CN206457271U - Light-catalyzed reaction purifier - Google Patents
Light-catalyzed reaction purifier Download PDFInfo
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- CN206457271U CN206457271U CN201720066268.4U CN201720066268U CN206457271U CN 206457271 U CN206457271 U CN 206457271U CN 201720066268 U CN201720066268 U CN 201720066268U CN 206457271 U CN206457271 U CN 206457271U
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- heat insulation
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- layer heat
- stainless steel
- steel casing
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02W—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO WASTEWATER TREATMENT OR WASTE MANAGEMENT
- Y02W10/00—Technologies for wastewater treatment
- Y02W10/30—Wastewater or sewage treatment systems using renewable energies
- Y02W10/37—Wastewater or sewage treatment systems using renewable energies using solar energy
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- Physical Water Treatments (AREA)
- Treatment Of Water By Oxidation Or Reduction (AREA)
Abstract
The utility model is related to a kind of light-catalyzed reaction purifier, including double-layer heat insulation stainless steel casing, aerator, pH meter probe, ultraviolet specrophotometer, ultrasonic generator, lid, heating wire and changeable type light source；Ultrasonic generator is placed in the interlayer of double-layer heat insulation stainless steel casing；Air inlet and liquid outlet are provided with the wall of double-layer heat insulation stainless steel casing side；Aerator is by air inlet with being connected inside double-layer heat insulation stainless steel casing；Liquid outlet is connected with pH meter probe and ultraviolet specrophotometer respectively；The exhaust outlet with being connected inside double-layer heat insulation stainless steel casing is provided with lid；One end of changeable type light source is arranged on lid, and the other end is stretched into inside double-layer heat insulation stainless steel casing；Heating wire is arranged on double-layer heat insulation stainless steel casing bottom.The utility model can realize adjustable light source, constant temperature, course of reaction detect, can reduce light-catalyzed reaction to the experimental procedure of detection and can significantly improve light-catalyzed reaction conventional efficient in real time.
Description
Technical field
The utility model belongs to light-catalyzed reaction degradable organic pollutant and determination techniques field, is related to a kind of photocatalysis anti-
Answer purifier, especially a kind of supersonic synergy ozone, the light-catalyzed reaction purifier of ultraviolet pH meter combination temperature control integration.
Background technology
Photocatalitic Technique of Semiconductor is application of the semi-conducting material in photocatalysis field, mainly uses semi-conducting material to inhale
Solar radiation is received, semiconductor, which is stimulated, produces electronics and hole, electronics and hole are again with absorption in semiconductor material surface
A series of chemical reaction occurs for material.Tokyo Univ Japan Fujishima and scientist Honda existed first in 1972
Delivered on Nature on titanium dioxide single crystalline electrode in the paper of photodissociation aquatic products hydrogen phenomenon, caused scientists from all over the world to two
The great attention of titanium oxide semiconductor.In recent years, various new catalyst were widely studied, and for sun transformation of energy
With the application in terms of storage, photochemical syntheses, photocatalysis degradation organic contaminant, photo-catalyst.
Although various new photochemical catalysts are constantly found out, it is used for the Photoreactor of catalyst reaction
Seldom, the especially traditional photocatalysis apparatus in laboratory, lamp source, light-catalyzed reaction bottle, pH detections, UV spectrophotometer measuring
Mostly it is used separately, uses cumbersome.Publication number be propose in CN105582871A patent application it is a kind of super
Sound assisted photo-catalysis reacts purifier, and ultrasonic wave is combined with light-catalyzed reaction purifier, to improve photocatalysis effect
Rate；Publication number is to propose a kind of ozone, ultraviolet light, ultrasonic wave synergistic reaction wastewater treatment in CN104803469A patent application
Device, utilizes ultrasonic wave, ozone and assist process sewage；Notification number be propose in CN103112924B patent of invention it is a kind of super
The experimental provision of sound synergy ozone degrading pesticide, by weighing sensor, acidity-basicity sensor and temperature sensor and experimental provision
It is connected, in real time the quality of detection solution, the change of thermometer soda acid；Publication number is to propose one in CN102627370A patent application
The wastewater degradation microwave photocatalytic device that can continue to maintain high treatment efficiency is planted, using ultrasonic wave on the premise of machine is not torn open
Fuselage dirt is cleared up, to maintain the efficiency operation of device.But, ultrasonic wave, ozone and ultraviolet assistance degraded, pH and
Ultraviolet real-time monitoring and temperature-controllable and the light-catalyzed reaction purifier of instrument automatically cleaning integration are seldom.
Utility model content
For above-mentioned technical problem present in prior art, the purpose of this utility model is to provide a kind of achievable light
Source is adjustable, constant temperature, course of reaction are detected in real time, light-catalyzed reaction can be reduced to detection experimental procedure and light can be significantly improved urge
Change the light-catalyzed reaction purifier of reaction experiment efficiency.
To achieve the above object, the utility model is adopted the following technical scheme that：
A kind of light-catalyzed reaction purifier, it is characterised in that：The light-catalyzed reaction purifier includes double-layer heat insulation
Stainless steel casing, aerator, pH meter probe, ultraviolet specrophotometer, ultrasonic generator, lid, heating wire and replaceable
Formula light source；The double-layer heat insulation stainless steel casing is integrally the tubular structure of one end open；The ultrasonic generator is placed in bilayer
In the interlayer for being incubated stainless steel casing；Air inlet and liquid outlet are provided with the double-layer heat insulation stainless steel casing side wall；Institute
Aerator is stated by the air inlet on the wall of double-layer heat insulation stainless steel casing side with being connected inside double-layer heat insulation stainless steel casing；
Liquid outlet on the double-layer heat insulation stainless steel casing side wall is connected with pH meter probe and ultraviolet specrophotometer respectively；It is described
The exhaust outlet with being connected inside double-layer heat insulation stainless steel casing is provided with lid；It is stainless that the lid is arranged on double-layer heat insulation
The top of outer steel shell；One end of the changeable type light source is arranged on lid, and the other end stretches into double-layer heat insulation stainless steel casing
It is internal；The heating wire is arranged on the bottom of double-layer heat insulation stainless steel casing.
Preferably, the light-catalyzed reaction purifier that the utility model is used is also stainless including being arranged on double-layer heat insulation
Magnetic stirring apparatus and temperature sensor inside outer steel shell.
Preferably, the light-catalyzed reaction purifier that the utility model is used is also stainless including being arranged on double-layer heat insulation
The filter of the replaceable filter membrane at liquid outlet on the wall of outer steel shell side.
Preferably, the light-catalyzed reaction purifier that the utility model is used also includes outlet valve, pH meter valve
Door and ultraviolet detection valve；Liquid outlet on the double-layer heat insulation stainless steel casing side wall by the filter of replaceable filter membrane with
Mouth of a river valve is connected；Liquid outlet on the double-layer heat insulation stainless steel casing side wall by the filter of replaceable filter membrane respectively with
PH meter valve and ultraviolet detection valve are connected；The pH meter valve is connected with pH meter probe；The ultraviolet detection valve with
The cuvette of ultraviolet specrophotometer is connected.
Preferably, the aerator that the utility model is used includes ventilation pump, gas flowmeter and breather pipe；Institute
Ventilation pump is stated by gas flowmeter with breather pipe to be connected；The breather pipe passes through on the wall of double-layer heat insulation stainless steel casing side
Air inlet inside double-layer heat insulation stainless steel casing with connecting；The end of the breather pipe inside double-layer heat insulation stainless steel casing
Portion is provided with aeration head.
Preferably, the lid that the utility model is used is provided with light source through holes, the changeable type light source is placed in light
Fixed in the through hole of source and by lamp tube replacement knob.
Preferably, the changeable type light source that the utility model is used includes glass outer, glass inner cover and fluorescent tube；
The glass outer covers in outside glass inner cover and is provided with space between glass inner cover；The fluorescent tube is placed in glass inner cover
In；Water inlet and delivery port are provided with the glass outer；The water inlet passes through between glass outer and glass inner cover
Space connected with delivery port.
Preferably, the fluorescent tube that the utility model is used is any one in xenon lamp, mercury lamp or LED, the lamp
The intensity of light source of pipe is adjustable.
Preferably, being additionally provided with magnetic agitation on the side wall for the double-layer heat insulation stainless steel casing that the utility model is used
Switch, heater switch, ultrasonic switch, lamp current adjusting knob and temperature display.
Preferably, the gas that the utility model is passed through is one kind of ozone, oxygen or air.
Preferably, the exhaust outlet of cover of the present utility model is general ground, it can be connected with drying tube, condenser pipe, with
Prevent the effusion of steam in course of reaction.
Preferably, the utility model can connect ultraviolet specrophotometer, pH meter, reaction can in real time be monitored, and
And light-catalyzed reaction fuselage can be separated with detection means.
The utility model has the advantages that：
The utility model provides a kind of light-catalyzed reaction purifier, including double-layer heat insulation stainless steel casing, aeration dress
Put, pH meter probe, ultraviolet specrophotometer, ultrasonic generator, lid, heating wire and changeable type light source；Double-layer heat insulation is not
Rust outer steel shell is integrally the tubular structure of one end open；Ultrasonic generator is placed in the interlayer of double-layer heat insulation stainless steel casing；It is double
Air inlet and liquid outlet are provided with the wall of layer insulation stainless steel casing side；Aerator passes through double-layer heat insulation stainless steel casing side
Air inlet on wall inside double-layer heat insulation stainless steel casing with connecting；Liquid outlet point on the wall of double-layer heat insulation stainless steel casing side
It is not connected with pH meter probe and ultraviolet specrophotometer；It is provided with lid with being connected inside double-layer heat insulation stainless steel casing
Exhaust outlet；Lid is arranged on the top of double-layer heat insulation stainless steel casing；One end of changeable type light source is arranged on lid, separately
One end is stretched into inside double-layer heat insulation stainless steel casing；Heating wire is arranged on the bottom of double-layer heat insulation stainless steel casing.Utilize this reality
With new device, ultrasound, ventilation (ozone, oxygen or air), constant temperature and light-catalyzed reaction can be carried out simultaneously, realize that reaction is real-time
Monitoring, can reduce light-catalyzed reaction to the experimental procedure of detection, significantly improve light-catalyzed reaction conventional efficient.Meanwhile, ultraviolet light,
Ultrasonic wave, ozone all has sterilizing function, and the present apparatus can be additionally used in reacted automatically cleaning.
Brief description of the drawings
Fig. 1 is the structural representation of light-catalyzed reaction purifier provided by the utility model；
Fig. 2 is the structural representation for the cover part that the utility model is used；
Fig. 3 is the structural representation for the base portion that the utility model is used；
Fig. 4 is the structural representation for the lamp tube that the utility model is used；
Fig. 5 is rhodamine B degradation uv-spectrogram in the utility model embodiment 1；
Fig. 6 is the pH variation diagrams of catalysis oxidation methanol in the utility model embodiment 2；
Description of reference numerals is as follows：
1- lids；2- exhaust outlets；3- glass outers；4- glass inner covers；5- fluorescent tubes；6- water inlets；7- delivery ports；8- fluorescent tubes
Change knob；9- ultrasonic generators；10- aeration heads；11- gas flowmeters；12- ventilation pumps；13- heating wire；14- magnetic agitations
Device；15- temperature sensors；16- outlet valves；17-pH counts valve；18-pH meter probes；The filter of the replaceable filter membranes of 19-；
20- ultraviolet detection valves；21- cuvettes；22- double-layer heat insulation stainless steel casings.
Embodiment
In order to be better understood from above-mentioned technical proposal of the present utility model, below in conjunction with the accompanying drawings with specific embodiment to this reality
It is described in further detail with new.
Referring to Fig. 1, Fig. 2, Fig. 3 and Fig. 4, the utility model provides a kind of light-catalyzed reaction purifier, photocatalysis
Reacting purifier includes double-layer heat insulation stainless steel casing 22, aerator, pH meter probe 18, ultraviolet specrophotometer, ultrasound
Generator 9, lid 1, heating wire 13 and changeable type light source；The entirety of double-layer heat insulation stainless steel casing 22 is the cylinder of one end open
Shape structure；Ultrasonic generator 9 is placed in the interlayer of double-layer heat insulation stainless steel casing 22；On the side wall of double-layer heat insulation stainless steel casing 22
It is provided with air inlet and liquid outlet；Aerator is protected by the air inlet on the side wall of double-layer heat insulation stainless steel casing 22 with double-deck
Connected inside warm stainless steel casing 22；Liquid outlet on the side wall of double-layer heat insulation stainless steel casing 22 respectively with pH meter probe 18 with
And ultraviolet specrophotometer is connected；The exhaust outlet 2 with being connected inside double-layer heat insulation stainless steel casing 22 is provided with lid 1；
Lid 1 is arranged on the top of double-layer heat insulation stainless steel casing 22；One end of changeable type light source is arranged on lid 1 (referring to Fig. 2
And Fig. 4), the other end is stretched into inside double-layer heat insulation stainless steel casing 22；Heating wire 13 is arranged on double-layer heat insulation stainless steel casing
22 bottom (referring to Fig. 3).
Light-catalyzed reaction purifier also includes being arranged on the magnetic stirring apparatus inside double-layer heat insulation stainless steel casing 22
14 and temperature sensor 15.
Light-catalyzed reaction purifier also includes being arranged at the liquid outlet on the side wall of double-layer heat insulation stainless steel casing 22
The filter 19 of replaceable filter membrane.
Light-catalyzed reaction purifier also includes outlet valve 16, pH meter valve 17 and ultraviolet detection valve 20；It is double
Liquid outlet on the layer insulation side wall of stainless steel casing 22 is connected by the filter 19 of replaceable filter membrane with mouth of a river valve 16；It is double-deck
Be incubated liquid outlet on the side wall of stainless steel casing 22 by the filter 19 of replaceable filter membrane respectively with pH meter valve 17 and ultraviolet
Detection valve 20 is connected；PH meter valve 17 is connected with pH meter probe 18；Ultraviolet detection valve 20 and ultraviolet specrophotometer
Cuvette 21 is connected.
Aerator includes ventilation pump 12, gas flowmeter 11 and breather pipe；Ventilation pump 12 passes through gas flowmeter 11
It is connected with breather pipe；Breather pipe passes through outside the air inlet on the side wall of double-layer heat insulation stainless steel casing 22 and double-layer heat insulation stainless steel
Connected inside shell 22；The end of breather pipe inside double-layer heat insulation stainless steel casing 22 is provided with aeration head 10.
Lid 1 is provided with light source through holes, and changeable type light source is placed in light source through holes and solid by lamp tube replacement knob 8
It is fixed.
Referring to Fig. 2, there is the blow vent 2 of general ground on cover 1, drying tube or spherical condensation tube, this reality can be installed
Include glass outer 3, glass inner cover 4 and fluorescent tube 5 with new used changeable type light source；Glass outer 3 covers in glass
The outside of inner cover 4 is simultaneously provided with space between glass inner cover 4；Fluorescent tube 5 is placed in glass inner cover 4；Be provided with glass outer 3 into
The mouth of a river 6 and delivery port 7；Water inlet 6 is connected by the space between glass outer 3 and glass inner cover 4 with delivery port 7；Lamp
Pipe 5 is any one in xenon lamp, mercury lamp or LED, and the intensity of light source of fluorescent tube 5 is adjustable.
Magnetic agitation switch, heater switch, ultrasonic switch, lamp are additionally provided with the side wall of double-layer heat insulation stainless steel casing 22
Tube current adjusting knob and temperature display.
The utility model is when specifically used, it is first determined fluorescent tube 5 (uviol lamp, xenon lamp or LED), by fluorescent tube more
Change knob 8 and install；Secondly, cover 1 is opened, pours into and treats degraded solutions and catalyst, and installs cover, circulation is passed through cold
Solidifying water, condensed water is entered by water inlet 6, discharged from delivery port 7；Gas flowmeter 11 is opened, gas is pumped into by ventilation pump 12 (smelly
Oxygen, oxygen or air)；Magnetic agitation switch and ultrasonic switch are opened, lamp source electric current and temperature are adjusted by adjusting panel
Degree；New filter membrane is installed at the filter 19 of replaceable filter membrane；Determine pH value of solution：Close outlet valve 16 and ultraviolet detection
Valve 20, by certain reaction time, opens pH meter valve 17, the solution of reaction is contacted with pH meter probe 18, by aobvious
Show the pH of panel recording solution.
Determine solution uv-spectrophotometric：Outlet valve 16 and pH meter valve 17 are closed, by certain reaction time,
Ultraviolet detection valve 20 is opened, solution is entered cuvette 21, passes through the ultraviolet absorption value of computer monitor recording solution.
After reaction terminates, condensed water and all switches are closed；PH meter valve 17 and ultraviolet detection valve 20 are closed, is opened out
Mouth of a river valve 16, solution is discharged from delivery port；
The cleaning of instrument：Running water is poured into cabinet, ultrasonic switch is opened, ultraviolet lamp tube is changed, the certainly clear of fuselage is realized
It is clean.
1 constant temperature of embodiment-xenon lamp-ultraviolet detection
First, it is xenon lamp to determine fluorescent tube, by lamp tube replacement knob 8 and is installed；Secondly, cover 1 is opened, pours into and waits to drop
Solving solution rhodamine B, (concentration is 1*10-5Mol/L, 100mL), p25 (100mg) is added, and cover is installed, it is passed through circulation cold
Solidifying water, condensed water is entered by water inlet 6, discharged from delivery port 7；Gas flowmeter 11 is opened, air is pumped into by ventilation pump 12；Beat
Magnetic agitation switch is driven, is 25 DEG C of 8A and thermostatic by adjusting panel to adjust lamp source electric current；In the filter of replaceable filter membrane
New filter membrane is installed at first 19；Outlet valve 16 and pH meter valve 17 are closed, starts timing, every 10 minutes, opens purple
Outer detection valve 20, makes solution enter cuvette 21, by the ultraviolet absorption value of computer monitor recording solution, takes altogether 6 times
Sample terminates；After reaction terminates, condensed water and all switches are closed；PH meter valve 17 and ultraviolet detection valve 20 are closed, is opened out
Mouth of a river valve 16, solution is discharged from delivery port.The uv-spectrogram of degraded solutions rhodamine B refers to Fig. 5.Wherein, first
For initial rhodamine B uv-spectrogram (collection of illustrative plates peak area is directly proportional to concentration, peak area reduce, rhodamine B concentration reduce),
Afterwards, reaction solution enters cuvette every 10 minutes, ultraviolet specrophotometer can record its corresponding collection of illustrative plates, totally 7 samples.
There is collection of illustrative plates as can be seen that catalyst p25 rhodamine B degradations are with the time, the trend of light intensity change shows the Photoreactor relatively to manage
The photo catalysis reactor for the experiment thought.
2 constant temperature of embodiment-xenon lamp-pH detections
It is xenon lamp to determine fluorescent tube, by lamp tube replacement knob 8 and is installed；Secondly, cover 1 is opened, question response is poured into
Solution methanol (100mL), adds Cob altporphyrin class catalyst (100mg), and installs cover, is passed through circulating condensing water, condensed water
Entered by water inlet 6, discharged from delivery port 7；Gas flowmeter 11 is opened, oxygen is pumped into by ventilation pump 12, and adjusted by flowmeter
Throttle body flow is 1 unit atmospheric pressure；Magnetic agitation switch is opened, is 8A and temperature by adjusting panel to adjust lamp source electric current
Spend 25 DEG C of constant temperature；New filter membrane is installed at the filter 19 of replaceable filter membrane；Close outlet valve 16 and ultraviolet detection valve
Door 20, every 1 hour, opens pH meter valve 17, the solution of reaction is contacted with pH meter probe 18, recorded by display panel
The pH of solution, takes altogether 6 samples to terminate；After reaction terminates, condensed water and all switches are closed；Close pH meter valve 17 and ultraviolet
Valve 20 is detected, outlet valve 16 is opened, solution is discharged from delivery port.The pH value reference picture 6 of catalysis oxidation methanol, its
In, with the reaction time, pH is tapered into, and illustrates that reactant methanol becomes formaldehyde in gradually reaction, so as to cause pH gradually to become
It is small.
3 constant temperature of embodiment-ultrasound-uviol lamp-ultraviolet detection
It is uviol lamp to determine fluorescent tube, by lamp tube replacement knob 8 and is installed；Secondly, cover 1 is opened, pours into and waits to degrade
(concentration is 1*10 to solution methylene blue-5Mol/L, 100mL), p25 (100mg) is added, and cover is installed, it is passed through circulating condensing
Water, condensed water is entered by water inlet 6, is discharged from delivery port 7；Gas flowmeter 11 is opened, ozone is pumped into by ventilation pump 12, and by
Flowmeter adjusting gas flow is 1 unit atmospheric pressure；Ultrasound is opened, magnetic agitation switch adjusts lamp source by adjusting panel
Electric current is 25 DEG C of 8A and thermostatic；New filter membrane is installed at the filter 19 of replaceable filter membrane；Close outlet valve
16 and pH meter valve 17, start timing, every 10 minutes, open ultraviolet detection valve 20, solution is entered cuvette 21, pass through
The ultraviolet absorption value of computer monitor recording solution, takes altogether 6 samples to terminate；After reaction terminates, close condensed water and all open
Close；PH meter valve 17 and ultraviolet detection valve 20 are closed, outlet valve 16 is opened, solution is discharged from delivery port.
4 constant temperature of embodiment-ultrasound-xenon lamp-ultraviolet-pH detections
It is xenon lamp to determine fluorescent tube, by lamp tube replacement knob 8 and is installed；Secondly, cover 1 is opened, pours into and treats that degraded is molten
(concentration is 1*10 to liquid X3B-5Mol/L, 100mL), p25 (100mg) is added, and cover is installed, circulating condensing water is passed through, is condensed
Water is entered by water inlet 6, is discharged from delivery port 7；Gas flowmeter 11 is opened, oxygen is pumped into by ventilation pump 12, and by flowmeter
Adjusting gas flow is 1 unit atmospheric pressure；Open ultrasonic agitation switch, by adjust panel adjust lamp source electric current be 8A and
25 DEG C of thermostatic；New filter membrane is installed at the filter 19 of replaceable filter membrane；Close outlet valve 16 and ultraviolet detection
Valve 20, every 20 minutes, opens pH meter valve 17, the solution of reaction is contacted with pH meter probe 18, remembered by display panel
The pH of solution is recorded, after sampling terminates, pH meter valve 17 is closed, opens ultraviolet detection valve 20, solution is entered cuvette 21, lead to
The ultraviolet absorption value of computer monitor recording solution is crossed, takes 6 samples to terminate altogether；After reaction terminates, condensed water is closed and all
Switch；PH meter valve 17 and ultraviolet detection valve 20 are closed, outlet valve 16 is opened, solution is discharged from delivery port.
The instrument automatically cleaning of embodiment 5
Lamp source is defined as uviol lamp, and adjusts electric current for 8A；Certain volume running water is poured into reaction unit；It is passed through smelly
Oxygen, and open ultrasonic switch；Reaction 1~2 hour, is purified and is sterilized to reaction unit；After reaction terminates, ozone is closed,
Water is discharged from outlet valve 16, uviol lamp and ultrasonic switch is closed.
Embodiment above is intended merely to illustrate the technical solution of the utility model, and is not intended as to of the present utility model
Limit, any change made based on essence of the present utility model to embodiment described above, deformation will all fall new in this practicality
In the scope of the claims of type.
Claims (10)
1. a kind of light-catalyzed reaction purifier, it is characterised in that：The light-catalyzed reaction purifier includes double-layer heat insulation not
Become rusty outer steel shell（22）, aerator, pH meter probe（18）, ultraviolet specrophotometer, ultrasonic generator（9）, lid（1）, electric heating
Silk（13）And changeable type light source；The double-layer heat insulation stainless steel casing（22）Entirety is the tubular structure of one end open；Institute
State ultrasonic generator（9）It is placed in double-layer heat insulation stainless steel casing（22）Interlayer in；The double-layer heat insulation stainless steel casing（22）
Air inlet and liquid outlet are provided with the wall of side；The aerator passes through double-layer heat insulation stainless steel casing（22）Entering on the wall of side
Gas port and double-layer heat insulation stainless steel casing（22）Inside connects；The double-layer heat insulation stainless steel casing（22）Go out liquid on the wall of side
Mouth respectively with pH meter probe（18）And ultraviolet specrophotometer is connected；The lid（1）On be provided with it is stainless with double-layer heat insulation
Outer steel shell（22）The exhaust outlet that inside connects（2）；The lid（1）It is arranged on double-layer heat insulation stainless steel casing（22）Top
Portion；One end of the changeable type light source is arranged on lid（1）On, the other end stretches into double-layer heat insulation stainless steel casing（22）It is interior
Portion；The heating wire（13）It is arranged on double-layer heat insulation stainless steel casing（22）Bottom.
2. light-catalyzed reaction purifier according to claim 1, it is characterised in that：The light-catalyzed reaction purifier
Also include being arranged on double-layer heat insulation stainless steel casing（22）Internal magnetic stirring apparatus（14）And temperature sensor（15）.
3. light-catalyzed reaction purifier according to claim 2, it is characterised in that：The light-catalyzed reaction purifier
Also include being arranged on double-layer heat insulation stainless steel casing（22）The filter of replaceable filter membrane at liquid outlet on the wall of side（19）.
4. light-catalyzed reaction purifier according to claim 3, it is characterised in that：The light-catalyzed reaction purifier
Also include outlet valve（16）, pH meter valve（17）And ultraviolet detection valve（20）；The double-layer heat insulation stainless steel casing
（22）The filter that liquid outlet on the wall of side passes through replaceable filter membrane（19）With mouth of a river valve（16）It is connected；The double-layer heat insulation is not
Become rusty outer steel shell（22）The filter that liquid outlet on the wall of side passes through replaceable filter membrane（19）Respectively with pH meter valve（17）And it is ultraviolet
Detect valve（20）It is connected；The pH meter valve（17）With pH meter probe（18）It is connected；The ultraviolet detection valve（20）With
The cuvette of ultraviolet specrophotometer（21）It is connected.
5. light-catalyzed reaction purifier according to claim 4, it is characterised in that：The aerator includes ventilation pump
（12）, gas flowmeter（11）And breather pipe；The ventilation pump（12）Pass through gas flowmeter（11）It is connected with breather pipe；
The breather pipe passes through double-layer heat insulation stainless steel casing（22）Air inlet and double-layer heat insulation stainless steel casing on the wall of side（22）It is interior
Portion connects；It is described in double-layer heat insulation stainless steel casing（22）The end of internal breather pipe is provided with aeration head（10）.
6. the light-catalyzed reaction purifier according to claim 1 or 2 or 3 or 4 or 5, it is characterised in that：The lid
（1）Light source through holes are provided with, the changeable type light source is placed in light source through holes and by lamp tube replacement knob（8）It is fixed.
7. light-catalyzed reaction purifier according to claim 6, it is characterised in that：The changeable type light source includes glass
Glass outer cover（3）, glass inner cover（4）And fluorescent tube（5）；The glass outer（3）Cover in glass inner cover（4）It is outside and with glass
Cover（4）Between be provided with space；The fluorescent tube（5）It is placed in glass inner cover（4）In；The glass outer（3）On be provided with into water
Mouthful（6）And delivery port（7）；The water inlet（6）Pass through glass outer（3）With glass inner cover（4）Between space and water outlet
Mouthful（7）Connect.
8. light-catalyzed reaction purifier according to claim 7, it is characterised in that：The fluorescent tube（5）It is xenon lamp, mercury lamp
Or any one in LED, the fluorescent tube（5）The intensity of light source it is adjustable.
9. light-catalyzed reaction purifier according to claim 8, it is characterised in that：The double-layer heat insulation stainless steel casing
（22）Side wall on to be additionally provided with magnetic agitation switch, heater switch, ultrasonic switch, lamp current adjusting knob and temperature aobvious
Display screen.
10. light-catalyzed reaction purifier according to claim 9, it is characterised in that：The exhaust outlet（2）It is general mill
Mouthful.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720066268.4U CN206457271U (en) | 2017-01-19 | 2017-01-19 | Light-catalyzed reaction purifier |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720066268.4U CN206457271U (en) | 2017-01-19 | 2017-01-19 | Light-catalyzed reaction purifier |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206457271U true CN206457271U (en) | 2017-09-01 |
Family
ID=59698725
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720066268.4U Expired - Fee Related CN206457271U (en) | 2017-01-19 | 2017-01-19 | Light-catalyzed reaction purifier |
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| Country | Link |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106745486A (en) * | 2017-01-19 | 2017-05-31 | 中南民族大学 | Light-catalyzed reaction purifier |
| CN107899530A (en) * | 2017-12-15 | 2018-04-13 | 中南民族大学 | A kind of organic chemical synthesis reactor of integration operation |
| CN113908790A (en) * | 2021-09-29 | 2022-01-11 | 华北电力大学 | Catalysis experiment platform and acousto-optic thermal catalysis experiment system |
| CN107899530B (en) * | 2017-12-15 | 2024-06-11 | 中南民族大学 | Organic chemical synthesis reactor of integration operation |
-
2017
- 2017-01-19 CN CN201720066268.4U patent/CN206457271U/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106745486A (en) * | 2017-01-19 | 2017-05-31 | 中南民族大学 | Light-catalyzed reaction purifier |
| CN107899530A (en) * | 2017-12-15 | 2018-04-13 | 中南民族大学 | A kind of organic chemical synthesis reactor of integration operation |
| CN107899530B (en) * | 2017-12-15 | 2024-06-11 | 中南民族大学 | Organic chemical synthesis reactor of integration operation |
| CN113908790A (en) * | 2021-09-29 | 2022-01-11 | 华北电力大学 | Catalysis experiment platform and acousto-optic thermal catalysis experiment system |
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