CN206474122U - A kind of device for being used to reclaim DMF gases - Google Patents

A kind of device for being used to reclaim DMF gases Download PDF

Info

Publication number
CN206474122U
CN206474122U CN201720171103.3U CN201720171103U CN206474122U CN 206474122 U CN206474122 U CN 206474122U CN 201720171103 U CN201720171103 U CN 201720171103U CN 206474122 U CN206474122 U CN 206474122U
Authority
CN
China
Prior art keywords
dmf
gases
recycling
gas extraction
gas
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720171103.3U
Other languages
Chinese (zh)
Inventor
邢政国
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Weifang Hao Hai New Material Co Ltd
Original Assignee
Weifang Hao Hai New Material Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Weifang Hao Hai New Material Co Ltd filed Critical Weifang Hao Hai New Material Co Ltd
Priority to CN201720171103.3U priority Critical patent/CN206474122U/en
Application granted granted Critical
Publication of CN206474122U publication Critical patent/CN206474122U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Separation, Recovery Or Treatment Of Waste Materials Containing Plastics (AREA)
  • Processing And Handling Of Plastics And Other Materials For Molding In General (AREA)
  • Manufacture Of Porous Articles, And Recovery And Treatment Of Waste Products (AREA)

Abstract

The utility model discloses a kind of device for being used to reclaim DMF gases, belong to polyurethane resin production equipment technical field, including reactor, side at the top of the reactor is provided with gas extraction mouth, the gas extraction mouth is communicated with gas extraction pipeline, the other end of the gas extraction pipeline is communicated with air-introduced machine, and the port of export of the air-introduced machine is communicated with recycling can by gas recovery conduit;The first water condenser is provided with the gas recovery conduit, the recycling can upper end is provided with the second water condenser, the gaseous phase outlet and atmosphere of second water condenser.The utility model by the DMF gases that reaction is not involved in kettle by drawing reactor, liquid is condensed into using water condenser to be stored, the recycling to DMF gases can be achieved, has the advantages that simple in construction, easy to operate and production process is safe, small to personnel and environmental hazard.

Description

A kind of device for being used to reclaim DMF gases
Technical field
The utility model is related to polyurethane resin production equipment technical field, and in particular to one kind is used to reclaim DMF gases Device.
Background technology
When at present, using reactor synthesis of polyurethane naval stores, partial solvent DMF is had in kettle(N, N- dimethyl methyl Acid amides)Gas is evaporated from reaction mass, and the portion gas is difficult to continue to participate in reaction in kettle.In addition, anti-in synthesis Often opening kettle cover is needed to add corresponding additive according to production during answering, meanwhile, to ensure in product quality, production process Many sub-samplings are also needed, part DMF gases are had in the operating process from being evaporated in kettle and being directly discharged to air.At present The recycling and processing device to part DMF gases is there is no in workshop.If waste gas is without processing, it is directly released into air, meeting Severe contamination is caused to environment, personal injury is caused to producers, certain wasting of resources is also resulted in enterprise.
The content of the invention
For above technological deficiency, technical problem to be solved in the utility model is to provide a kind of for reclaiming DMF gas The device of body, the device is condensed into by the way that the DMF gases that reaction is not involved in kettle are drawn into reactor using water condenser Liquid is stored, and the recycling to DMF gases can be achieved, safe, right with simple in construction, easy to operate and production process Personnel and the small advantage of environmental hazard.
To solve above technical problem, the technical solution adopted in the utility model is:
A kind of side at the top of device for being used to reclaim DMF gases, including reactor, the reactor is provided with gas and adopted Outlet, the gas extraction mouth is communicated with gas extraction pipeline, and the other end of the gas extraction pipeline is communicated with air-introduced machine, institute The port of export for stating air-introduced machine is communicated with recycling can by gas recovery conduit;The first water cooling is provided with the gas recovery conduit Condenser, the recycling can upper end is provided with the second water condenser, the gaseous phase outlet and atmosphere of second water condenser.
As an improvement scheme, first water condenser is tubular heat exchanger.
As an improvement scheme, magnetic valve is provided between the gas extraction mouth and gas extraction pipeline.
As an improvement scheme, magnetic valve is provided between first water condenser and the recycling can.
Wherein, the reactor bottom is provided with discharging opening.
By adopting the above-described technical solution, the beneficial effects of the utility model are:
Due to a kind of device for being used to reclaim DMF gases that the utility model is provided, it is included at the top of reactor, reactor Side be provided with gas extraction mouth, gas extraction mouth be communicated with gas extraction pipeline, gas extraction pipeline the other end connection There is air-introduced machine, the port of export of air-introduced machine is communicated with recycling can by gas recovery conduit;First is provided with gas recovery conduit The DMF gases volatilized in polyurethane synthetic reaction process in reactor are led to water condensation by this structure of water condenser by pipeline At device, liquid is condensed into by introducing cooling water by DMF gases, is stored in standby in recycling can, the recovery profit to DMF is realized With, so that production cost is saved, drop low exhaust gas emission, it is ensured that the production environment of product.Recycling can upper end is provided with the second water cooling Condenser, the gaseous phase outlet and atmosphere of the second water condenser, this structure can ensure that the pressure in recycling can is maintained at normal pressure shape State, and further condensing reflux is carried out to the DMF that may be volatilized, it is ensured that the DMF qualified discharges in gaseous phase outlet, it is ensured that work Environment.
Brief description of the drawings
Fig. 1 is a kind of structural representation for being used to reclaim the device of DMF gases that the utility model is provided;
In figure:1. reactor, 2. discharging openings, 3. gases extraction mouth, 4. magnetic valves, 5. gases extraction pipeline, 6. air-introduced machines, 7. gas recovery conduit, 8. recycling cans, 9. first water condensers, 10. water inlets, 11. delivery ports, 12. second water condensers, 13. cooling water inlet, 14. cooling water outlets, 15. gaseous phase outlets.
Embodiment
With reference to the accompanying drawings and examples, the utility model is expanded on further.
As shown in figure 1, a kind of device for being used to reclaim DMF gases that the utility model is provided, including reactor 1, reaction The bottom of kettle 1 is provided with discharging opening 2, and the side at top is provided with gas extraction mouth 3, and gas extraction mouth 3 is communicated with by magnetic valve 4 Gas produces pipeline 5, and the other end of gas extraction pipeline 5 is communicated with air-introduced machine 6, and the port of export of air-introduced machine 6 is reclaimed by gas Pipeline 7 is communicated with recycling can 8;Magnetic valve 4 is provided between first water condenser 9 and recycling can 8.
As shown in figure 1, being provided with the first water condenser 9 on gas recovery conduit 7, the first water condenser 9 changes for shell and tube Hot device, its water inlet 10 and delivery port 11 are respectively arranged at below and top.
As shown in figure 1, the top of recycling can 8 is provided with the second water condenser 12, its cooling water inlet 13 and cooling water outlet 14 It is respectively arranged at below and top, gaseous phase outlet 15 and atmosphere.
As shown in figure 1, the utility model is by the DMF gases of volatilization lead in reactor 1 in polyurethane synthetic reaction process Piping is led at the first water condenser 9, is condensed into liquid by introducing cooling water by DMF gases, is stored in standby in recycling can 8 With, the recycling to DMF is realized, so that production cost is saved, drop low exhaust gas emission, it is ensured that the production environment of product.Simultaneously The gaseous phase outlet 13 of the second water condenser 12 and atmosphere that the upper end of recycling can 8 is set, make the pressure in recycling can be maintained at normal Pressure condition, and further condensing reflux is carried out to the DMF that may be volatilized, it is ensured that the DMF qualified discharges in gaseous phase outlet.
Embodiment described above is only that preferred embodiment of the present utility model is described, not to this practicality New spirit and scope are defined.Therefore, on the premise of the utility model setting design is not departed from, this area ordinary people The all variations and modifications that member makes to the technical solution of the utility model, all should drop into protection domain of the present utility model, The claimed technology contents of the utility model, have all been recorded in detail in the claims.

Claims (5)

1. a kind of device for being used to reclaim DMF gases, including reactor, it is characterised in that:Side at the top of the reactor is set Gas extraction mouth is equipped with, the gas extraction mouth is communicated with gas extraction pipeline, the other end connection of the gas extraction pipeline There is air-introduced machine, the port of export of the air-introduced machine is communicated with recycling can by gas recovery conduit;Set on the gas recovery conduit The first water condenser is equipped with, the recycling can upper end is provided with the second water condenser, the gaseous phase outlet of second water condenser With atmosphere.
2. a kind of device for being used to reclaim DMF gases according to claim 1, it is characterised in that:First water condensation Device is tubular heat exchanger.
3. a kind of device for being used to reclaim DMF gases according to claim 2, it is characterised in that:The gas produces mouth Magnetic valve is provided between gas extraction pipeline.
4. a kind of device for being used to reclaim DMF gases according to claim 3, it is characterised in that:First water condensation Magnetic valve is provided between device and the recycling can.
5. a kind of device for being used to reclaim DMF gases according to claim 4, it is characterised in that:The reactor bottom It is provided with discharging opening.
CN201720171103.3U 2017-02-24 2017-02-24 A kind of device for being used to reclaim DMF gases Expired - Fee Related CN206474122U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720171103.3U CN206474122U (en) 2017-02-24 2017-02-24 A kind of device for being used to reclaim DMF gases

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720171103.3U CN206474122U (en) 2017-02-24 2017-02-24 A kind of device for being used to reclaim DMF gases

Publications (1)

Publication Number Publication Date
CN206474122U true CN206474122U (en) 2017-09-08

Family

ID=59747160

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720171103.3U Expired - Fee Related CN206474122U (en) 2017-02-24 2017-02-24 A kind of device for being used to reclaim DMF gases

Country Status (1)

Country Link
CN (1) CN206474122U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111662203A (en) * 2020-05-25 2020-09-15 安徽金禾实业股份有限公司 Method and device for recycling heat energy of DMF (dimethyl formamide) rectification recovery device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN111662203A (en) * 2020-05-25 2020-09-15 安徽金禾实业股份有限公司 Method and device for recycling heat energy of DMF (dimethyl formamide) rectification recovery device
CN111662203B (en) * 2020-05-25 2023-03-03 安徽金禾实业股份有限公司 Method and device for recycling heat energy of DMF (dimethyl formamide) rectification recycling device

Similar Documents

Publication Publication Date Title
CN104748507B (en) Treatment system for recovering chemical plant waste gas containing ammonia into liquid ammonia and treatment method thereof
CN206474122U (en) A kind of device for being used to reclaim DMF gases
CN102764517B (en) Waste gas reclamation treatment system and recovery processing technique thereof during for chemicals entrucking
CN203678369U (en) Circulating cooling system of reaction kettle
CN108325285A (en) A kind of chemical industry equipment exhaust gas processing device of anti-leak
CN205391788U (en) Waste gas recovery heat transfer system
CN205505536U (en) Chemical production multitube spray cooling machine
CN203598663U (en) Hydrocarbon solution recovery system
CN202131087U (en) Device for recovering fluorine hydride from fluorinated raffinate
CN104689587A (en) Liquid ring type vacuum pump system for chlorinated benzene vacuum rectification
CN204159067U (en) Chemical solvent gas concentration unit in discharging waste gas
CN207385424U (en) Automatic control structure raw material decomposes device
CN205925677U (en) Acylation reaction device
CN208898682U (en) A kind of circulating water for gasification high-efficiency comprehensive utilization controlling device
CN205616575U (en) Lithium iron phosphate material finished product is nitrogen gas recovery system of recycling for drying
CN204502443U (en) For the liquid-ring vacuum pump system of Benzene Chloride rectification under vacuum
CN206881463U (en) Vacuum tail gas cools down absorption recycling device
CN204873864U (en) Ammonium nitrate production neutralizer gaseous phase condensation waste water recycling device
CN204125193U (en) A kind of secondary stripper plant
CN205940216U (en) Rare nitre energy -saving appliance export heat reclaim unit
CN104291403B (en) A kind of secondary stripper plant
CN205556135U (en) Vacuum environmental protection liquid waste processing system
CN205128182U (en) Quick cooling device of cutting fluid
CN100584534C (en) Hard alloy mixing material vibration drying method and device
CN205287684U (en) Gaseous condensation recovery device

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170908

Termination date: 20210224