CN206511936U - High titanium slag chlorination reactor with adjustable swash plate - Google Patents

High titanium slag chlorination reactor with adjustable swash plate Download PDF

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Publication number
CN206511936U
CN206511936U CN201720130995.2U CN201720130995U CN206511936U CN 206511936 U CN206511936 U CN 206511936U CN 201720130995 U CN201720130995 U CN 201720130995U CN 206511936 U CN206511936 U CN 206511936U
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CN
China
Prior art keywords
swash plate
reactor
plate
reaction
chlorine
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720130995.2U
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Chinese (zh)
Inventor
吴伟
熊燕玲
吴重言
吴静
陆静
吴言富
徐其文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
KESHENG GROUP CO Ltd JIANGSU PROV
JIANGSU KESHENG CROP TECHNOLOGY Co Ltd
Original Assignee
KESHENG GROUP CO Ltd JIANGSU PROV
JIANGSU KESHENG CROP TECHNOLOGY Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by KESHENG GROUP CO Ltd JIANGSU PROV, JIANGSU KESHENG CROP TECHNOLOGY Co Ltd filed Critical KESHENG GROUP CO Ltd JIANGSU PROV
Priority to CN201720130995.2U priority Critical patent/CN206511936U/en
Application granted granted Critical
Publication of CN206511936U publication Critical patent/CN206511936U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model discloses a kind of high titanium slag chlorination reactor with adjustable swash plate, the cross section of reactor shell is square, connection, swash plate low side is collected while being provided with breach with reactor shell inwall, the high-end one side of gas cover plate is provided with breach with reactor shell inwall, the high-end one side of gas cover plate is with collecting swash plate low side while being fixedly connected, reaction swash plate is connected while being rotated with the face inwall of reactor shell one jaggy, expansion link one end is with answering device inner walls to be connected, the expansion link other end is provided with roller, roller is contacted with reaction swash plate lower surface, interlayer is formed between gas cover plate and reaction swash plate, heater is provided with interlayer, reactor chlorine gas distribution plate is provided with interlayer, reactor chlorine gas distribution plate is connected with reactor chlorine pipeline;The high titanium slag chlorination reactor that the utility model carries adjustable swash plate can produce the pulverulent mixture of high titanium slag and petroleum coke and chlorine in hot environment efficient, uninterrupted, nonclogging chlorination reaction.

Description

High titanium slag chlorination reactor with adjustable swash plate
Technical field
The utility model belongs to chemical production equipment field, and particularly a kind of high titanium slag chlorination with adjustable swash plate is anti- Answer device.
Background technology
A particularly important link is during the rich titanium material production TiCl4, TiCl4 of chlorination is Ti industry in Ti industry Most important intermediate products, are chloridising production titanium dioxides, and hydro-thermal method produces the important intermediate products of nano barium phthalate.TiCl4 It can be obtained by fluidizing chlorination, fluidizing chlorination is also referred to as fluidization chlorination, be using chlorine as fluid and chlorinating agent, by high titanium slag and stone The compound of oil coke is under suspended state in fluidized bed furnace, and the process of chlorination reaction producing titanium tetrachloride t 5 bx is carried out at high temperature.
Domestic many enterprises all produce TiCl4, the residue and high boiling chlorine of chlorination reaction generation using boiling chloridizing furnace Compound is all fallen on the sieve plate of chlorination furnace, intermittently from chlorination furnace bottom deslagging, chlorine and high titanium valve shape mixture material chlorination Reaction is insufficient, causes part material to waste.
Utility model content
The technical problem that the utility model is solved is that a kind of quick, anti-blocking, raising reaction efficiency carry of offer can Adjust the high titanium slag chlorination reactor of swash plate.
The technical solution for realizing the utility model purpose is:A kind of high titanium slag chlorination reaction with adjustable swash plate Device, including collect swash plate, gas cover plate, reaction swash plate, expansion link, roller, heater, reactor shell, reactor chlorine Distribution grid, reactor chlorine pipeline, the cross section of the reactor shell is square, is collected in the side of swash plate three and reactor enclosure body Wall is sealedly and fixedly connected, and collects swash plate low side and is provided with breach between reactor shell inwall on one side, the side of gas cover plate three with it is anti- Answer device inner walls to be sealedly and fixedly connected, breach, gas lid are provided between the high-end one side of gas cover plate and reactor shell inwall The high-end one side of plate with collect swash plate low side on one side be fixedly connected, react swash plate while with the face inwall of reactor shell one jaggy Connection is rotated, expansion link one end is connected with reactor shell inwall, the expansion link other end is provided with roller, and roller is with reacting under swash plate Surface is contacted, and is wherein left gap between gas cover plate and reaction swash plate, is formed interlayer between gas cover plate and reaction swash plate, press from both sides It is provided with layer in heater, interlayer and is provided with reactor chlorine gas distribution plate, reactor chlorine gas distribution plate and reactor chlorine pipeline Connection.
Preferably, the expansion link is spiral expanding bar.
Preferably, the heater is Elema.
The utility model compared with prior art, its remarkable advantage:
(1)The high titanium slag chlorination reactor that the utility model carries adjustable swash plate will can partly not have in boiling chloridizing furnace There is the pulverulent mixture of reaction or without the pulverulent mixture chlorination reaction again that boiling is got up, improve raw material availability, save Cost.
(2)The utility model carry the reaction swash plate of the high titanium slag chlorination reactor of adjustable swash plate and horizontal plane angle compared with Small, so having can ensure that pulverulent mixture stops the enough reaction time on reaction swash plate, when the excessive heap of pulverulent mixture Product is when reacting on swash plate, and expansion link can adjust the angle of reaction swash plate and horizontal plane, pulverulent mixture is continued in reaction Flowed on swash plate, prevent from blocking.
The high titanium slag chlorination reactor for carrying adjustable swash plate to the utility model below in conjunction with the accompanying drawings makees further detailed Description.
Brief description of the drawings
Fig. 1 is the structural representation for the high titanium slag chlorination reactor that utility model carries adjustable swash plate.
Fig. 2 is the overlooking the structure diagram for the high titanium slag chlorination reactor that the utility model carries adjustable swash plate.
Embodiment
As Figure 1-Figure 2:
A kind of high titanium slag chlorination reactor with adjustable swash plate, including collect swash plate 1, gas cover plate 2, reaction swash plate 3rd, expansion link 4, roller 5, heater 6, reactor shell 7, reactor chlorine gas distribution plate 8, reactor chlorine pipeline 9, described The cross section of reactor shell 7 is square, collects the side of swash plate 1 three and is fixedly connected with the inner wall sealing of reactor shell 7, collects swash plate 1 low side is provided with breach between the inwall of reactor shell 7 on one side, and the side of gas cover plate 2 three is fixed with the inner wall sealing of reactor shell 7 Connection, is provided with breach between the high-end one side of gas cover plate 2 and the inwall of reactor shell 7, the high-end one side of gas cover plate 2 is oblique with collecting The low side of plate 1 is while be fixedly connected, and reaction one side of swash plate 3 rotates with the face inwall of reactor shell 7 one jaggy and is connected, expansion link 4 one end are connected with the inwall of reactor shell 7, and the other end of expansion link 4 is provided with roller 5, and roller 5 is contacted with the reaction lower surface of swash plate 3, Gap wherein is left between gas cover plate 2 and reaction swash plate 3, is formed between gas cover plate 2 and reaction swash plate 3 in interlayer, interlayer Provided with heater 6, reactor chlorine gas distribution plate 8, reactor chlorine gas distribution plate 8 and reactor chlorine pipeline 9 are provided with interlayer Connection.
Expansion link 4 is spiral expanding bar, is stretched in hot environment stable.
Heater 6 is Elema, and Elema heating effect is good, anticorrosive.
The utility model carries the operation principle of the high titanium slag chlorination reactor of adjustable swash plate:
High titanium slag chlorination reactor with adjustable swash plate is heated to 900 DEG C~1000 DEG C of temperature environment in Elema Under, high titanium slag(Mainly contain TiO2, Ti2O3, TiO, TiN, TiC, FeO, MnO2, MgO, CaO, SiO2, V2O5)With petroleum coke Mixing powder enters boiling chloridizing furnace progress chlorination reaction, the solid residue reacted, part unreacted according to a certain percentage Mixing powder and the mixing powder that gets up of not boiling be sent to gas cover plate 2 and reaction swash plate 3 by collecting swash plate 1 Into in interlayer, chlorine is full of by reactor chlorine gas distribution plate 8 in interlayer, unreacted pulverulent mixture produces chlorination with chlorine Reaction.When pulverulent mixture is excessively deposited on reaction swash plate 3, expansion link 4 can increase the folder of backslash plate 3 and horizontal plane Angle, makes pulverulent mixture continue, in the reaction surface flow of swash plate 3, to prevent from blocking.

Claims (3)

1. a kind of high titanium slag chlorination reactor with adjustable swash plate, it is characterised in that including collecting swash plate(1), gas lid Plate(2), reaction swash plate(3), expansion link(4), roller(5), heater(6), reactor shell(7), reactor chlorine distribution Plate(8), reactor chlorine pipeline(9), the reactor shell(7)Cross section to be square, collect swash plate(1)Three sides and reaction Device housing(7)Inner wall sealing is fixedly connected, and collects swash plate(1)Low side one side and reactor shell(7)Breach is provided between inwall, Gas cover plate(2)Three sides and reactor shell(7)Inner wall sealing is fixedly connected, gas cover plate(2)High-end one side and reactor enclosure Body(7)Breach, gas cover plate are provided between inwall(2)High-end one side is with collecting swash plate(1)Low side is while be fixedly connected, and reaction is oblique Plate(3)While with reactor shell jaggy(7)One face inwall rotates connection, expansion link(4)One end and reactor shell(7) Inwall is connected, expansion link(4)The other end is provided with roller(5), roller(5)With reaction swash plate(3)Lower surface is contacted, wherein gas lid Plate(2)With reaction swash plate(3)Between leave gap, gas cover plate(2)With reaction swash plate(3)Between formed and set in interlayer, interlayer There is heater(6), interlayer is interior to be provided with reactor chlorine gas distribution plate(8), reactor chlorine gas distribution plate(8)With reactor chlorine tube Road(9)Connection.
2. the high titanium slag chlorination reactor according to claim 1 with adjustable swash plate, it is characterised in that described flexible Bar(4)For spiral expanding bar.
3. the high titanium slag chlorination reactor according to claim 1 with adjustable swash plate, it is characterised in that the heating Device(6)For Elema.
CN201720130995.2U 2017-02-14 2017-02-14 High titanium slag chlorination reactor with adjustable swash plate Expired - Fee Related CN206511936U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720130995.2U CN206511936U (en) 2017-02-14 2017-02-14 High titanium slag chlorination reactor with adjustable swash plate

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720130995.2U CN206511936U (en) 2017-02-14 2017-02-14 High titanium slag chlorination reactor with adjustable swash plate

Publications (1)

Publication Number Publication Date
CN206511936U true CN206511936U (en) 2017-09-22

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113932614A (en) * 2021-10-31 2022-01-14 龙佰禄丰钛业有限公司 Chlorination furnace gas inlet system and control method

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN113932614A (en) * 2021-10-31 2022-01-14 龙佰禄丰钛业有限公司 Chlorination furnace gas inlet system and control method

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CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170922

Termination date: 20220214

CF01 Termination of patent right due to non-payment of annual fee