CN206454642U - A kind of synthesis reaction vessel of adjustable catalytic amount - Google Patents
A kind of synthesis reaction vessel of adjustable catalytic amount Download PDFInfo
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- CN206454642U CN206454642U CN201720113757.0U CN201720113757U CN206454642U CN 206454642 U CN206454642 U CN 206454642U CN 201720113757 U CN201720113757 U CN 201720113757U CN 206454642 U CN206454642 U CN 206454642U
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- storage silo
- catalyst
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Abstract
The utility model embodiment provides in a kind of synthesis reaction vessel of adjustable catalytic amount, including hollow sealing kettle, seal pot body and is provided with rabbling mechanism;Also include catalyst storage silo, pressure mechanism;Pressure mechanism includes air processing unit, pressure control module, and air processing unit includes compression pump, the valve that gas is discharged for the make-up gas into seal pot body or out of seal pot body, and pressure control module connects compression pump with control pressure pump work;Pressure sensor is provided with seal pot body, pressure sensor connects pressure control module by wireless network;The top and bottom of catalyst storage silo are by sealing for tubing joints kettle and turn on, and are provided with catalyst storage silo on multistage filtering plate, each filter and are designed with sieve aperture.
Description
Technical field
The utility model is related to field of mechanical technique, refers in particular to a kind of synthesis reaction vessel of adjustable catalytic amount.
Background technology
Reactor is widely used in oil, chemical industry, rubber, agricultural chemicals, dyestuff, medicine, food, for completing to vulcanize, nitrify,
The pressure vessel of the technical process such as hydrogenation, hydrocarbonylation, polymerization, condensation, such as reactor, reaction pot, decomposition pot, polymeric kettle.Instead
Answer kettle to be widely used in physically or chemically field, the material in reactor can be heated according to technological requirement, evaporated, cold
But, the function such as low high speed mixture.
By taking chemical field as an example, reactor is most important in chemical reagent preparing technical field, be chemical assistant production and
The basis of preparation and core apparatus.The developing history of chemical industry shows that structure and feature and the production efficiency of reactor cease
It is related.Mixer design selects improper, causes chemical reaction degree not reach production requirement much, causes the quality of production poor,
Loss is brought for user.
At present in the auxiliary agent preparing technical field such as neutralization and oxidation, conventional reactor has following several:
1) Chinese invention patent, application number 201310301630.8 is entitled:" a kind of inherent filtration dimeric dibasic acid reactor ".
It proposes a kind of reactor, and the top of the reactor is provided with charging aperture, and discharging opening is provided with the reaction of dismountable screen pack
Kettle.This reactor can be filtered to reacted material, with simple in construction and can improve the spy of dimeric dibasic acid processing efficiency
Point.The shortcoming of this reactor is:Simple in construction, function is single, adaptability and very flexible.
2) Chinese invention patent, application number 201410373498.6 is entitled:" a kind of neutralization reaction kettle ".It is proposed
Including paddle, ph analyzers, meter, control valve, filter screen and the neutralization reaction kettle for replacing cylinder;This reactor can be realized
The stirring that slow motion is combined with snap-action;Simultaneously through with the combined measurement such as ph analyzers, meter and control valve and control, be effectively ensured
Good reaction controlling and solid matter filtering.The shortcoming of this reactor is:Filter ring layout unreasonable, easily cause
Filter material blocks or filters insufficient, so as to influence general reaction effect and performance.
3) Chinese utility model patent, application number 201520661894.9 is entitled:" a kind of novel two-stage reactor ".
It proposes a kind of reactor, including U-shaped agitating paddle, lower motor and ectonexine kettle.This reactor is applied to classification
Reaction, and filtering is combined with stirring, it can effectively control the rotating speed and material reaction speed of screen pack.The shortcoming of this reactor
It is:Be not suitable for the complicated neutralization reaction that temperature control and pressure are present.
4) Chinese invention patent, application number 201410176425.8 is entitled:" a kind of temperature control reactor ".It is proposed
A kind of reactor, the wherein empty embedding L-type gas pipeline of inner wall of kettle and teeter column, and gas pipeline is for controlling reactant
Temperature.The shortcoming of this reactor is:Gas controls the less efficient of temperature.
5) Chinese invention patent, application number 201210196167.0 is entitled:" a kind of reactor easily cleaned ".Its
A kind of reactor is proposed, includes agitating device, filter, Drainage pipe and waste liquid outlet;With detachable, easy cleaning
Advantage.The shortcoming of this reactor is:Aforesaid reaction vessel structure simple structure, narrow application range.
It can thus be seen that the problem of these above-mentioned reactor generally existing unreasonable structures, these structures generally can not
The demands such as stirring, temperature control filtering, convenient cleaning are met simultaneously, particularly catalytic amount can not be all controlled.
Utility model content
For the problem of reactor structure is not reasonable present in prior art, the purpose of the utility model embodiment is
Propose a kind of good reactor of rational in infrastructure, using effect.
In order to solve the above problems, the utility model embodiment proposes a kind of synthetic reaction of adjustable catalytic amount
Rabbling mechanism is provided with kettle, including hollow sealing kettle, the seal pot body;Also include catalyst storage silo, pressure mechanism;
Wherein described pressure mechanism includes air processing unit, pressure control module, and the air processing unit includes being used for described
In seal pot body make-up gas or out of described seal pot body discharge gas compression pump, valve, the Stress control mould
Block connects the compression pump to control the pressure pump work;The compression pump connects the sealing kettle to control by valve
Pressure in the seal pot body;Pressure sensor is provided with wherein described seal pot body, the pressure sensor passes through wireless
Pressure control module described in network connection, the pressure control module connects the compression pump with according to the pressure in seal pot body
The value control compression pump and valve working;
The top and bottom of wherein described catalyst storage silo connect the sealing kettle by pipeline and turned on, described to urge
It is provided with agent storage silo on multistage filtering plate, each filter and is designed with sieve aperture;It is provided with the catalyst storage silo
Pump is respectively equipped with to control gas flow at the top and bottom of catalyst, the catalyst storage silo, so that gas is from catalyst
The catalyst on filter is brought into seal pot body when at the top of storage silo to catalyst storage silo flows, and in gas
Catalyst brings catalyst storage silo into out of seal pot body when from catalyst storage silo bottom to catalyst storage silo, top is flowed
And filter step by step on filter.
Wherein, sieve aperture, and the sieve of the filter positioned at top are designed with each filter in the multistage filtering plate
Hole is minimum, and the multistage filtering plate gradually increases along top-down direction screen-aperture.
Wherein, the bulkhead of the catalyst storage silo is coated with temperature control chuck, and the temperature control chuck includes
Two layers of chuck wall with formed sealed cavity with house temperature control medium.
Wherein, solid filtering material is provided between the multistage filtering plate.
Wherein, the catalyst storage silo bottom is provided with catalyst material mouth.
Wherein, the sealing kettle is provided with material inlet and discharging opening.
Wherein, in addition to gas tank, the gas tank connects the sealing kettle by compression pump, and the gas tank internal memory contains nitrogen
Gas or ammonia.
Above-mentioned technical proposal of the present utility model has the beneficial effect that:Above-mentioned technical proposal proposes a kind of can adjust and urged
The synthesis reaction vessel of agent amount, can utilize compression pump by the pressure sensor in pressure control module fitted seal kettle
With the pressure value in Valve controlling seal pot body.Further, in addition to catalyst storage silo, the two ends of catalyst storage silo are all
The connection sealing kettle and each own pump in two ends is to control gas flow.And multistage filtering plate is provided with catalyst storage silo, urging
Agent storage silo internal memory contains catalyst;So gas at the top of catalyst storage silo to catalyst storage silo flows when
Catalyst on filter is brought into seal pot body, and silo roof is stored from catalyst storage silo bottom to catalyst in gas
Catalyst is brought catalyst storage silo into out of seal pot body and filtered step by step on filter when portion is flowed.
Brief description of the drawings
Fig. 1 is the structural representation of the synthesis reaction vessel of the adjustable catalytic amount of the utility model embodiment;
Fig. 2 is the structural representation of another embodiment of the utility model.
Embodiment
To make the technical problems to be solved in the utility model, technical scheme and advantage clearer, below in conjunction with accompanying drawing
And specific embodiment is described in detail.
The utility model embodiment proposes a kind of synthesis reaction vessel of adjustable catalytic amount as shown in Figure 1 and Figure 2,
Including hollow sealing kettle 1, rabbling mechanism 5 is provided with the sealing kettle 1;Also include catalyst storage silo 4, forcing press
Structure;Wherein described pressure mechanism includes air processing unit 2, pressure control module 3, and the air processing unit 2 includes being used for
Make-up gas or compression pump, the valve from release gas in the sealing kettle 1, the pressure into the sealing kettle 1
Power control module 3 connects the compression pump to control the pressure pump work;The compression pump connects the sealing by valve
Kettle 1 with control it is described sealing kettle 1 in pressure;The top and bottom of wherein described catalyst storage silo 4 are connected by pipeline
Connect the sealing kettle 1 and turn on, be provided with the catalyst storage silo 4 on multistage filtering plate 41, each filter 41
It is designed with sieve aperture;Catalyst is provided with the catalyst storage silo 4, the top and bottom of the catalyst storage silo 4 are set respectively
Have pump 43 to control gas flow so that gas from the top of catalyst storage silo 4 to during catalyst 4 flows of storage silo incited somebody to action
Catalyst on filter plate 41 is brought into sealing kettle 1, and in gas from the bottom of catalyst storage silo 4 to catalyst storage silo 4
Catalyst is brought catalyst storage silo 4 into out of sealing kettle 1 and filtered step by step on filter 41 when top is flowed.
As shown in Figure 2, wherein being provided with pressure sensor 6 in the seal pot body 1, the pressure sensor 6 passes through nothing
Pressure control module 3 described in line network connection, the pressure control module 3 connects the compression pump with according in sealing kettle 1
Pressure value control the compression pump and valve working.
Wherein, sieve aperture is designed with each filter 41 in the multistage filtering plate 41, and positioned at the filter at top
41 sieve aperture is minimum, and the multistage filtering plate 41 gradually increases along top-down direction screen-aperture.Wherein, the catalysis
The bulkhead of agent storage silo 4 is coated with temperature control chuck, and the temperature control chuck includes two layers of chuck wall to form sealing
Cavity with house temperature control medium.Wherein, solid filtering material is provided between the multistage filtering plate 41.Wherein, the catalysis
The bottom of agent storage silo 4 is provided with catalyst material mouth 42.Wherein, the sealing kettle 1 is provided with material inlet and discharging opening.Wherein, it is described
The top and bottom of catalyst storage silo 4 are respectively equipped with retractable air valve 44.Wherein, in addition to gas tank, the gas tank passes through
The compression pump connection sealing kettle 1, the gas tank internal memory contains nitrogen or ammonia.
Described above is preferred embodiment of the present utility model, it is noted that for the ordinary skill of the art
For personnel, on the premise of principle described in the utility model is not departed from, some improvements and modifications can also be made, these improvement
Protection domain of the present utility model is also should be regarded as with retouching.
Claims (7)
- Stirred 1. being provided with a kind of synthesis reaction vessel of adjustable catalytic amount, including hollow sealing kettle, the seal pot body Mix mechanism;Characterized in that, also including catalyst storage silo, pressure mechanism;Wherein described pressure mechanism includes gas treatment list Member, pressure control module, the air processing unit include being used for into the seal pot body make-up gas or from described Compression pump, the valve of release gas in seal pot body, the pressure control module connect the compression pump to control the pressure Pump work;The compression pump connects the sealing kettle to control the pressure in the seal pot body by valve;It is wherein described Pressure sensor is provided with seal pot body, the pressure sensor connects the pressure control module by wireless network, described Pressure control module connects the compression pump to control the compression pump and valve working according to the pressure value in seal pot body;The top and bottom of wherein described catalyst storage silo connect the sealing kettle by pipeline and turned on, the catalyst It is provided with storage silo on multistage filtering plate, each filter and is designed with sieve aperture;Provided with catalysis in the catalyst storage silo Pump is respectively equipped with to control gas flow at the top and bottom of agent, the catalyst storage silo, so that gas is stored from catalyst The catalyst on filter is brought into seal pot body when silo roof portion is to catalyst storage silo flows, and in gas from urging Agent storage silo bottom to catalyst when flowing at the top of catalyst storage silo brought into out of seal pot body catalyst storage silo and by Level filtering is on filter.
- 2. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that the multistage filtering plate In each filter on be designed with sieve aperture, and the sieve aperture of the filter positioned at top is minimum, and the multistage filtering plate along from Direction screen-aperture under above gradually increases.
- 3. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that the catalyst storage The bulkhead in storehouse is coated with temperature control chuck, the temperature control chuck include two layers of chuck wall with formed sealed cavity with Accommodating temperature control medium.
- 4. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that the multistage filtering plate Between be provided with solid filtering material.
- 5. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that the catalyst storage Orlop portion is provided with catalyst material mouth.
- 6. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that the sealing kettle is set There are material inlet and discharging opening.
- 7. the synthesis reaction vessel of adjustable catalytic amount according to claim 1, it is characterised in that also including gas tank, institute State gas tank and the sealing kettle is connected by compression pump, the gas tank internal memory contains nitrogen or ammonia.
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Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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CN110270281A (en) * | 2019-07-01 | 2019-09-24 | 华东理工大学 | A kind of catalyst reaction equipment |
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Cited By (2)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110270281A (en) * | 2019-07-01 | 2019-09-24 | 华东理工大学 | A kind of catalyst reaction equipment |
CN110270281B (en) * | 2019-07-01 | 2021-07-23 | 华东理工大学 | Catalyst reaction device |
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Address after: 102402 north side of Jiyang village substation, Shilou Town, Fangshan District, Beijing Patentee after: Beijing Jiyi Holding Group Co.,Ltd. Address before: 102402 north side of Jiyang village substation, Shilou Town, Fangshan District, Beijing Patentee before: BEIJING JIYI CHEMICAL(BEIJING) CO.,LTD. |
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