CN207109142U - Crystal growing furnace - Google Patents

Crystal growing furnace Download PDF

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Publication number
CN207109142U
CN207109142U CN201721005669.5U CN201721005669U CN207109142U CN 207109142 U CN207109142 U CN 207109142U CN 201721005669 U CN201721005669 U CN 201721005669U CN 207109142 U CN207109142 U CN 207109142U
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China
Prior art keywords
crucible
heater
crystal growing
growing furnace
heat
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CN201721005669.5U
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Chinese (zh)
Inventor
付亚杰
刘久明
吴诚
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Hebei Corefra Silicon Nitride Material Co Ltd
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Hebei Corefra Silicon Nitride Material Co Ltd
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Abstract

The utility model discloses a kind of crystal growing furnace that crystal is prepared using directional solidification method as principle, its chief component is body of heater, takes out blow-off system, heater, lifting rotation mechanism, thermal insulation system, heat-exchange system, crucible holder.Bridgman method is combined by the growth furnace with heat-exchanging method, is specially:Temperature difference during crystal growth is provided by the relative movement between crucible and calandria, the heat exchange platform of crucible bottom and circulation argon gas.The characteristics of the utility model, is, is additionally arranged rotating mechanism so that during crystal growth, around axis uniform rotation while heater and thermal insulation system slowly move up.It can also ensure that thermal field is uniform when so even if calandria designs less reasonable or local fault.

Description

Crystal growing furnace
Technical field
A kind of crystal growing furnace is the utility model is related to, suitable for field of crystal growth.
Background technology
Growing method and equipment have vital influence to the quality for preparing crystal.Common crystal growth side Method has Bridgman method, zone melting method, czochralski method, heat-exchanging method, casting method etc..Currently realize large-scale industrial production Crystal is mainly monocrystalline silicon, polysilicon, and the optimization of polycrystalline silicon ingot or purifying furnace is concentrated mainly on expansion and the thermal field of ingot furnace size Optimization design, and the optimization design of current thermal field is mainly to be set from the optimization of heater shape, position and insulation cage Meter angularly sets out.
The content of the invention
The utility model provides a kind of crystal growing furnace, and chief component is body of heater, takes out blow-off system, heater, liter Rotating mechanism, thermal insulation system, heat-exchange system, crucible holder drop.The growth furnace is by Bridgman method and heat-exchanging method phase With reference to specially:Temperature difference during crystal growth by the relative movement between crucible and calandria, the heat exchange platform of crucible bottom and Argon gas is circulated to provide.Optimization design with current thermal field is mainly from the excellent of heater shape, position and insulation cage Change design angularly to set out and compares, be the characteristics of the utility model, be additionally arranged rotating mechanism so that during crystal growth, heating Around axis uniform rotation while device and thermal insulation system slowly move up.Even if so calandria design is less rationally or local Also it can ensure that thermal field is uniform during failure.
Figure of description
Fig. 1 is the structure chart of the utility model crystal growing furnace.
Mark is in figure(1), rotary lifting mechanism(2), subiculum warming plate(3), stay-warm case(4), air inlet pipe(5), Air inlet pipe(5), bleeding point(6), crucible cover plate(7), crucible guard boards(8), graphite bottom plate(9), crucible(10), carbon felt(11), heat Switching plane(12), graphite column(13), side heater(14), top heater(15), air exchanging hole(16), spout hole (17), overflow blanket(18).In addition, graphite column(13)Between, overflow blanket(18)On be evenly equipped with overflow silk(19).
Embodiment
Particular content of the present utility model is further illustrated below in conjunction with the accompanying drawings:
As shown in figure 1, the crystal growing furnace includes body, takes out blow-off system, heater, lifting rotation mechanism, thermal insulation separation Hot systems, heat-exchange system, crucible holder.Each several part relation is as follows:
Body of heater(1)Rotary lifting mechanism is set on axis(2), rotary lifting mechanism one end is connected with thermal insulation system Connect, thermal insulation system is by being built in body of heater(1)Subiculum warming plate(3)With stay-warm case(4)Composition;Rotary lifting mechanism(2) It is arranged to hollow, inside sets air inlet pipe(5), air inlet pipe(5)With bleeding point(6)Collectively constitute and take out blow-off system, wherein, bleeding point (6)Located at body of heater(1)On, air inlet pipe(5)One end is connected to crucible cover plate(7)And gas exchanges can be kept with crucible;Crucible cover Plate(7), crucible guard boards(8), graphite bottom plate(9)Collectively constitute crucible holder, crucible(10)It is put in crucible holder, and crucible (10)With being provided with carbon felt among crucible rack side wall(11);Graphite bottom plate between crucible(8)Have heat exchange platform (12), heat exchange platform(12)Pass through graphite column(13)It is fixed on body of heater(1)On, heat exchange platform(12)It is passed through with extraction gas Circulation argon gas collectively constitute heat-exchange system;Crucible holder is surrounded by side heater(14), top is heated provided with top Device(15).Wherein, crucible guard boards(8)It is provided with air exchanging hole(16);Warming plate(3)It is provided with spout hole(17);Body of heater(1) Bottom is covered with overflow blanket(18);Graphite column(13)Between, overflow blanket(18)On be evenly equipped with overflow silk(19).
The running of the crystal growing furnace is as follows:The first step, after crucible charge, it is positioned on crucible holder, seals Closed furnace body.
Second step, vacuumize, lead to argon gas, be repeated several times, until stove chamber air drains.
3rd step, temperature program(me), calandria climbing speed, the calandria speed of rotation are set.
4th step, operation.Melting sources heat is provided by side heater and top heater.In running, heating Body rotation rises, and argon gas is taken out, enters circulation, and heat exchange platform three parts provide the temperature difference of crystal growth.If during, crucible is careless Rupture, the melt of spilling can be left by spout hole, when touching the overflow silk between graphite column or on overflow blanket, i.e., can be reported It is alert, avoid the further expansion of loss.

Claims (5)

1. crystal growing furnace, chief component is body of heater, takes out blow-off system, heater, lifting rotation mechanism, insulation system System, heat-exchange system, crucible holder;The physical relationship of each several part is body of heater(1)Rotary lifting mechanism is set on axis(2), rotation Turn elevating mechanism one end with thermal insulation system to be connected, thermal insulation system is by being built in body of heater(1)Subiculum warming plate(3) With stay-warm case(4)Composition;Rotary lifting mechanism(2)It is arranged to hollow, inside sets air inlet pipe(5), air inlet pipe(5)With bleeding point(6) Collectively constitute and take out blow-off system, wherein, bleeding point(6)Located at body of heater(1)On, air inlet pipe(5)One end is connected to crucible cover plate (7);Crucible cover plate(7), crucible guard boards(8), graphite bottom plate(9)Collectively constitute crucible holder, crucible(10)It is put in crucible holder In, and crucible(10)With being provided with carbon felt among crucible rack side wall(11);Graphite bottom plate between crucible(9)Have hot friendship Change platform(12), heat exchange platform(12)Pass through graphite column(13)It is fixed on body of heater(1)On, heat exchange platform(12)With extraction The circulation argon gas that gas is passed through collectively constitutes heat-exchange system;Crucible holder is surrounded by side heater(14), top is provided with top Portion's heater(15).
2. crystal growing furnace as claimed in claim 1, it is characterised in that crucible guard boards(8)It is provided with air exchanging hole(16).
3. crystal growing furnace as claimed in claim 1, it is characterised in that warming plate(3)It is provided with spout hole(17).
4. crystal growing furnace as claimed in claim 1, it is characterised in that body of heater(1)Bottom is covered with overflow blanket(18).
5. crystal growing furnace as claimed in claim 1, it is characterised in that graphite column(13)Between, overflow blanket(18)It is upper uniform There is overflow silk(19).
CN201721005669.5U 2017-08-12 2017-08-12 Crystal growing furnace Active CN207109142U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201721005669.5U CN207109142U (en) 2017-08-12 2017-08-12 Crystal growing furnace

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201721005669.5U CN207109142U (en) 2017-08-12 2017-08-12 Crystal growing furnace

Publications (1)

Publication Number Publication Date
CN207109142U true CN207109142U (en) 2018-03-16

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN201721005669.5U Active CN207109142U (en) 2017-08-12 2017-08-12 Crystal growing furnace

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CN (1) CN207109142U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110158151A (en) * 2019-06-21 2019-08-23 河北普兴电子科技股份有限公司 For the crucible cover of silicon carbide monocrystal growth, crucible and the method for crystal growth
CN114959871A (en) * 2022-06-16 2022-08-30 西安交通大学 Heat radiation structure of single crystal casting furnace and single crystal casting furnace

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN110158151A (en) * 2019-06-21 2019-08-23 河北普兴电子科技股份有限公司 For the crucible cover of silicon carbide monocrystal growth, crucible and the method for crystal growth
CN114959871A (en) * 2022-06-16 2022-08-30 西安交通大学 Heat radiation structure of single crystal casting furnace and single crystal casting furnace

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