CN206330819U - A kind of device for being used to filter large volume water sample - Google Patents
A kind of device for being used to filter large volume water sample Download PDFInfo
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- CN206330819U CN206330819U CN201621213093.7U CN201621213093U CN206330819U CN 206330819 U CN206330819 U CN 206330819U CN 201621213093 U CN201621213093 U CN 201621213093U CN 206330819 U CN206330819 U CN 206330819U
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Abstract
The utility model is related to a kind of device for being used to filter large volume water sample, and specifically a kind of auxiliary frame and auxiliary device for the live water sample filtering of large volume belongs to ocean water quality process field.A kind of device for being used to filter large volume water sample, including sample filtering mechanism, automatic liquid-feeding structure and auxiliary frame, the sample filtering mechanism includes the cylindrical sample bottle for being used to contain water sample to be filtered, the sample bottle bottom end outlet, which is connected, is provided with ball valve in stainless steel tube, the stainless steel tube;The bottom end opening portion of the stainless steel tube inserts the first half of sand core funnel;In the sand core funnel bottom end opening portion insertion conical collection bottle.Using the large volume water sample filtering in the utility model and the servicing unit of automatic liquid-feeding, the automatic fitration and dosing of large volume water sample can be achieved, saves and repeatedly operates repeatedly.
Description
Technical field
The utility model is related to a kind of device for being used to filter large volume water sample, specifically a kind of to be used for substantially
The auxiliary frame and auxiliary device of product scene water sample filtering, belong to ocean water quality process field.
Background technology
With the development that China's ocean development and marine protection work, marine environmental monitoring and investigation work are increasingly frequent,
And the water sample that marine monitoring inquiry agency is adopted generally requires to be filtered and dosing (fixative) is stored refrigerated afterwards, to ensure
The validity of sample data.
The filtering of water sample is general according to National Standard of the People's Republic of China (GB17378.3- in marine environment investigation
2007) method in is carried out, and is measured certain volume water sample into sand core funnel, using Vacuum filtration device, is passed through 0.45 micron
Fibrous filter membrane filtered (wherein heavy metal water sample need to adjust pH value to less than 2), the water sample after all filterings need to refrigerate guarantor
Deposit, final transport to laboratory is analyzed.Filter in GB17378.3-2007 is adopted always during marine monitoring works
Traditional water sample filter, general sand core funnel volume is generally used, bottom is without fixation in an experiment in 0.5-1L
Device (is used) in land laboratory.
Laboratory on the important step that sample filtering works as marine environment investigation sample pre-treatments, ocean monitoring ship
Often the very first time filters to field sample, for the water sample of some routine monitoring indexs, such as nutrient salts (inorganic nitrogen,
Reactive phosphate), heavy metal (copper, lead, zinc, cadmium etc.), chlorophyll a etc., often only need to filter 0.1-1L or so water quality sample
Product, you can meet refrigeration and preserve the minimum volume requirement of sample., can in the water sample filter process of routine monitoring index
So that the volume of water sample number of required sample is well disposably poured into the funnel of filter with measurer amount, it is to be filtered be about at the end of plus
Enter the filter process that the medicines such as fixative just complete such assay.But working as needs the specific of high-volume measure in monitoring
When water sample volume is larger needed for index, such as the measure (polycyclic aromatic hydrocarbon, benzene homologues) of some organic indexs, often
Need to filter 4-10L seawater sample and add the medicines such as fixative, this kind of monitoring index sample volume exceeds well over core often
The capacity (generally 0.5-1L) of funnel, it is impossible to the water sample of required volume was just added to sand core funnel once or several times
In, and organic assay often requires that filtering terminates or adds another liquid (fixative class medicine at the end of being bordering on
Product), this just forces the scientific research personnel on ship to expend considerable time and effort and measured to carry out the volume of seawater sample, count with
Dosing.In addition, cabin where marine experimental implementation is general very narrow, space is limited, and liquid is measured using multigroup large volume measuring device
Body is natively very inconvenient, if the bulk sample of high-volume filtering simultaneously, easily causes operation chaotic and personnel wastes, and
When the sea is rough, for security consideration, or even sample filtering work can only be stopped.On the other hand, even in normal work
Under the conditions of, the funnel volume of conventional water filter be it is fixed, it is temporarily customized for different marine monitoring tasks and index
Many size large volume filters are very inconvenient and actual.To sum up, considered based on above real work situation, one kind can be with
The design and use of servicing unit for filtering large volume water sample and Automatic Dosing liquid are current marine environmental monitoring works
In work in the urgent need to.
The content of the invention
The purpose of this utility model is to provide a kind of sample pretreatment apparatus (the large volume water quality of marine monitoring field investigation
Sample filtering), specifically a kind of auxiliary frame and auxiliary device for the live water sample filtering of large volume, using this reality
The sample treatment efficiency of marine monitoring personnel can be obviously improved with the device of new offer, simplifies sample filtering flow and improves work
Make comfort level.
A kind of device for being used to filter large volume water sample, including sample filtering mechanism, automatic liquid-feeding structure and auxiliary
Frame,
The sample filtering mechanism includes the cylindrical sample bottle for being used to contain water sample to be filtered, the sample bottle bottom
Bring out in mouth connection stainless steel tube, the stainless steel tube and be provided with ball valve;The bottom end opening portion insertion core leakage of the stainless steel tube
The first half of bucket;In the sand core funnel bottom end opening portion insertion conical collection bottle;
The automatic liquid-feeding structure includes a medicinal liquid bottle, and the medicinal liquid bottle top export connects soft air inlet pipe, soft
The other end of air inlet pipe inserts the first half of sand core funnel;The medicinal liquid bottle bottom end outlet connects soft liquid-feeding tube, soft liquid feeding
The other end of pipe inserts the first half of sand core funnel.
The device described in the utility model for being used to filter large volume water sample includes sample filtering mechanism, automatic liquid-feeding knot
Sample filtering mechanism and automatic liquid-feeding structure are integrally fastened to wherein by structure and auxiliary frame, the auxiliary frame.Wherein, the cylinder
Shape sample bottle is set with bottleneck towards the direction on ground, and bottleneck is sealed using bottle stopper, and one is fixed in bottle stopper has ball valve and sufficient
Enough thick stainless steel tubes, stainless steel tube connection sample bottle.The cylindrical sample bottle is preferably the sample that volume is more than 4L vials
Product bottle, the need for meeting the detection of large volume water sample.The body of the further preferred sample bottle is provided with scale.Using
Metal material outlet pipe is the influence in order to prevent the organic materials such as plastics to organic index to be measured in water sample.Stainless steel tube
The mouth of pipe probe into the sand core funnel first half, sample is disposably loaded sample bottle by water sample when filtering, then is fixed on auxiliary frame
After turn in ball valve, sand core funnel when water sample liquid level is less than the stainless steel tube mouth of pipe that sample is automatic to flow from sample bottle
Go out, when sample liquid level is higher than the stainless steel tube mouth of pipe because the equilibrium relation of atmospheric pressure ensures that fluid sample too fast will not outflow
Cause to overflow edge on sand core funnel, sample bottle stainless steel tube valve can be closed when there is temporary condition to interrupt filtering, suspend
Operation.In whole filtering servicing unit, outlet pipe (stainless steel tube) caliber on sample bottle is than larger (D water outlets bore/D
Sample bottle internal diameter is not less than 1/5, preferably 1/5), it is ensured that have gas to enter sample simultaneously during fluid sample flows out
Bottle, could so maintain air pressure in sample bottle not decline always, water sample to be filtered is smoothly flowed slowly into sand core funnel
In.
The effect of medicinal liquid bottle is to be automatically added to decoction after whole volume water samples completion filterings in sample bottle (to fix
Agent) into sand core funnel, be preferably separatory funnel, (selection of separatory funnel can determine volume according to fixative addition) and
Two flexible hose compositions, separatory funnel bottom connects liquid-feeding tube, the plug connection air inlet pipe in top apparatus hole, air inlet pipe lower half
Probe into that sand core funnel is needed plus (fixative class decoction is thrown when being usually the remaining a small amount of liquid in sand core funnel for the position of decoction
Plus), when sample liquid level is less than the position of the separatory funnel air inlet mouth of pipe in sand core funnel, air can enter separatory funnel, make point
Air pressure is balanced with ambient pressure in liquid funnel, and decoction is automatically flowed into sand core funnel along liquid-feeding tube, realizes Automatic Dosing.Sample
Bottle can be fixed on auxiliary frame with medicinal liquid bottle, can highly be adjusted according to factors such as sample bottle sizes, whole auxiliary frame can be fixed
On the table, be prevented from filter because ship is rocked with stormy waves bring topple over risk.
In above-mentioned technical proposal, " sand core funnel " is commercially available, and those skilled in the art can be according to treating capacity etc.
Selected.The sand core funnel has cup type profile, is provided with filter membrane at the middle part of its inner chamber, the filter membrane is by sand core funnel
Inner chamber is divided into the first half and the part of lower half two.
Auxiliary frame described in the utility model, which includes two, has mutually isostructural support side plate, square floor and overall structure
Part, wherein,
Described two support side plates are staggered relatively, and mutually fixed with two sides of base plate;The base plate center has circle
Hole;Two row tooth form grooves are provided with the first half of support side plate;
The integrated member by two there are mutually isostructural component side plate and three fixed plates to constitute;Fixed plate I and solid
Fixed board III is mutually fixed with the top and bottom of two component side plates respectively, and fixed plates II is fixed on the middle part of component side plate;It is described
Fix two fixed columns on the outside of component side plate, the integrated member is by the way that fixed column to be installed on to the tooth forms of two support side plates
Mutually fixed with support side plate in groove;The center of the fixed plate I, fixed plates II and fixed plates II I is equipped with circular opening, its
In, the circular opening diameter on fixed plates II I is less than the diameter of section of sample bottle and not less than the diameter of section of bottleneck.
Two support side plates described in the utility model are staggered relatively, and mutually fixed with two sides of base plate, form U-shaped knot
Structure, further, device described in the utility model two sides that preferably square floor is not fixed mutually with support side plate
Upper fixing support rack;Described four angles of base plate are provided with the hole for being used for assembling bolt.Can will be auxiliary using above-mentioned hole and support frame
Support is helped to be fixed on desk or on deck.The base plate center has circular opening, the diameter of the circular opening preferably with receipts
Collect bottle bottom of bottle diameter identical, or slightly larger than bottom of bottle diameter, play certain fixation.
Further, the auxiliary frame, which can also include two, has mutually isostructural portable plate, the portable plate side
Provided with semicircle hole, opposite side is fixed in support side plate by hinge;Portable plate has the side of the side of semicircle hole
Ferrite members are fixed at angle;Be provided with magnet in the middle part of support side plate, the position of the magnet cause portable plate parallel to
During ground, magnet is completely attached to ferrite members.
Above-mentioned two portable plate can be rocked in hull comparison it is violent when the fixed receiving flask of auxiliary, when needed, will
Two portable plates are lifted, using the magnet on the ferrite members and support side plate on portable plate by portable plate be maintained at level with
On the position on ground.
It is described in the utility model be used to filtering the device integrated member, portable plate, base plate of large volume water sample according to by
Sequentially it is fixed under up between two support side plates.During assembling, sample bottle is arranged in integrated member, the bottleneck of sample bottle
In the hole for inserting fixed plates II I centers, the bottleneck of sample bottle fixes bottle stopper stainless steel tube, stainless steel tube insertion sand core funnel
Top;In the bottom insertion receiving flask of sand core funnel, receiving flask is fixed in the hole at base plate center.
Further, there is the square sheet material of circular opening, the circular opening centered on the fixed plate I main body
Not less than sample bottle diameter of section;There is circular opening centered on fixed plate I body side fixed salient, the protuberance
Square sheet material;There is the square sheet material of circular opening, the circular opening is not less than sample centered on the fixed plates II
Bottle diameter of section;There is the square sheet material of circular opening centered on the fixed plates II I.
Using above-mentioned integrated member, it can be fixed on auxiliary frame, have centered on the fixed plates II I by what sample bottle was consolidated
There is the square sheet material of circular opening, and the circular opening diameter on fixed plates II I is less than the diameter of section of sample bottle and not small
In the diameter of section of bottleneck.Sample bottle can be installed on to fixed plates II I top, preferably fixed plates II I using said apparatus
On circular opening diameter be less than the diameter of section and the equal or slightly larger than diameter of section of bottleneck of sample bottle.The utility model institute
State the device preferably fixed plate I, fixed plates II and fixed plates II I and be provided with the passage being used for by air inlet pipe and liquid-feeding tube.
The device described in the utility model preferably medicinal liquid bottle is separatory funnel.In order that consolidating of can consolidating of separatory funnel
It is scheduled on auxiliary frame, the diameter of the circular opening at the protuberance center is less than the diameter at separatory funnel maximum cross-section.
The preferred described device of device described in the utility model includes vavuum pump, and the vavuum pump connects receiving flask;The branch
Supportting side plate and being provided with is used for the through hole through vavuum pump pipeline.
The beneficial effects of the utility model are:In the sample pretreatment work of marine monitoring field investigation, filtered sample
It is necessary operating procedure, for the filtering of high-volume large volume water sample, because cabin where marine experimental implementation is general
Very narrow, space is limited, measures liquid using multigroup large volume measuring device very inconvenient, easily causes operation chaotic, and work as
When the sea is rough, for security consideration, or even sample filtering work can only be stopped.Using the large volume water quality sample in the present invention
Product filtering and the servicing unit of automatic liquid-feeding, can be achieved the automatic fitration and dosing of large volume water sample, save repeatedly repeatedly
Operation, allows the monitoring personnel at sea while filtering large batch of large volume water sample, saves substantial amounts of manpower and energy,
Avoid the process that operating personnel constantly repeat to measure, count, add sample and medicament when filtering bulk sample, Yi Jicao
Error and chaotic possibility, improve operating efficiency, simplify workflow when making.
Brief description of the drawings
Fig. 1 is for the schematic diagram for the device for filtering large volume water sample;
Fig. 2 is the schematic diagram of sample bottle;
Fig. 3 is the schematic diagram of medicinal liquid bottle;
Fig. 4 is the schematic diagram of auxiliary frame support side plate;
Fig. 5 is the schematic diagram of auxiliary frame integrated member;
Fig. 6 (a)~(f) is respectively base plate, portable plate, fixed plates II, fixed plate I, fixed plates II I, component side plate
Schematic diagram.
Embodiment
Following non-limiting examples can make one of ordinary skill in the art be more fully understood the present invention, but not with
Any mode limits the present invention.
Test method described in following embodiments, unless otherwise specified, is conventional method;The reagent and material, such as
Without specified otherwise, commercially obtain.
Embodiment 1
A kind of device for being used to filter large volume water sample, including sample filtering mechanism, automatic liquid-feeding structure and auxiliary
Frame 1,
The sample filtering mechanism includes the cylindrical sample bottle 2 for being used to contain water sample to be filtered, the sample bottle 2
Bottom end outlet, which is connected, is provided with ball valve 202 in stainless steel tube 201, the stainless steel tube 201;Open the bottom of the stainless steel tube 201
Oral area inserts the first half of sand core funnel 4;In the bottom end opening portion of the sand core funnel 4 insertion conical collection bottle 5;
The automatic liquid-feeding structure includes a medicinal liquid bottle 3, and the top export of medicinal liquid bottle 3 connects soft air inlet pipe 301,
The other end of soft air inlet pipe 301 inserts the first half of sand core funnel 4;The medicinal liquid bottle bottom end outlet connects soft liquid-feeding tube
302, the other end of soft liquid-feeding tube 302 inserts the first half of sand core funnel 4.
Sample filtering mechanism and automatic liquid-feeding structure are integrally fastened to wherein by the auxiliary frame 1.Wherein, the cylinder
Sample bottle 2 is set with bottleneck towards the direction on ground, and bottleneck is sealed using bottle stopper, and one is fixed in bottle stopper has the stainless of ball valve
Steel pipe 201, the connection sample bottle 2 of stainless steel tube 201.The vial sample bottle that the cylindrical sample bottle 2 is volume 4L.Sample bottle
2 body is provided with scale.The internal diameter of 201 caliber D/ sample bottles of stainless steel tube 2 is 1/5 on sample bottle 2.
The auxiliary frame 1, which includes two, has mutually isostructural support side plate 108, square floor 101 and integrated member,
Wherein, described two support side plates 108 are staggered relatively, and mutually fixed with 101 two sides of base plate;The center of base plate 101 tool
There is circular opening;Two row tooth form groove 108a are provided with the first half of support side plate 108;
Described two support side plates 108 are staggered relatively, and mutually fixed with 101 two sides of base plate, form U-shaped structure, institute
State fixing support rack 101a on two sides that square floor 101 is not fixed mutually with support side plate 108;The base plate 101 4
Individual angle is provided with the hole for being used for assembling bolt.The center of base plate 101 has circular opening, the diameter of the circular opening and collection
Bottle bottom of bottle diameter is identical.
The auxiliary frame 1, which includes two, has mutually isostructural portable plate 102, and the side of portable plate 102 is provided with semicircle
Shape hole, opposite side is fixed on side plate 108 by hinge;The edge that portable plate 102 has the side of semicircle hole is consolidated
Determine ferrite members 102a;Magnet 108b is provided with the middle part of support side plate 108, the position of the magnet 108b causes portable plate
102 when parallel to ground, and magnet 108b and ferrite members 102a is completely attached to.
The integrated member by two there are mutually isostructural component side plate 106 and three fixed plates to constitute;Fixed plate
I103 and fixed plates II I105 are mutually fixed with the top and bottom of two component side plates 106 respectively, and fixed plates II 104 is fixed on structure
The middle part of part side plate 106;Two fixed column 106a are fixed in the outside of the component side plate 106, and the integrated member passes through admittedly
Fixed column 106a is installed in the tooth form groove 108a of two support side plates 108 and mutually fixed with support side plate 108;The fixed plate
I103, fixed plates II 104 and fixed plates II I105 center are equipped with circular opening, wherein, the circle on fixed plates II I105
Hole diameter is less than the diameter of section of sample bottle 2 and equal to the diameter of section of bottleneck.
There is the square sheet material of circular opening, the circular opening is not less than sample centered on the main body of fixed plate I 103
Product 2 diameter of sections of bottle;There is circular port centered on fixed plate I 103 body side fixed salient 103a, the protuberance 103a
The square sheet material in hole;There is the square sheet material of circular opening, the circular opening is not small centered on the fixed plates II 104
In the diameter of section of sample bottle 2;There is the square sheet material of circular opening centered on the fixed plates II I105.
Using above-mentioned integrated member, sample bottle 2 is installed on to the circle on fixed plates II I105 top, fixed plates II I105
Shape hole diameter is less than the diameter of section of sample bottle 2 and equal to the diameter of section of bottleneck.The fixed plate I 103, fixed plate
II104 and fixed plates II I105 is provided with the passage being used for by air inlet pipe 301 and liquid-feeding tube 302.The medicinal liquid bottle 3 is a point liquid leakage
Bucket.In order that being fixed on auxiliary frame of can consolidating of separatory funnel, the diameter of the circular opening at the protuberance 103a centers
Less than the diameter at separatory funnel maximum cross-section.Described device includes vavuum pump 6, and the vavuum pump connects receiving flask 5;The branch
Supportting side plate 108 and being provided with is used for the through hole through vavuum pump pipeline.
Claims (10)
1. a kind of device for being used to filter large volume water sample, it is characterised in that:Including sample filtering mechanism, automatic liquid-feeding knot
Structure and auxiliary frame (1),
The sample filtering mechanism includes the cylindrical sample bottle (2) for being used to contain water sample to be filtered, the sample bottle (2)
Ball valve (202) is provided with bottom end outlet connection stainless steel tube (201), the stainless steel tube (201);The stainless steel tube (201)
Bottom end opening portion insertion sand core funnel (4) the first half;Sand core funnel (4) the bottom end opening portion insertion conical collection bottle
(5) in;
The automatic liquid-feeding structure includes a medicinal liquid bottle (3), and medicinal liquid bottle (3) top export connects soft air inlet pipe
(301), the first half of the other end insertion sand core funnel (4) of soft air inlet pipe (301);The medicinal liquid bottle bottom end outlet connection is soft
Matter liquid-feeding tube (302), the first half of the other end insertion sand core funnel (4) of soft liquid-feeding tube (302).
2. device according to claim 1, it is characterised in that:The auxiliary frame (1) includes two with mutually isostructural
Support side plate (108), square floor (101) and integrated member, wherein,
Described two support side plates (108) are staggered relatively, and mutually fixed with (101) two sides of base plate;In the base plate (101)
The heart has circular opening;Two row tooth form grooves (108a) are provided with the first half of support side plate (108);
The integrated member by two there are mutually isostructural component side plate (106) and three fixed plates to constitute;Fixed plate I
(103) mutually fixed with top and bottom of the fixed plates II I (105) respectively with two component side plates (106), fixed plates II (104)
It is fixed on the middle part of component side plate (106);Two fixed columns (106a) are fixed on the outside of the component side plate (106), it is described whole
Fixed column (106a) by being installed in the tooth form grooves (108a) of two support side plates (108) and support side plate by body component
(108) mutually fix;The center of the fixed plate I (103), fixed plates II (104) and fixed plates II I (105) is equipped with circular port
Hole, wherein, the circular opening diameter on fixed plates II I (105) is less than the diameter of section of sample bottle (2) and cutting not less than bottleneck
Face diameter.
3. device according to claim 1, it is characterised in that:The auxiliary frame (1) includes two with mutually isostructural
Portable plate (102), portable plate (102) side is provided with semicircle hole, and opposite side is fixed on support side plate by hinge
(108) on;The edge that portable plate (102) has the side of semicircle hole fixes ferrite members (102a);
Magnet (108b) is provided with the middle part of support side plate (108), the position of the magnet (108b) causes portable plate (102)
When parallel to ground, magnet (108b) is completely attached to ferrite members (102a).
4. device according to claim 2, it is characterised in that:
There is the square sheet material of circular opening, the circular opening is not less than sample centered on fixed plate I (103) main body
Bottle (2) diameter of section;Have centered on fixed plate I (103) body side fixed salient (103a), the protuberance (103a)
The square sheet material of circular opening;
There is the square sheet material of circular opening, the circular opening is not less than sample bottle centered on the fixed plates II (104)
(2) diameter of section;
There is the square sheet material of circular opening centered on the fixed plates II I (105).
5. device according to claim 4, it is characterised in that:The medicinal liquid bottle (3) is separatory funnel.
6. device according to claim 5, it is characterised in that:The diameter of the circular opening at protuberance (103a) center
Less than the diameter at separatory funnel maximum cross-section.
7. device according to claim 4, it is characterised in that:The fixed plate I (103), fixed plates II (104) and fixation
Plate III (105) is provided with the passage being used for by air inlet pipe (301) and liquid-feeding tube (302).
8. device according to claim 2, it is characterised in that:The square floor (101) not with support side plate (108)
Fixing support rack (101a) on two sides mutually fixed;Described (101) four angles of base plate are provided with the hole for being used for assembling bolt.
9. device according to claim 1, it is characterised in that:Internal diameter/sample bottle internal diameter of the stainless steel tube (201) is
1/5。
10. device according to claim 2, it is characterised in that:Described device includes vavuum pump (6), the vavuum pump (6)
Connect receiving flask (5);The support side plate (108), which is provided with, is used for the through hole through vavuum pump pipeline.
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201621213093.7U CN206330819U (en) | 2016-11-10 | 2016-11-10 | A kind of device for being used to filter large volume water sample |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN201621213093.7U CN206330819U (en) | 2016-11-10 | 2016-11-10 | A kind of device for being used to filter large volume water sample |
Publications (1)
Publication Number | Publication Date |
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CN206330819U true CN206330819U (en) | 2017-07-14 |
Family
ID=59287612
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
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CN201621213093.7U Expired - Fee Related CN206330819U (en) | 2016-11-10 | 2016-11-10 | A kind of device for being used to filter large volume water sample |
Country Status (1)
Country | Link |
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CN (1) | CN206330819U (en) |
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2016
- 2016-11-10 CN CN201621213093.7U patent/CN206330819U/en not_active Expired - Fee Related
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