CN206511935U - Dish-shaped high titanium slag chlorination reactor - Google Patents
Dish-shaped high titanium slag chlorination reactor Download PDFInfo
- Publication number
- CN206511935U CN206511935U CN201720130993.3U CN201720130993U CN206511935U CN 206511935 U CN206511935 U CN 206511935U CN 201720130993 U CN201720130993 U CN 201720130993U CN 206511935 U CN206511935 U CN 206511935U
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- China
- Prior art keywords
- dish
- infundibulate
- gas hood
- heat insulation
- shaped
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Abstract
The utility model discloses a kind of dish-shaped high titanium slag chlorination reactor, including dish-shaped distributor, infundibulate gas hood, drive shaft, speed changer, motor, powder charging aperture, heat insulation bottom board, reactor shell, the dish-shaped distributor is made up of two cones, drive shaft is rotated with heat insulation bottom board and is connected, motor is connected by speed changer with the drive shaft other end, infundibulate gas hood is placed in above dish-shaped distributor, the conical surface of infundibulate gas hood and dish-shaped distributor leaves gap, powder charging aperture is suspended in the charging aperture of infundibulate gas hood, heat insulation bottom board is provided with waste outlet and chlorine air admission hole；Dish-shaped high titanium slag chlorination reactor of the present utility model can produce the pulverulent mixture of high titanium slag and petroleum coke and chlorine in hot environment efficient, uninterrupted, nonclogging chlorination reaction.
Description
Technical field
The utility model belongs to chemical production equipment field, particularly a kind of dish-shaped high titanium slag chlorination reactor.
Background technology
A particularly important link is during the rich titanium material production TiCl4, TiCl4 of chlorination is Ti industry in Ti industry
Most important intermediate products, are chloridising production titanium dioxides, and hydro-thermal method produces the important intermediate products of nano barium phthalate.TiCl4
It can be obtained by fluidizing chlorination, fluidizing chlorination is also referred to as fluidization chlorination, be using chlorine as fluid and chlorinating agent, by high titanium slag and stone
The compound of oil coke is under suspended state in fluidized bed furnace, and the process of chlorination reaction producing titanium tetrachloride t 5 bx is carried out at high temperature.
Domestic many enterprises all produce TiCl4, the residue and high boiling chlorine of chlorination reaction generation using boiling chloridizing furnace
Compound is all fallen on the sieve plate of chlorination furnace, intermittently from chlorination furnace bottom deslagging, chlorine and high titanium valve shape mixture material chlorination
Reaction is insufficient, causes part material to waste.
Utility model content
The technical problem that the utility model is solved is to provide a kind of dish height that is quick, anti-blocking, improving reaction efficiency
Titanium slag chlorination reactor.
The technical solution for realizing the utility model purpose is：A kind of dish-shaped high titanium slag chlorination reactor, including dish
Distributor, infundibulate gas hood, drive shaft, speed changer, motor, infundibulate collector, heat insulation bottom board, reactor shell,
The dish-shaped distributor is made up of two cones, and two cone base diameters are identical, and two cone bottoms are fixedly connected,
Dish-shaped distributor bottom is fixedly connected with drive shaft one end, and heat insulation bottom board is fixedly connected with the inwall of reactor shell, transmission
Rotating shaft is rotated with heat insulation bottom board and is connected, and motor is fixed in reactor shell, and motor is turned by speed changer with transmission
The axle other end is connected, and infundibulate gas hood is placed in above dish-shaped distributor, and the inwall of infundibulate gas hood edge and reactor shell is consolidated
Surely it is tightly connected, the conical surface of infundibulate gas hood and dish-shaped distributor leaves gap, infundibulate collector edge and reactor shell
Inwall fixed seal connection, the wherein charging aperture of infundibulate gas hood is connected with the discharging opening of infundibulate collector, described heat-insulated
Bottom plate is provided with waste outlet and chlorine air admission hole.
Preferably, the heat insulation bottom board is set to a circle groove, and the crosscutting section of groove is that waste outlet is provided with V-arrangement, groove.
The utility model compared with prior art, its remarkable advantage：
（1）The utility model dish high titanium slag chlorination reactor can be by the responseless powdery in part in boiling chloridizing furnace
Mixture or without the pulverulent mixture chlorination reaction again that boiling is got up, improves raw material availability, saves cost.
（2）Between the infundibulate gas hood of the utility model dish high titanium slag chlorination reactor and the conical surface of dish-shaped distributor leave
Gap, forms narrow chlorine passage, high titanium slag is fully contacted with chlorine with petroleum coke pulverulent mixture, improves chlorination reaction effect
Rate.
（3）The utility model dish high titanium slag chlorination reactor is in order to have the time of abundance for pulverulent mixture and chlorine chlorine
Change reaction, the conical surface gradient inclination angle of dish-shaped distributor can not be too big, and domatic inclination angle is too small and pulverulent mixture can be caused to exist
Conical surface accumulation produces blocking, therefore dish-shaped distributor is rotated under motor with certain speed, can effectively prevent powdery from mixing
Compound is accumulated in the conical surface of dish-shaped distributor, eliminates and blocks.
（4）The heat insulation bottom board of the utility model dish high titanium slag chlorination reactor is set to a circle groove, and groove is easier to receive
Reactant is fixed after collection chlorination reaction, it is discharged from waste outlet.
The dish-shaped high titanium slag chlorination reactor of the utility model is described in further detail below in conjunction with the accompanying drawings.
Brief description of the drawings
Fig. 1 is the structural representation of the dish-shaped high titanium slag chlorination reactor of utility model.
Fig. 2 is the overlooking the structure diagram of the dish-shaped high titanium slag chlorination reactor of the utility model.
Embodiment
As Figure 1-Figure 2：
A kind of dish-shaped high titanium slag chlorination reactor, it is characterised in that including dish-shaped distributor 1, infundibulate gas hood 2, transmission
Rotating shaft 3, speed changer 4, motor 5, infundibulate collector 6, heat insulation bottom board 7, reactor shell 8, the dish-shaped distributor 1 by
Two cone compositions, two cone base diameters are identical, and two cone bottoms are fixedly connected, the dish-shaped bottom of distributor 1
Be fixedly connected with the one end of drive shaft 3, heat insulation bottom board 7 is fixedly connected with the inwall of reactor shell 8, drive shaft 3 with it is heat-insulated
Bottom plate 7 rotates connection, and motor 5 is fixed in reactor shell 8, and motor 5 is another by speed changer 4 and drive shaft 3
One end is connected, and infundibulate gas hood 2 is placed in the dish-shaped top of distributor 1, and the edge of infundibulate gas hood 2 and the inwall of reactor shell 8 are consolidated
Surely it is tightly connected, the conical surface of infundibulate gas hood 2 and dish-shaped distributor 1 leaves gap, the edge of infundibulate collector 6 and reactor enclosure
The inwall fixed seal connection of body 8, the wherein charging aperture of infundibulate gas hood 2 are connected with the discharging opening of infundibulate collector 6, described
Heat insulation bottom board 7 is provided with waste outlet 71 and chlorine air admission hole 72.
Heat insulation bottom board 7 is set to a circle groove, and the crosscutting section of groove is that waste outlet 71 is provided with V-arrangement, groove, and groove more holds
Reactant is fixed after easily collecting chlorination reaction, it is discharged from waste outlet.
The operation principle of the utility model dish high titanium slag chlorination reactor：
Dish-shaped high titanium slag chlorination reactor is under 900 DEG C~1000 DEG C of temperature environment, high titanium slag（Mainly contain TiO2,
Ti2O3, TiO, TiN, TiC, FeO, MnO2, MgO, CaO, SiO2, V2O5）Powder is mixed according to a certain percentage with petroleum coke to enter
Enter boiling chloridizing furnace and carry out chlorination reaction, the solid residue reacted, the unreacted mixing powder in part and not boiling
Mixing powder be uniformly sprinkling upon on the conical surface of dish-shaped distributor 1, chlorine from chlorine air admission hole 72 enter infundibulate gas hood 2 with
Gap between dish-shaped distributor 1, chlorine produces chlorination reaction with the unreacted powdery thing that mixes, and reacts the TiCl4 gas produced
The charging aperture of body from infundibulate gas hood 2 is discharged for next step production, waste outlet of the remaining reaction residues from heat insulation bottom board 7
71 discharges；Dish-shaped distributor 1 is rotated under the driving of motor 5 with certain speed simultaneously, prevents that mixing powder accumulation is stifled
Plug.
Claims (2)
1. a kind of dish-shaped high titanium slag chlorination reactor, it is characterised in that including dish-shaped distributor（1）, infundibulate gas hood（2）, pass
Dynamic rotating shaft（3）, speed changer（4）, motor（5）, infundibulate collector（6）, heat insulation bottom board（7）, reactor shell（8）, institute
State dish-shaped distributor（1）It is made up of two cones, two cone base diameters are identical, two cone bottoms, which are fixed, to be connected
Connect, dish-shaped distributor（1）Bottom and drive shaft（3）One end is fixedly connected, heat insulation bottom board（7）With reactor shell（8）It is interior
Wall is fixedly connected, drive shaft（3）With heat insulation bottom board（7）Rotate connection, motor（5）It is fixed on reactor shell（8）On,
Motor（5）Pass through speed changer（4）With drive shaft（3）The other end is connected, infundibulate gas hood（2）It is placed in dish-shaped distributor
（1）Top, infundibulate gas hood（2）Edge and reactor shell（8）Inwall fixed seal connection, infundibulate gas hood（2）With dish
Shape distributor（1）The conical surface leave gap, infundibulate collector（6）Edge and reactor shell（8）Inwall fixing seal connect
Connect, wherein infundibulate gas hood（2）Charging aperture and infundibulate collector（6）Discharging opening connection, the heat insulation bottom board（7）It is provided with
Waste outlet（71）With chlorine air admission hole（72）.
2. dish-shaped high titanium slag chlorination reactor according to claim 1, it is characterised in that the heat insulation bottom board（7）It is set to
One circle groove, the crosscutting section of groove is that waste outlet is provided with V-arrangement, groove（71）.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720130993.3U CN206511935U (en) | 2017-02-14 | 2017-02-14 | Dish-shaped high titanium slag chlorination reactor |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720130993.3U CN206511935U (en) | 2017-02-14 | 2017-02-14 | Dish-shaped high titanium slag chlorination reactor |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206511935U true CN206511935U (en) | 2017-09-22 |
Family
ID=59867614
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720130993.3U Expired - Fee Related CN206511935U (en) | 2017-02-14 | 2017-02-14 | Dish-shaped high titanium slag chlorination reactor |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206511935U (en) |
-
2017
- 2017-02-14 CN CN201720130993.3U patent/CN206511935U/en not_active Expired - Fee Related
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170922 Termination date: 20220214 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |