CN206345893U - A kind of high pure metal vacuum distillation plant - Google Patents
A kind of high pure metal vacuum distillation plant Download PDFInfo
- Publication number
- CN206345893U CN206345893U CN201621406486.XU CN201621406486U CN206345893U CN 206345893 U CN206345893 U CN 206345893U CN 201621406486 U CN201621406486 U CN 201621406486U CN 206345893 U CN206345893 U CN 206345893U
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- crucible
- retort
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- high pure
- pure metal
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- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
Abstract
The utility model discloses a kind of high pure metal vacuum distillation plant, the condensation being connected including distillation component and with distillation component, distilling component includes retort, it is arranged on the crucible in the middle part of retort, crucible outer wall is enclosed with heat transfer layer successively from inside to outside, zone of heating and thermal insulation layer, crucible top is provided with crucible cover, bell is provided with the top of retort, distillation component also includes the mixing component for being arranged on retort side, mixing component includes being arranged on the stirring motor outside retort side, through retort and the agitating shaft of the avris wall of crucible one, the agitating shaft other end is provided with agitating vane, through hole is provided with agitating vane, condensation includes steam collection hood, U-shaped condenser pipe, steam collection hood is connected through bell with crucible cover, the U-shaped condenser pipe other end is connected with air exhauster.Its is simple in construction, and being heated evenly steam, rising is quick, and condensation is quick, distilation efficiency high.
Description
Technical field
The utility model is related to purification of metals equipment technical field, more particularly to a kind of high pure metal vacuum distillation plant.
Background technology
In the high-tech area such as Aero-Space, navigation, infrared, various high pure metals are both needed to former as the basis of critical component
Material.With the development of science and technology its purity requirement more and more higher to high pure metal.It is main to use in order to improve metal purity
Chemical method and physical method.Wherein physical refining method of purification is mainly：Utilize distillation, solidification, crystallization, diffusion, electromigration etc.
Physical process removes impurity.Wherein generally required using process for purifying distillation and use the components such as retort, condenser, existing steaming
There is the heated uneven rising of steam in stove slowly in furnace, the low problem of distillation efficiency, and condensation is low there is also condensation efficiency, finally
Cause the problem of purification efficiency is low.
Therefore, design a kind of steam in retort and be heated evenly rising rapidly, condensation efficiency is high, and purification efficiency is high
High pure metal vacuum distillation plant is those skilled in the art of the present technique's urgent problem to be solved.
Utility model content
The utility model aims to provide a kind of high pure metal vacuum distillation plant, and above mentioned problem is solved well, and it is tied
Structure is simple, and being heated evenly steam, rising is quick, and condensation is quick, distilation efficiency high.
The technical solution of the utility model is a kind of high pure metal vacuum distillation plant, including distillation component and with distillation group
The condensation of part connection, the distillation component includes retort, the crucible that is arranged in the middle part of retort, the crucible outer wall by
It is enclosed with heat transfer layer, zone of heating and thermal insulation layer successively from inside to outside, the crucible top is provided with the top of crucible cover, the retort
Bell is provided with, the distillation component also includes the mixing component for being arranged on retort side, and the mixing component includes installing
Stirring motor outside retort side, through retort and the agitating shaft of the avris wall of crucible one, described agitating shaft one end with
Stirring motor rotates connection, and the agitating shaft other end is provided with agitating vane, the agitating vane and is provided with through hole, described
Agitating vane is arranged on inside crucible, and the condensation includes steam collection hood, U-shaped condenser pipe, and the steam collection hood is worn
Cross bell to connect with crucible cover, described U-shaped condenser pipe one end at the top of steam collection hood with connecting, the U-shaped condenser pipe other end
It is connected with air exhauster.
Further, vacuum-pumping tube is provided with the bell, the vacuum-pumping tube is connected with retort, crucible；Side
Just extract the air in retort and crucible out, make to form vacuum in distillation component, it is to avoid the gas in air is in hot environment
It is lower to be reacted with being refined metal, pollute.
Further, the crucible is graphite crucible.
Further, temperature measuring set is installed on the retort；The temperature in retort can be monitored at any time.
Further, the zone of heating is resistance heating wire；The heating of resistance heating wire is stable, and temperature control precision is high.
Further, be coated with outside the U-shaped condenser pipe in cooling layer, the U-shaped condenser pipe pipe be provided with it is porous cold
Solidifying plate, the U-shaped condensation bottom of the tube offers molten metal outlet, and molten metal outlet bottom is provided with conflux disk, the remittance
Flow table bottom is provided with discharge gate；Can rapidly and efficiently condensed steam, while collection condensate liquid rapidly and efficiently, improves condensation effect
Rate.
The beneficial effects of the utility model are：
1. the utility model is provided with mixing component in crucible, the velocity of liquid assets of steam in crucible is improved, makes steam
Be uniformly heated, and the most parts of the mixing component be located at crucible side, not stop steam rising passway,
Improve the efficiency to form steam；
2. the design of through hole, adds the circulation of steam, the velocity of liquid assets of steam is further increased, makes it heated more
Plus it is uniform, evaporation is rapid；
3. the design of steam collection hood and U-shaped condenser pipe, the rising of steam is concentrated rapid, at the same add steam with it is cold
The contact area of solidifying pipe, improves condensation effect and efficiency.
Brief description of the drawings
Fig. 1 is structural representation of the present utility model；
In figure：1. component is distilled, 11. retorts, 111. bells, 12. crucibles, 121. crucible covers, 13. heat transfer layers, 14. add
Thermosphere, 15. thermal insulation layers, 2. condensations, 21. steam collection hoods, 22.U type condenser pipes, 221. cooling layers, 222. porous condensations
Plate, the outlet of 223. molten metals, 23. air exhausters, 24. conflux disks, 241. discharge gates, 3. mixing components, 31. stirring motors, 32. stir
Mix axle, 33. agitating vanes, 332. through holes, 4. vacuum-pumping tubes.
Embodiment
In order that the purpose of this utility model, technical scheme and advantage are more clearly understood, below in conjunction with accompanying drawing, to this reality
It is further elaborated with new.
As shown in figure 1, the utility model provide a kind of high pure metal vacuum distillation plant, including distillation component 1 and with
The condensation 2 that component 1 is connected is distilled, the distillation component 1 includes retort 11, is arranged on the crucible at the middle part of retort 11
12, the outer wall of crucible 12 is enclosed with heat transfer layer 13, zone of heating 14 and thermal insulation layer 15, the top of crucible 12 successively from inside to outside
Crucible cover 121 is provided with, the top of retort 11 is provided with bell 111, and the distillation component 1 also includes being arranged on distillation
The mixing component 3 of the side of stove 11, the mixing component 3 include be arranged on the side of retort 11 outside stirring motor 31, run through
The agitating shaft 32 of retort 11 and the avris wall of crucible 12 1, described one end of agitating shaft 32 rotates with stirring motor 31 and is connected, described
The other end of agitating shaft 32, which is provided with agitating vane 33, the agitating vane 33, is provided with through hole 332, the agitating vane 33
It is arranged on inside crucible 12, the condensation 2 includes steam collection hood 21, U-shaped condenser pipe 22, the steam collection hood 21
Connected through bell 111 with crucible cover 121, described U-shaped one end of condenser pipe 22 is connected with the top of steam collection hood 21, described U-shaped
The other end of condenser pipe 22 is connected with air exhauster 23.
Vacuum-pumping tube 4 is provided with the bell 111, the vacuum-pumping tube 4 is connected with retort 11, crucible 12；Side
Just extract the air in retort 11 and crucible 12 out, make to form vacuum in distillation component 1, it is to avoid the gas in air is in high temperature
React, pollute with being refined metal under environment.The crucible 12 is graphite crucible.It is provided with the retort 1
Temperature measuring set；The temperature in retort 11 can be monitored at any time.The zone of heating 14 is resistance heating wire；Resistance heating wire's
Heating is stable, and temperature control precision is high.Cooling layer 221 is coated with outside the U-shaped condenser pipe 22, the U-shaped condenser pipe 22 is managed
Porous cold plate 222 is inside provided with, the U-shaped bottom of condenser pipe 22 offers molten metal outlet 223, the molten metal outlet
223 bottoms are provided with conflux disk 24, and the bottom of conflux disk 24 is provided with discharge gate 241；Can rapidly and efficiently condensed steam, simultaneously
Collection condensate liquid rapidly and efficiently, improves condensation efficiency.
The utility model is provided with mixing component 3 in crucible, improves the velocity of liquid assets of steam in crucible 12, makes steam
Be uniformly heated, and the most parts of mixing component 3 be located at the side of crucible 12, not stop steam rising lead to
Road, improves the efficiency to form steam；The design of through hole 332, adds the circulation of steam, further increases the stream of steam
Logical speed, is uniformly heated it, and evaporation is rapid；The design of steam collection hood 21 and U-shaped condenser pipe 22, makes the rising of steam
Concentrate rapid, while adding the contact area of steam and condenser pipe, improve condensation effect and efficiency.
Certainly, the utility model can also have other various embodiments, spiritual and its essence without departing substantially from the utility model
In the case of, those skilled in the art can make various corresponding changes and deformation, but these phases according to the utility model
The change and deformation answered should all belong to the scope of the claims appended by the utility model.
Claims (6)
1. a kind of high pure metal vacuum distillation plant, it is characterised in that：The condensation being connected including distillation component and with distillation component
Component, the distillation component includes retort, the crucible being arranged in the middle part of retort, and the crucible outer wall is wrapped successively from inside to outside
Heat transfer layer, zone of heating and thermal insulation layer are wrapped with, the crucible top is provided with the top of crucible cover, the retort and is provided with bell,
The distillation component also includes the mixing component for being arranged on retort side, and the mixing component includes being arranged on retort side
Outside stirring motor, through retort and the agitating shaft of the avris wall of crucible one, described agitating shaft one end is rotated with stirring motor
Connection, the agitating shaft other end, which is provided with agitating vane, the agitating vane, is provided with through hole, and the agitating vane is set
Inside crucible, the condensation includes steam collection hood, U-shaped condenser pipe, and the steam collection hood passes through bell and crucible
Lid connection, described U-shaped condenser pipe one end at the top of steam collection hood with connecting, and the U-shaped condenser pipe other end is connected with air exhauster.
2. high pure metal vacuum distillation plant according to claim 1, it is characterised in that：It is provided with the bell and takes out true
Blank pipe, the vacuum-pumping tube is connected with retort, crucible.
3. high pure metal vacuum distillation plant according to claim 1, it is characterised in that：The crucible is graphite crucible.
4. high pure metal vacuum distillation plant according to claim 1, it is characterised in that：Temperature is installed on the retort
Spend measuring instrument.
5. high pure metal vacuum distillation plant according to claim 1, it is characterised in that：The zone of heating is resistance heating
Silk.
6. high pure metal vacuum distillation plant according to claim 1, it is characterised in that：Wrapped outside the U-shaped condenser pipe
It is covered with cooling layer, the U-shaped condenser pipe pipe and is provided with porous cold plate, the U-shaped condensation bottom of the tube offers molten metal and gone out
Mouthful, molten metal outlet bottom is provided with conflux disk, and the tray bottom of confluxing is provided with discharge gate.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621406486.XU CN206345893U (en) | 2016-12-20 | 2016-12-20 | A kind of high pure metal vacuum distillation plant |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201621406486.XU CN206345893U (en) | 2016-12-20 | 2016-12-20 | A kind of high pure metal vacuum distillation plant |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206345893U true CN206345893U (en) | 2017-07-21 |
Family
ID=59317725
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201621406486.XU Active CN206345893U (en) | 2016-12-20 | 2016-12-20 | A kind of high pure metal vacuum distillation plant |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206345893U (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108452546A (en) * | 2018-04-09 | 2018-08-28 | 昆山佳鹿石英有限公司 | Antimony purifies rectifier unit and the method using device purification antimony |
| CN109971963A (en) * | 2019-04-17 | 2019-07-05 | 湖南省金润碲业有限公司 | A kind of silver-zine slag vacuum distillation plant |
| CN111235398A (en) * | 2020-03-13 | 2020-06-05 | 河南国玺超纯新材料股份有限公司 | Distillation plant is used in high-purity zinc production |
| CN113476876A (en) * | 2021-09-08 | 2021-10-08 | 南通辉正医药科技有限公司 | Distillation furnace device for medicine intermediate |
| CN113832358A (en) * | 2021-11-04 | 2021-12-24 | 江西水木机电设备有限公司 | Zinc-aluminum vacuum distillation separator |
-
2016
- 2016-12-20 CN CN201621406486.XU patent/CN206345893U/en active Active
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN108452546A (en) * | 2018-04-09 | 2018-08-28 | 昆山佳鹿石英有限公司 | Antimony purifies rectifier unit and the method using device purification antimony |
| CN109971963A (en) * | 2019-04-17 | 2019-07-05 | 湖南省金润碲业有限公司 | A kind of silver-zine slag vacuum distillation plant |
| CN111235398A (en) * | 2020-03-13 | 2020-06-05 | 河南国玺超纯新材料股份有限公司 | Distillation plant is used in high-purity zinc production |
| CN113476876A (en) * | 2021-09-08 | 2021-10-08 | 南通辉正医药科技有限公司 | Distillation furnace device for medicine intermediate |
| CN113832358A (en) * | 2021-11-04 | 2021-12-24 | 江西水木机电设备有限公司 | Zinc-aluminum vacuum distillation separator |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20200812 Address after: 311200 No. 83 Hongken Road, Hongken Farm, Xiaoshan Economic and Technological Development Zone, Hangzhou City, Zhejiang Province Patentee after: Hangzhou kaiyada semiconductor materials Co., Ltd Address before: Jiajiang Xinchang Town hongqicun 614000 Sichuan city in Leshan province 5. Patentee before: LESHAN KAIYADA OPTOELECTRONICS TECHNOLOGY Co.,Ltd. |
|
| TR01 | Transfer of patent right |