heat can be quickly discharged into environment sky In gas, avoid the cold intraductal pressure of heat excessive and flow backwards liquid nitrogen, so as to ensure the lasting supply of liquid nitrogen, realize to around the cold pipe of heat The cold shock of coal body;Certainly, communicating pipe can also discharge hot blast in time, ensure that hot blast can be without interruption.In addition, this practicality New structure is simple, is easily installed and uses.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the schematic top plan view of plectane in Fig. 1;
Fig. 3 is the enlarged drawing at A in Fig. 1;
Fig. 4 is the enlarged drawing at B in Fig. 1.
Embodiment
As shown in Figure 1, Figure 2, Figure 3 and Figure 4, coal body permeability test device includes heat under hot cold shock of the present utility model Device for cooling, permeability apparatus, gas flow testing device and gas supply device;
Hot device for cooling, which includes liquid nitrogen container 1, hot-air blower 5, the cold pipe 4 of note and heat injection pipe 9, hot-air blower 5, has fan switch 6;Liquid nitrogen container 1 connects the cold pipe 4 of note, notes the one end that cold pipe 4 is connected with liquid nitrogen container 1 and is provided with pressure charging valve 2 and liquid feed valve 3; Hot-air blower 5 connects the heat injection pipe 9, and heat injection pipe 9 is provided with the first stop valve 8;
Gas flow testing device includes blast pipe 21, and blast pipe 21 is provided with the second stop valve 22 and digital display gas flow Meter 23, for measuring the flow of gas in real time.
Permeability apparatus includes coal sample tank 14, end cap 10, the cold pipe 15 of heat, plug 13 in plectane 16 and end cap, under the cold pipe 15 of heat End is fixed at the center of plectane 16 vertically downward, and plectane 16 is evenly arranged with positioned at the part of the cold radial outside of pipe 15 of heat Under penetrating permeable hole 51;Plectane 16 is not provided with permeable hole positioned at the part of the cold radially inner side of pipe 15 of heat, so as to close heat The bottom of cold pipe 15;
End cap 10 coordinates with the sealing of the top of coal sample tank 14, is provided with the branch of annular in coal sample tank 14 in side wall and bottom wall joint Step 52 is supportted, plectane 16 is erected on support level 52 and is connected with the madial wall of coal sample tank 14;Plectane 16 with below The bottom wall of coal sample tank 14 surrounds permeable chamber 53, and the permeable side wall of chamber 53 is connected with air water discharge pipe 18, and air water discharge pipe 18 stretches out permeable The part of chamber 53 has connected up the blast pipe 21 and has been connected with drainpipe 59 downwards, and drainpipe 59 is provided with the 3rd stop valve 20;The bottom of plug 13 is provided with up big and down small prismoid section 54 in end cap, and prismoid section 54 is inserted the cold pipe 15 of heat and pressed with the cold pipe 15 of heat Connect sealing;
Heat injection pipe 9 and the cold pipe 4 of note are each passed through plug 13 in end cap and stretched into the cold pipe 15 of heat, and heat injection pipe 9 and the cold pipe 4 of note are equal Coordinate with the sealing of plug 13 in end cap;The pipeline section side wall of heat injection pipe 9 and the cold pipe 4 of note in the cold pipe 15 of heat is uniformly provided with radially respectively Through hole;Setting radial direction through hole is routine techniques with space in communicating pipe and the pipe external space on tube wall, and the not shown radial direction is led to Hole.Communicating pipe 24 for discharging nitrogen and hot blast is vertically installed on plug 13 in end cap, communicating pipe 24 bottom stretch into the cold pipe of heat 15 and its top stretch out plug 13 in end cap upwards;
Gas supply device includes high pressure gas gas cylinder 30, and the top of high pressure gas gas cylinder 30 passes through the connection of gas outlet switch 29 There is airway tube 25, airway tube 25 is provided with pressure-reducing valve 28 and air gauge 27, and methane gas is supplied for permeability apparatus.
The end cap 10 is coordinated with the top of coal sample tank 14 by following sealing structure:
10 cylindrical place of end cap is convexly equipped with downwards connection annulus 55, and connection annulus 55 bottom surface is provided with annular groove 56, coal sample tank 14 Top exterior walls radial protrusion is provided with the connecting plate 57 of annular, and connecting plate 57 and the underrun bolt 12 for being connected annulus 55 are detachable It is fixed together, the side wall of coal sample tank 14 of connecting plate more than 57 is connected in annular groove 56, the side wall top of coal sample tank 14 Pressure is provided with seal washer 11 between the cell wall of annular groove 56;The structure that this sealing coordinates is very firm, seal degree it is high and It is easily installed and dismantles.Sealing ring 11 is less than the lower surface of end cap 10, surrounded between the lower surface of end cap 10 and the top of coal sample tank 14 into Air cavity 58.
The airway tube 25 is provided with the 4th stop valve 26, after test job is completed, simultaneously closes off gas outlet switch 29 With the 4th stop valve 26, can prevent at the gas backflow containing small coal particle to air gauge 27 and at pressure-reducing valve 28, so as to Protect air gauge 27 at and pressure-reducing valve 28.
Wherein, the material of coal sample tank 14 is aluminium alloy, and the material of the cold pipe 15 of heat preferably uses 304 stainless steels.Filled in end cap 13 materials used is polytetrafluoroethylene (PTFE).
The invention also discloses surveyed using the coal body permeability of coal body permeability test device under above-mentioned hot cold shock Method for testing, carry out according to the following steps successively:
First step is to prepare coal sample 17;Coal sample 17 is made up of the raw material of following weight:10~30 parts of cement, coal 60~90 parts of powder, add suitable quantity of water to be poured into after being mixed evenly on the plectane 16 in coal sample tank 14, make the height and coal of compound The top of sample tank 14 is flush, and then stands until compound solidifies;
In compound process of setting, the water in compound flows downwardly to permeable chamber 53 through the permeable hole 51 of plectane 16;Beat The 3rd stop valve 20 is opened, closes the second stop valve 22, water is discharged by drainpipe 59;Formation after compound dehydration solidification is dried Rationality matter and the close coal sample 17 of coal, in case carrying out permeability test.After coal sample 17 prepares, by end cap 10 by bolt 12 with Coal sample tank 14 is secured together, while notes cold pipe 4 and heat injection pipe 9 through the cold pipe 15 of the insertion of plug 13 heat in end cap;
Second step is that temperature shock is carried out to coal sample 17, including thermal shock and cold shock;
It is thermal shock first, opens the fan switch 6 on hot-air blower 5, fan switch 6 has regulation temperature control panel 7, will The leaving air temp of hot-air blower 5 is adjusted to 300 ± 10 DEG C, while opens the first stop valve 8, and hot blast enters heat by heat injection pipe 9 In cold pipe 15, and the inwall of the cold pipe 15 of heat is uniformly blown to from the radial direction through hole of the side wall of heat injection pipe 9, the inwall of the cold pipe 15 of heat is by heat Conduct to coal sample 17;The duration of heat of hot-air blower 5 is adjusted according to test experiments requirement within 10-60 minutes;Close Hot blast is sent in the stop valve 8 of fan switch 6 and first, stopping;
Next to that cold shock, adjusts the pressure charging valve 2 on liquid nitrogen container 1, liquid feed valve 3 is opened, liquid nitrogen enters rapidly by noting cold pipe 4 Enter in the cold pipe 15 of heat, the inner chamber of the cold pipe 15 of heat is uniformly sprayed onto from the radial direction through hole for noting the cold side wall of pipe 4, the cold pipe 15 of heat transmits cold To coal sample 17, coal sample 17 is cooled down rapidly;Liquid nitrogen gasifies in the cold pipe 15 of heat, and the nitrogen after gasification passes through the row of communicating pipe 24 Go out;After noting cold 30 minutes, liquid feed valve 3 is closed;
According to the requirement of test experiments, thermal shock and cold shock circulation are carried out 1-10 times, and preferable cycle-index is 1-3 Secondary, specific number is specifically determined by test experiments personnel, and thermal shock and cold shock produce hot cold shock effect, coal to coal sample 17 Body destroys damage, the increase of the permeability of coal sample 17;
Third step is the permeability for testing coal sample 17;Open the gas outlet switch 29 in high pressure gas gas cylinder 30, regulation Pressure-reducing valve 28, import gas pressure P1, P1 that record air gauge 27 is now shown unit are MPa;The 4th stop valve 26 is opened, Methane gas enters inlet chamber 58 by airway tube 25;Keep air-suction state more than 10 minutes, then open the second stop valve 22, methane gas enters the body of coal sample 17 by the upper surface of coal sample 17, is entered then down through the permeable hole 51 on plectane 16 In permeable chamber 53, methane gas is then flowed out by air water discharge pipe 18 and blast pipe 21, in the process on blast pipe 21 Digital display gas flowmeter 23 shows gas flow, and flow value Q, flow value Q are recorded after the registration of digital display gas flowmeter 23 is stable Unit be a cube meter per second;
Methane gas by coal sample 17, permeable hole 51, permeable chamber 53 enter blast pipe 21 after its pressures near atmospheric P0, P0 unit is MPa, and the height of coal sample 17 is H, and H unit is rice;Methane gas is coal sample 17 in the area of mobile section The area S, S of horizontal cross-section unit for square metre, methane gas viscosity coefficient is constant μ(The viscosity coefficient of gas with various is equal , can be by tabling look-up to obtain for constant), the permeability K of coal body 17 is:
After the permeability for calculating coal body, increasing of the assay temperature shock to coal body can be carried out using the permeability of coal body Saturating effect, optimal temperature shock parameter is obtained by experiment, is provided guidance for colliery operation, is improved the efficiency of colliery operation.
In the third step, after keeping air-suction state more than 10 minutes, before opening stop valve 22, pass through closing Whether the registration of the observation air gauge 27 of gas outlet switch 29 is stablized to examine air-tightness, if turned off 30 points after gas outlet switch 29 Clock, the registration fluctuation range of air gauge 27 are less than or equal to 0.01MPa, then judge that system air-tightness is good, now open second section Only valve 22 carries out subsequent operation;If the registration fluctuation range of air gauge 27 is more than 0.01MPa, stop experiment, inspection system Air-tightness, it is ensured that open the second stop valve 22 after system air-tightness is good again and carry out subsequent operation.
Above example is only to illustrative and not limiting the technical solution of the utility model, although with reference to above-described embodiment pair The utility model is described in detail, it will be understood by those within the art that:The utility model can still be entered Row modification or equivalent substitution, without departing from any modification or partial replacement of spirit and scope of the present utility model, it all should Cover among right of the present utility model.

Claims (3)

1. coal body permeability test device under hot cold shock, it is characterised in that:Including hot device for cooling, permeability apparatus, gas flow Test device and gas supply device;
Hot device for cooling, which includes liquid nitrogen container, hot-air blower, the cold pipe of note and heat injection pipe, hot-air blower, has fan switch;Liquid nitrogen container connects The cold pipe of note is connect, the one end that cold pipe is connected with liquid nitrogen container is noted and is provided with pressure charging valve and liquid feed valve;Described in hot-air blower connection Heat injection pipe, heat injection pipe are provided with the first stop valve;
Gas flow testing device includes blast pipe, and blast pipe is provided with the second stop valve and gas flow meter;
Permeability apparatus includes filling in coal sample tank, end cap, the cold pipe of heat, plectane and end cap, and the lower end of the cold pipe of heat is fixed on vertically downward At the center of plectane, part of the plectane positioned at the cold caliber of heat laterally is evenly arranged with permeable hole penetrating up and down;End cap with The sealing of coal sample tank top coordinates, and is provided with the support level of annular in coal sample tank in side wall and bottom wall joint, and plectane is erected at branch It is connected on support step and with the madial wall of coal sample tank;Plectane surrounds permeable chamber, permeable chamber side with coal sample tank bottom wall below Wall is connected with air water discharge pipe, and the part that air water discharge pipe stretches out permeable chamber has connected up the blast pipe and has been connected with downwards Drainpipe, drainpipe are provided with the 3rd stop valve;The bottom of plug is provided with up big and down small prismoid section, prismoid section insertion heat in end cap The cold cold pipe crimping sealing of Guan Bingyu heat;
Heat injection pipe and the cold pipe of note, which are each passed through, to be filled in and stretches into end cap in the cold pipe of heat, heat injection pipe and the cold Guan Junyu end caps Nei Saimi of note Envelope coordinates;The pipeline section side wall of heat injection pipe and the cold pipe of note in the cold pipe of heat is uniformly provided with radial direction through hole respectively;Erected beyond the Great Wall in end cap To the communicating pipe being provided with for discharging nitrogen and hot blast, communicating pipe bottom stretch into hot cold pipe and its top is stretched out in end cap upwards Plug;
Gas supply device includes high pressure gas gas cylinder, is switched at the top of high pressure gas gas cylinder by gas outlet and is connected with airway tube, Airway tube is provided with pressure-reducing valve and air gauge.
2. coal body permeability test device under hot cold shock according to claim 1, it is characterised in that:The end cap and coal Sample tank top is coordinated by following sealing structure:
The cylindrical place of end cap is convexly equipped with downwards connection annulus, and connection annulus bottom surface is provided with annular groove, coal sample tank top outer wall radial convex The connecting plate provided with annular is played, connecting plate is detachably fixed with being connected the underrun bolt of annulus and linked together, connecting plate Coal sample pot sidewall above is connected in annular groove, and pressure is provided with sealing gasket between the side wall top of coal sample tank and the cell wall of annular groove Circle;Sealing ring is less than end cap lower surface, and inlet chamber is surrounded between end cap lower surface and coal sample upper end.
3. coal body permeability test device under hot cold shock according to claim 1, it is characterised in that:On the airway tube Provided with the 4th stop valve.
CN201720427889.0U 2017-04-22 2017-04-22 Coal body permeability test device under hot cold shock Expired - Fee Related CN206627410U (en)

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Application Number Priority Date Filing Date Title
CN201720427889.0U CN206627410U (en) 2017-04-22 2017-04-22 Coal body permeability test device under hot cold shock

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Application Number Priority Date Filing Date Title
CN201720427889.0U CN206627410U (en) 2017-04-22 2017-04-22 Coal body permeability test device under hot cold shock

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108444882A (en) * 2018-01-17 2018-08-24 南方电网科学研究院有限责任公司 A kind of experiment porch for measuring deep-well exhaust efficiency

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN108444882A (en) * 2018-01-17 2018-08-24 南方电网科学研究院有限责任公司 A kind of experiment porch for measuring deep-well exhaust efficiency

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Granted publication date: 20171110