CN206381687U - A kind of two grades of gas-liquid separation purifiers for sulfonation workshop - Google Patents

A kind of two grades of gas-liquid separation purifiers for sulfonation workshop Download PDF

Info

Publication number
CN206381687U
CN206381687U CN201621309574.8U CN201621309574U CN206381687U CN 206381687 U CN206381687 U CN 206381687U CN 201621309574 U CN201621309574 U CN 201621309574U CN 206381687 U CN206381687 U CN 206381687U
Authority
CN
China
Prior art keywords
liquid
gas
charge
level
outlet
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201621309574.8U
Other languages
Chinese (zh)
Inventor
肖志涛
黄林海
刘景旭
田晓龙
杨超
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
TIANJIN TIANZHI FINE CHEMICAL CO Ltd
Original Assignee
TIANJIN TIANZHI FINE CHEMICAL CO Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by TIANJIN TIANZHI FINE CHEMICAL CO Ltd filed Critical TIANJIN TIANZHI FINE CHEMICAL CO Ltd
Priority to CN201621309574.8U priority Critical patent/CN206381687U/en
Application granted granted Critical
Publication of CN206381687U publication Critical patent/CN206381687U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Landscapes

  • Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)

Abstract

The utility model is a kind of two grades of gas-liquid separation purifiers for sulfonation workshop, including gas-liquid separator, the gas-liquid separator is provided with one-level gas vent, level liquid is exported and gas-liquid mixture import, the level liquid outlet is connected with liquid effuser line, the one-level gas vent is connected with cyclone separator, the cyclone separator is provided with secondary gas outlet and secondary liquid outlet, the secondary gas outlet is connected with gas cleaning plant, secondary liquid outlet, which is connected with liquid and collected, to be in charge of, the liquid collects to be in charge of and is connected with the liquid effuser line, the liquid, which collects, is in charge of outer wall provided with heating jacket, the heating jacket and the liquid collect be in charge of between be provided with thermal source.The utility model separating effect more preferably, can avoid liquid liquid collect be in charge of in due to temperature reduction and Crystallization Plugging pipeline, it is ensured that the normal operation of whole equipment;Meanwhile, gas cleaning plant does not pollute the environment to the further purification of gas.

Description

A kind of two grades of gas-liquid separation purifiers for sulfonation workshop
Technical field
The utility model is related to gas-liquid separation field, more particularly to a kind of two grades of gas-liquid separations for sulfonation workshop are purified Device.
Background technology
With the raising of China's economic level, become increasingly abundant using the chemical products of membrane-type sulfonation technique productions, such as alkyl Benzene sulfonic acid sodium salt (LAS), ether alcohol sulfate (AES), aliphatic alcohol sulfate (K12), leather fat, farm chemical emulgent, weaving are helped Agent and petroleum sulfonate etc..Recently as the expansion of these chemical products species and scale, market competition is also more and more fierce, Therefore, for the xanthator of scale, how continuous and stable production can be kept from the production technology such as technique, equipment link, from And ensure that the performance of sulfonated product is stable, energy consumption is reduced, production cost is saved significant.
Gas-liquid separation part can be often related in sulfonation plant manufacturing process, will be entrained in product liquid or intermediate Gas separated.The means being generally separated be using gas-liquid separator carry out one-level separation, separating effect sometimes up to less than It is required that, also have and multi-stage separation is carried out using multigroup device, when the liquid isolated from separator is pooled to supervisor, sometimes Because the reduction of temperature crystallizes residual on branch line, time length can cause the blocking of pipeline, further result in separation dress Putting to run well;Gas after separation also can be emptied directly sometimes, and deleterious effect is caused to environment.
The content of the invention
The utility model aims to solve the problem that the deficiencies in the prior art, and provides a kind of two grades of gas-liquid separations for sulfonation workshop Purifier.
The utility model to achieve the above object, using following technical scheme:A kind of two grades of gas-liquids for sulfonation workshop One-level gas vent and one are respectively equipped with the top and bottom of separating purifying device, including gas-liquid separator, the gas-liquid separator Level liquid outlet, the gas-liquid separator side is provided with gas-liquid mixture import, and the level liquid outlet is connected with liquid outflow Pipeline, the one-level gas vent is connected with the top and bottom of cyclone separator, the cyclone separator by pipeline and is respectively equipped with Secondary gas is exported and secondary liquid outlet, and the secondary gas outlet is connected with gas cleaning plant, described two grades by pipeline Liquid outlet, which is connected with liquid and collected, to be in charge of, and the liquid collects to be in charge of and is connected with the liquid effuser line, and the liquid collects Be in charge of outer wall provided with heating jacket, the heating jacket and the liquid collect be in charge of between be provided with thermal source.
Both sides are connected with steam/water supply pipeline and steam/water outflow pipeline respectively above and below the heating jacket.
The heating jacket and the liquid collect be in charge of between be wound with resistive heater, the resistive heater is connected with electricity Source.
Rule gas liquid separating layer and silk screen are sequentially provided with the gas-liquid separator above the gas-liquid mixture import Multiple filling balls are filled with gas-liquid separation layer, the rule gas liquid separating layer.
Level liquid outlet and the junction of the liquid effuser line and the secondary liquid export with it is described Liquid collects the junction being in charge of and is equipped with regarding object lens.
The beneficial effects of the utility model are:The utility model is mixed to gas-liquid using gas-liquid separator combination cyclone separator Compound carries out the second-order separation, and more preferably, the liquid under cyclone separator collects to be in charge of is externally provided with heating jacket to separating effect, heating Thermal source is provided with sheath, can avoid liquid within liquid collects and is in charge of due to temperature reduction and Crystallization Plugging pipeline, enter one Step ensures the normal operation of whole equipment.Meanwhile, cyclone separator is also connected with gas cleaning plant, to the gas after gas-liquid separation Further purification, does not pollute the environment.
Brief description of the drawings
Fig. 1 is structural representation of the utility model in specific embodiment 1;
Fig. 2 is structural representation of the utility model in specific embodiment 2;
In figure:1- gas-liquid separators;2- one-level gas vents;3- level liquids are exported;4- gas-liquid mixture imports;5- liquid Body flows out pipeline;6- cyclone separators;7- secondary gas is exported;8- secondary liquids are exported;9- gas cleaning plants;10- liquid Collect and be in charge of;11- heating jackets;12- steam/water supply pipelines;13- steam/waters flow out pipeline;14- advises gas liquid separating layer; 15- silk screens gas-liquid separation layer;16- regards object lens;17- resistive heaters;18- power supplys;
It is described in detail referring to the drawings below with reference to embodiment of the present utility model.
Embodiment
The utility model is described in further detail with reference to the accompanying drawings and examples:
Embodiment 1:
As shown in figure 1, a kind of two grades of gas-liquid separation purifiers for sulfonation workshop, including gas-liquid separator 1, it is described The top and bottom of gas-liquid separator 1 are respectively equipped with one-level gas vent 2 and level liquid outlet 3, the side of gas-liquid separator 1 Provided with gas-liquid mixture import 4, the level liquid outlet 3 is connected with liquid effuser line 5, and the one-level gas vent 2 passes through Pipeline is connected with cyclone separator 6, and the top and bottom of cyclone separator 6 are respectively equipped with secondary gas outlet 7 and secondary liquid Outlet 8, the secondary gas outlet 7 is connected with gas cleaning plant 9 by pipeline, and the secondary liquid outlet 8 is connected with liquid remittance Gather division tupe 10, the liquid, which collects, to be in charge of 10 and is connected with the liquid effuser line 5, and the liquid, which collects, to be in charge of 10 outer walls and be provided with Heating jacket 11, the heating jacket 11 and the liquid collect be in charge of 10 between be provided with thermal source.
The heating jacket is connected with steam/water supply pipeline 12 and steam/water outflow pipeline 13 in both sides respectively about 11.
In the gas-liquid separator 1 He of rule gas liquid separating layer 14 is sequentially provided with the top of gas-liquid mixture import 4 Multiple filling balls are filled with silk screen gas-liquid separation layer 15, the rule gas liquid separating layer 14.
The level liquid outlet 3 and the junction of the liquid effuser line 5 and secondary liquid outlet 8 and institute State liquid and collect and be in charge of 10 junction and be equipped with regarding object lens 16.
Embodiment 2:
As shown in Fig. 2 a kind of two grades of gas-liquid separation purifiers for sulfonation workshop, including gas-liquid separator 1, it is described The top and bottom of gas-liquid separator 1 are respectively equipped with one-level gas vent 2 and level liquid outlet 3, the side of gas-liquid separator 1 Provided with gas-liquid mixture import 4, the level liquid outlet 3 is connected with liquid effuser line 5, and the one-level gas vent 2 passes through Pipeline is connected with cyclone separator 6, and the top and bottom of cyclone separator 6 are respectively equipped with secondary gas outlet 7 and secondary liquid Outlet 8, the secondary gas outlet 7 is connected with gas cleaning plant 9 by pipeline, and the secondary liquid outlet 8 is connected with liquid remittance Gather division tupe 10, the liquid, which collects, to be in charge of 10 and is connected with the liquid effuser line 5, and the liquid, which collects, to be in charge of 10 outer walls and be provided with Heating jacket 11, the heating jacket 11 and the liquid collect be in charge of 10 between be provided with thermal source.
The heating jacket 11 and the liquid collect be in charge of 10 between be wound with resistive heater 17, the resistive heater 17 are connected with power supply 18.
In the gas-liquid separator 1 He of rule gas liquid separating layer 14 is sequentially provided with the top of gas-liquid mixture import 4 Multiple filling balls are filled with silk screen gas-liquid separation layer 15, the rule gas liquid separating layer 14.
The level liquid outlet 3 and the junction of the liquid effuser line 5 and secondary liquid outlet 8 and institute State liquid and collect and be in charge of 10 junction and be equipped with regarding object lens 16.
The utility model combines cyclone separator 6 using gas-liquid separator 1 and carries out the second-order separation, gas-liquid to gas-liquid mixture Provided with rule gas liquid separating layer 14 and silk screen gas-liquid separation layer 15 in separator 1, gas body separating layer 14 is advised built with filling ball, Make to shuttle in gap of the gas-liquid mixture of entrance between filling ball, increase contact area, and silk screen gas-liquid separation layer 15 Gas-liquid is further separated, separating effect is more preferable.Liquid under cyclone separator 6, which collects, to be in charge of 10 and is externally provided with heating jacket 11, Thermal source is provided with heating jacket 11, can avoid liquid liquid collect be in charge of in 11 due to temperature reduction and Crystallization Plugging pipe Line, is further ensured that the normal operation of whole equipment.Meanwhile, cyclone separator 6 is also connected with gas cleaning plant 9, to gas-liquid point Gas from after is further purified, and is not polluted the environment.Level liquid outlet 3 and the junction and two of liquid effuser line 5 Level liquid outlet 8 and liquid, which collect, to be in charge of 10 junction and is equipped with regarding object lens 16, facilitates the timely facilities for observation of staff Running situation, level condition, the state of liquid, it is more scientific and reasonable to the more exhaustive management of production process.
The utility model is exemplarily described above in conjunction with accompanying drawing, it is clear that the utility model implement not by The limitation of aforesaid way, if the various improvement that method design of the present utility model and technical scheme are carried out are employed, or without Improvement directly applies to other occasions, within protection domain of the present utility model.

Claims (6)

1. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop, including gas-liquid separator (1), the gas-liquid separator (1) top and bottom are respectively equipped with one-level gas vent (2) and level liquid outlet (3), and gas-liquid separator (1) side is set There is gas-liquid mixture import (4), it is characterised in that the level liquid outlet (3) is connected with liquid effuser line (5), described one Level gas vent (2) is connected with the top and bottom of cyclone separator (6), the cyclone separator (6) by pipeline and is respectively equipped with two Level gas vent (7) and secondary liquid outlet (8), the secondary gas outlet (7) are connected with gas cleaning plant by pipeline (9), secondary liquid outlet (8), which is connected with liquid and collected, is in charge of (10), and the liquid, which collects, is in charge of (10) and the liquid flow Go out pipeline (5) to be connected, the liquid, which collects, is in charge of (10) outer wall provided with heating jacket (11), the heating jacket (11) with it is described Liquid, which collects, to be in charge of between (10) provided with thermal source.
2. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop according to claim 1, it is characterised in that institute Stating heating jacket (11), both sides are connected with steam/water supply pipeline (12) and steam/water outflow pipeline (13) respectively up and down.
3. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop according to claim 2, it is characterised in that institute State and be sequentially provided with rule gas liquid separating layer (14) and silk screen above the inherent gas-liquid mixture import (4) of gas-liquid separator (1) Multiple filling balls are filled with gas-liquid separation layer (15), the rule gas liquid separating layer (14).
4. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop according to claim 1, it is characterised in that institute State heating jacket (11) and the liquid collects to be in charge of between (10) and is wound with resistive heater (17), the resistive heater (17) It is connected with power supply (18).
5. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop according to claim 4, it is characterised in that institute State and be sequentially provided with rule gas liquid separating layer (14) and silk screen above the inherent gas-liquid mixture import (4) of gas-liquid separator (1) Multiple filling balls are filled with gas-liquid separation layer (15), the rule gas liquid separating layer (14).
6. a kind of two grades of gas-liquid separation purifiers for sulfonation workshop according to claim 3 or 5, its feature exists In, level liquid outlet (3) and the junction of the liquid effuser line (5) and secondary liquid outlet (8) with The liquid, which collects, to be in charge of the junction of (10) and is equipped with regarding object lens (16).
CN201621309574.8U 2016-11-30 2016-11-30 A kind of two grades of gas-liquid separation purifiers for sulfonation workshop Expired - Fee Related CN206381687U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201621309574.8U CN206381687U (en) 2016-11-30 2016-11-30 A kind of two grades of gas-liquid separation purifiers for sulfonation workshop

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201621309574.8U CN206381687U (en) 2016-11-30 2016-11-30 A kind of two grades of gas-liquid separation purifiers for sulfonation workshop

Publications (1)

Publication Number Publication Date
CN206381687U true CN206381687U (en) 2017-08-08

Family

ID=59487753

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201621309574.8U Expired - Fee Related CN206381687U (en) 2016-11-30 2016-11-30 A kind of two grades of gas-liquid separation purifiers for sulfonation workshop

Country Status (1)

Country Link
CN (1) CN206381687U (en)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110368711A (en) * 2019-05-28 2019-10-25 汕头市佳禾生物科技有限公司 A kind of crystallizer suitable for biological raw material

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110368711A (en) * 2019-05-28 2019-10-25 汕头市佳禾生物科技有限公司 A kind of crystallizer suitable for biological raw material

Similar Documents

Publication Publication Date Title
CN104194929B (en) A kind of oils and fats refines system
CN206381687U (en) A kind of two grades of gas-liquid separation purifiers for sulfonation workshop
CN104033880A (en) Boiler blow-down water heat energy utilization system
CN203820492U (en) Continuous wastewater evaporation-concentration-crystallization device
CN203200237U (en) Physical deacidifying tower of vegetable oil with high acid value
CN202983253U (en) Novel quick ethanol recovery device
CN205235473U (en) A oil -water separator for production of plasticizer epoxidized soybean oil
CN207259466U (en) Crude oil alkali refining mechanism
CN203139998U (en) Novel efficient gas-liquid separator device
CN206014730U (en) A kind of phenylacetic acid continuous production device
CN206328320U (en) A kind of high purity caprolactam refining plant
CN208275191U (en) A kind of device of the associated gas removal of impurities of level Four one mode
CN204619933U (en) A kind of pyromellitic acid anhydride production filtering device for raw material
CN203959827U (en) Tripping device for process for preparation of CS 2 molten sulfur
CN106282518A (en) Heater for rolling steel coal gas is carried out the Apparatus and method for of freezing dehumidification
CN203382860U (en) Reverse-flow melt filter
CN205216238U (en) Crude carbolic acid system of processing
CN206809803U (en) Donkey-hide gelatin production evaporator and seperator steam water circulation utilization system
CN103961966A (en) System for solving ultrahigh gas temperature of dynamic wave furnace of waste acid recycling device
CN106734342B (en) Preformed armor rod cleaning equipment
CN204451128U (en) There is the high-performance PA66GF extruder of emission-control equipment
CN109652154A (en) A kind of prying gas deoiling, dewatering integrated device and method
CN204121945U (en) A kind of pickling tower
CN103771374B (en) A kind of electron-level phosphoric acid baffle crystallization device
CN208139912U (en) A kind of bathroom waste-heat recovery device

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170808

Termination date: 20201130

CF01 Termination of patent right due to non-payment of annual fee